• Title/Summary/Keyword: Hemicellulose

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Extraction of Hemicellulosic Sugar and Acetic Acid from Different Wood Species with Pressurized Dilute Acid Pretreatment

  • Um, Byung-Hwan;Park, Seong-Jik
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.2
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    • pp.172-182
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    • 2014
  • Extraction is a necessary element in the bioconversion of lignocellulosics to fuels and chemicals. Although various forms of chemical pretreatment of cellulosic materials have been proposed, their effectiveness varies depending on the treatment conditions and substrate. In this study, mixed hardwood (MH) and loblolly pine (LP) were pretreated with dilute acid in a 100 mL accelerated solvent extraction (ASE) at the predetermined optimal conditions: temperature: $170^{\circ}C$, acid concentration: 0.5% (w/v), and reaction time: 2~64 min. This method was highly effective for extracting the hemicellulose fraction. Total xmg (defined as the sum of xylose, mannose, and galactose) can be extracted from milled MH and LP through pressurized dilute acid treatment in maximum yields of 12.6 g/L and 15.3 g/L, respectively, representing 60.5% and 70.4% of the maximum possible yields, respectively. The crystallinity index increased upon pretreatment, reflecting the removal of the amorphous portion of biomass. The crystalline structure of the cellulose in the biomass, however, was not changed by the ASE extraction process.

Effect of Enzyme Retting on the Fiber Separation of Kenaf Bast - influence of chelator - (효소 레팅에 의한 케냐프 섬유의 분리 -킬레이터의 영향-)

  • 이혜자;안춘순;김정희;유혜자;한영숙;송경헌
    • Journal of the Korean Society of Clothing and Textiles
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    • v.28 no.7
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    • pp.873-881
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    • 2004
  • This research was aimed to investigate the effect of enzyme and the addition of chelators on rotting of the Kenaf bast. Enzyme rotting was effective only when the chelators were added with the enzyme. EDTA was a more effective chelator than oxalic acid under 1% concentration. There was no difference in the rotting effect under different enzyme concentration levels, and under different treatment time and temperature. Therefore, it was found that enzyme rotting can be carried out with low enzyme concentration(0.125%) at room temperature. Retting time can be shortened when higher enzyme concentration and higher temperature are applied. Cellulose I structure of kenaf fiber did not change after enzyme rotting, and different enzyme concentration did not affect the crytallinity structure. Non-cellulosic matters such as hemicellulose, lignin, and pectin were present in the descending order in the enzyme rotted kenaf fiber, and there were no differences in their amounts due to enzyme concentration levels. There was no difference in the dyeabilities of kenaf fiber rotted with different enzyme concentration levels. Enzyme rotted kenaf fiber showed better cyeability when pectin, lignin, and hemicellulose were removed.

Analysis on the Components of Brown Spot occurred in the Papers (지류에 발생하는 얼룩반점의 성분분석에 관하여)

  • Park, Seh-Youn;Lee, Kyu-Shik;Han, Sung-Hee;Ahn, Hee-Kyun
    • 보존과학연구
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    • s.13
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    • pp.81-95
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    • 1992
  • The old books which have been colored to brown spots were analyzed chemically to compare with white part. The original raw materials were paper mulberry (Broussonetia Kazine) and woodpulp. White part contained58.8%($\alpha$-37.2%,$\beta$-8.6%, $\gamma$-12.7%)cellulose, 21.7% hemicellulose, 19.8% lignin,4.4% pentosan and brown sopt part contained 49.1%($\alpha$-19.8%, $\beta$-14.5%,$\gamma$-14.8%) cellulose, 27.1% hemicellulose, 23.8% lignin, 4.8% pentosan. Both of brown spot and white parts contained starch without protein. The pH was 4.9 in brown and 5.0 in white part respecitively. The brown spot parts were more solidified than white parts according to SEM observation. Difference of organiccompinent in brown part came from white part were 2-hydroxy-benzaldehydeand phenol.

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Changes of Sugar Components in Cell Wall Polysaccharides from Tomato Fruits during Ripening (토마토 과실의 성숙중 세포벽 구성다당류의 변화)

  • Mun, Gwang-Deok;Cheon, Seong-Ho;Kim, Jong-Guk
    • Food Science and Preservation
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    • v.3 no.2
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    • pp.113-120
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    • 1996
  • This study was conducted to understand the characteristics of fruit softening during ripening which causes deep loses in quality of horticultural products during storage and marketing process after harvest. The changes of cell wall components during ripening was investigated. The climacteric rise was between 42 and 49 days after anthesis and then decreased. Ethylene evolution was similar to respiration. The hardness of fruit decreased markedly at this climacteric period and significances of textural parameters among the ripening periods were recognized but the significance between 50 and 55 days after anthesis was not. Sugar components of cell wall polysaccharides were uronic acid, galactose, glucose, arabinose, xylose, rhamnose, mannose and fucose. The contents of arabinose and mannose in alcohol-insoluble solids fraction increased, but other sugars were not changed. In cell wall fraction, the contents of uronic acid, galactose, glucose and arabinose were comparatively high, but galactose, arabinose and ironic acid were decreased markedly during ripening. ironic acid occupied above 75% of total monosaccharide in pectin fraction and decreased markedly during ripening. In acid-soluble hemicellulose fraction, the contents of uronic acid, glucose, galactose and rhamnose were high and they decreased from 50 days after anthesis. The contents of glucose and xylose were high in a alkali-soluble hemicellulose fraction and they decreased markedly at 55days after anthesis.

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Differences in Nutrient Quality among Rape Varieties for Oil Seed and Forage

  • Kwon, Byung-Sun;Lim, June-Taeg;Shin, Jeong-Sik;Ahn, Gae-Soo;Park, Hee-Jin
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.48 no.5
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    • pp.372-375
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    • 2003
  • In order to examine the possibility that oil seed rape could be used as a forage fodder crop and to select the most suitable variety of forage rape at the southern area of Korea, two varieties of oil seed rape currently grown for oil production and six introduced varieties of forage rape with relatively high yield and high nutritional value were grown at the same condition and their nutritional value were observed. Generally, rape was considered as a useful forage fodder crop with high content of crude protein and low contents of NDF, ADF, hemicellulose, cellulose and lignin. Differences in mean values of the above characters between two groups of rape were not statistically significant. Velox showed significantly higher content of crude protein and significantly lower contents of NDF, ADF, hemicellulose, cellulose and lignin compared with other varieties of forage rape. Rape was relatively high in IVDMD compared with other forage fodder crops, and forage rape was more or less higher in IVDMD and DDMM than oil seed rape. Velox was the highest in IVDMD and DDMM among the varieties of forage rape in this experiment.

Changes of Texture in terms of the Contents of Cellulose, Hemicellulose and Pectic Substances during Fermentation of Radish Kimchi (숙성 기간에 따른 무우 김치의 텍스쳐와 섬유소, 헤미셀루로오스, 펙틴질의 함량 변화)

  • Jung, Guy-Hwa;Lee, Hei-Soo
    • Korean journal of food and cookery science
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    • v.2 no.2
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    • pp.68-75
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    • 1986
  • The changes of dietary fiber and texture of radish Kimchi fermented at $17{\sim}20^{\circ}C$ were investigated. During the fermentation period, hardness and brittleness of radish Kimchi were decreased. The changes were more marked in the brittleness. But the contents of cellulose and hemicellulose were not changed considerably. The contents of AIS was decreased with fermentation. During the fermentation, hot soluble pectin was increased and protopection was decreased but the amount of changes was small. The texture of radish Kimchi was affected by contents of pectic subsrances, especially protopectin. The coefficient of correlation between hardness and protopectin contents was 0.85.(=r)

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Effects of Dietary Fiber on Lipid Metabolism of Albino Rats (보리의 식이섬유소(食餌纖維素)가 흰쥐의 지질대사(脂質代謝)에 미치는 영향(影響))

  • Kim, Yeong Soo;Min, Byeong Yong;Seo, Gi Bong
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.12 no.4
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    • pp.310-315
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    • 1983
  • The effects of DFP(Dietary Fiber Preparation) extracted from naked barley on the lipid metabolism of rats were investigated. 1. The composition of DFP was determined as cellulose 19.3%, hemicellulose 58.7%, lignin 10.5 % on dry weight basis. 2. DFP had no significant effect on the growth of rats. (p>0.05) 3. DFP had no significant effects on the composition of serum lipid and the lipid content per g of liver in rats, but caused significant decrease in serum and liver cholesterol levels of rats to a certain degree. (p<0.05)

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Characteristics and Effects of Radiation Treatment on Wood Pulping Process (목재 펄프 제조 공정에서의 방사선 효과 및 특성)

  • Won, So Ra;Shin, Hye Kyoung;Jeun, Joon Pyo;Kang, Phil Hyun
    • Journal of Radiation Industry
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    • v.5 no.3
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    • pp.227-230
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    • 2011
  • Pulps were separated from wood chips using an Electron beam irradiation (EBI) treatment without a NaOH-AQ (anthraquinone) treatment for cooking. The methods were based on a hot water treatment after EBI and two-step bleaching processes. Chemical compositions and FT-IR spectroscopy demonstrated that the content of lignin and hemicellulose in the bleached wood pulps treated with various EBI dose decreased with an increase of EBI doses. Specifically, the lignin in the bleached with pulps treated at 600 kGy of EBI dose was almost completely removed. Moreover, TGA analysis showed that a thermal stability increased with increasing the content of cellulose but the lignin decomposed slowly over the wide region.

Effects of Activated Carbon and Charcoal on in vitro Nutrient Disappearances and Ruminal Fermentation Characteristics (고농후사료에 대한 목탄 및 활성탄의 첨가 수준이 인공위내 소화율, 휘발성 지방산 및 개스 생산량에 미치는 영향)

  • Lee, Soo-Kee;Cha, Sang-Woo;Kim, Sun-Kyun
    • Korean Journal of Agricultural Science
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    • v.29 no.2
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    • pp.35-42
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    • 2002
  • This study was conducted to investigate the effects of the addition of activated charcoal (AC) and oak charcoal on in vitro ruminal fermentation characteristics, nutrient disappearance, and ruminal gas production. AC and oak charcoal were added at the levels of 0.50, and 1.00 % to experimental diet (roughage/concentrate ratio ; 2/8). Ruminal pH and ammonia-N tended to increase by adding AC(P<0.05). But oak charcoal did not affect the ruminal pH and ammonia-N. Although not significant, ruminal total VFA and molar percentage of butyric acid tended to decrease in AC diets. but molar percentage of acetate and propionate were not affected by adding AC. Ruminal degradation of dry matter, crude protein, NDF, and ADF in AC diets tended to increase than in non-AC diet, however, no tendency in ruminal degradation of hemicellulose was observed. Ruminal gas production tended to increase in the AC and oak charcoal diets(P<0.05). Although there appeared some beneficial effects in adding AC to ruminant diets in this study, more works should be done with AC before we can make clear conclusion on the use of AC in the ruminant diets.

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Effects of body weight and fiber sources on fiber digestibility and short chain fatty acid concentration in growing pigs

  • Zhao, Jinbiao;Liu, Xuzhou;Zhang, Yi;Liu, Ling;Wang, Junjun;Zhang, Shuai
    • Asian-Australasian Journal of Animal Sciences
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    • v.33 no.12
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    • pp.1975-1984
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    • 2020
  • Objective: The study was conducted to determine the effects of body weight (BW) and fiber sources on nutrient digestibility, fiber fermentation and short chain fatty acids (SCFA) concentration in different intestinal segments of growing pigs fed high-fiber diets. Methods: Nine barrows with initial BW of 25.17±0.73 kg and 9 barrows with initial BW of 63.47±2.18 kg were allotted to a duplicate 9×2 Youden Square design with 3 dietary treatments and 2 periods. The dietary treatments were formulated with 3 different high-fiber ingredients: corn bran, sugar beet pulp, and soybean hulls, respectively. Each diet was fed to 3 barrows with different stage of BW in each period. Results: There were no differences in the apparent ileal digestibility (AID) of most nutrients between pigs at different BW stages. Pigs at 60 kg had greater (p<0.05) apparent total tract digestibility (ATTD) of total dietary fiber (TDF), soluble dietary fiber (SDF) and insoluble dietary fiber (IDF), and had greater (p<0.05) hindgut disappearance of IDF and cellulose than pigs at 25 kg. The acetate, propionate and total SCFA concentrations in ileal digesta and feces of pigs at 60 kg were greater (p<0.05) than those of pigs at 25 kg. In addition, fiber sources affected (p<0.05) the AID of gross energy (GE), organic matter (OM), ether extract (EE), crude protein, SDF and hemicellulose, the hindgut disappearance and ATTD of dietary fiber components, the lactate and propionate concentrations in ileal digesta and the butyrate, valerate and total SCFA concentrations in feces. There were interactions (p<0.05) between BW and fiber sources on the AID of GE, OM, EE, SDF, hemicellulose, the ATTD of EE, TDF, and IDF, and the hindgut disappearance of SDF and hemicellulose. Conclusion: Increasing BW mainly improved the digestibility of dietary fiber fractions, and the dietary fiber sources influenced the digestibility of almost all the dietary nutrients in growing pigs.