• Title/Summary/Keyword: Heating treatment

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A Study On the Structure and Mechanical Properties of Isothermally Annealed after Elevated heating of PET filaments (ET filament의 승온열처리에 의한 구조 및 물성에 관한 연구)

  • Lee, Eun-Woo
    • Journal of the Korean Society of Industry Convergence
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    • v.6 no.4
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    • pp.387-392
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    • 2003
  • The change of crystalline structure and mechanical properties of PET filaments were investigated. Samples were treated by isothermally annealed after elevated heating. Measurements were carried out of density gradient tube for crystallinity and UTM for initial modulus and yield stress. Isothermally heat treatment were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min, in silicon oil bath. And isothermally heat treatment after elevated heating from $20^{\circ}C$ were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min., with heating rate of $5^{\circ}C/min$., $10^{\circ}C/min$. From the results of this study, it found the following facts. It was found that the crystallinity, initial modulus and yield stress of samples were increased with increasing of annealed temperature and time. Also crystallinity, initial modulus and yield stress of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were larger than those of isohtermally annealed samples.

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The Clinical Effects of Heating-Conduction Acupuncture Therapy(tentatively called) for Anterior Talofibular Ligament Injury Induced by Acute Ankle Sprain (전열침(가칭)이 급성 족관절 염좌로 인한 전거비 인대 손상에 미치는 임상적 효과)

  • An, Soon-Sun;Jang, Hyo-Kil;Heo, Dong-Seok
    • Journal of Korean Medicine Rehabilitation
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    • v.19 no.4
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    • pp.127-134
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    • 2009
  • Objectives : The purpose of this study is to investigate the clinical effects of heating-conduction acupuncture therapy on anterior talofibular ligament injury induced by acute ankle sprain. Methods : From October 31, 2008 to July 21, 2009, the 11 outpatients who had admitted to department of oriental rehabilitation medicine, Dae-Jeon oriental medicine hospital, Dae-Jeon university with acute ankle sprain were performed heating-conduction acupuncture therapy on anterior talofibular ligament injury. To evaluate the efficiency of heating-conduction acupuncture therapy, pain threshold with Pressure algometer and visual analogue scale(VAS) were applied before treatment and after 1st, 2nd treatment. Results : 1. The pain threshold score and the VAS score showed statistical significant improvement after 1st treatment. 2. The pain threshold score and the VAS score showed improvement but had no statistical significance after 2nd treatment. 3. The difference between left and right were not statistical significant in pain threshold score and VAS score. Conclusions : Heating-conduction acupuncture therapy has clinical effects of pain reduction on patient with anterior talofibular ligament injury induced by acute ankle sprain.

A Study On Crystalline Structure Change by Isothermally Annealed after Elevated heating of drawn PP filaments (연신한 PP filament의 승온열처리에 의한 결정구조 변화에 관한 연구)

  • Lee, Eun-Woo
    • Journal of the Korean Society of Industry Convergence
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    • v.3 no.4
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    • pp.345-351
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    • 2000
  • The change of crystalline structure of drawn PP filaments were investigated. Samples were treated by isothermally annealed after elevated heating from $20^{\circ}C$. Measurements were carried out with XRD for crystallite size and density gradient tube for crystallinity. Isothermally heat treatment were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. in dry oven. The isothermal heat treatment after elevated heating from $20^{\circ}C$ were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. with heating rate of $1^{\circ}C$/min., $5^{\circ}C$/min. and $10^{\circ}C$/min. From the results of this study, it found the following facts. It was found that the crystallinity and crystallite size of (110) plane of sample were increased with increasing of annealed temperature and time. Also crystallinity and crystallite size of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isohtermally annealed samples.

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Analysis of Microstructures and Mechanical Properties of Billet and Extrudate according to Heat Treatment for the Extrusion of 7075 alloy (7075 합금의 압출에서 원소재 빌렛과 압출재의 열처리에 따른 미세조직 및 기계적 특성 분석)

  • Lee, S.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.33 no.5
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    • pp.232-238
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    • 2020
  • Heating experiments using the 7075 aluminum alloy in the state of billet and extrudate have been performed to investigate the pertinent ranges of working temperatures and holding times for the application to the various automobile parts. The 7075 specimens from raw billet of 152 mm in diameter and 400 mm in length prior to extrusion were used for heating with a holding time of 10 minutes at temperatures between 380℃ and 550℃. Then, an extrusion process using the billet has been fulfilled at 380℃ with extrusion speed of 0.8 mm/min to get an plate-type extrudate of 75 mm in width and 4.2 mm in thickness. The samples from the extrudate were subjected to heating experiments at temperatures between 380℃ and 440℃ with holding times such as 10 min, 30 min, 60 min and 120 min at each heating temperature. The microstructures were investigated on the optical and EBSD micrographs. The hardness measurement and the tensile test have been performed to investigate the effect of the heat treatment on the mechanical property. The results showed for the 7075 extrusion process that the safe heating of billet can be performed below 450℃ and the extrusion can be done safely up to 400℃.

A Study on the Method of Transferring Metal Specimens for Real-time Transmission Electron Microscopy using Ultrasonic Treatment (초음파 처리 활용 실시간 투과전자현미경 관찰용 금속 시편 전사 방법에 관한 연구)

  • H. Kim
    • Transactions of Materials Processing
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    • v.33 no.2
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    • pp.118-122
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    • 2024
  • Micro-electromechanical systems (MEMS) based in-situ heating holders have been developed to enable high resolution imaging of heat treatment analysis. However, unlike the standard 3 mm metal disk specimens used in the furnace-based heating holder and general transmission electron microscopy holder, the MEMS-based in-situ heating holder requires thin specimens that can be penetrated by electrons to be transferred onto the MEMS chip. Previously, focused ion beam milling was used to transfer metal specimens, but it has the disadvantage of being expensive and the risk of specimen damage due to gallium ions. Therefore, in this study, we devised a method of transferring metallic materials by ultrasonic treatment using a transmission electron microscopy specimen made by electro jet polishing. A 3mm electropolished metal disk was placed in an appropriate solution, ultrasonicated, and then drop casted. The transfer of the specimen was successful, but it was confirmed that dislocations were formed inside the specimen due to ultrasonic treatment. This study provides a novel method for transferring metallic materials onto MEMS chips, which is cost-effective and less gallium ion damaging to the specimen. The results of this study can be used to improve the efficiency of heat treatment analysis using MEMS-based in-situ heating holders.

Effect of Pretreatments on Reducing Surface Cracks of Heat-treated Western Hemlock Roundwoods

  • Kim, Chung-Ho;Kang, Chun-Won;Kang, Seog-Goo;Kang, Ho-Yang
    • Journal of the Korean Wood Science and Technology
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    • v.40 no.5
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    • pp.343-351
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    • 2012
  • A large diameter roundwood is an important element of Korean traditional buildings, Hanok, and is hard to be dried without surface cracks. Four different pretreatments, such as pre-cracking, oil heating, kerfing-oil heating and PEG impregnation, were investigated for reducing the surface cracks of large-diameter roundwood specimens during heat treatment. The roundwood specimens of pre-cracking, oil heating and kerfing-oil heating showed surface cracks during pretreatment, but that of PEG impregnation did not. It was confirmed that kerfing reduced the total crack width. Among the four pretreatments and control only the PEG impregnation roundwood specimen had no crack on both outer and inner surfaces after heat treatment. The PEG impregnation specimen shrank only 1.6% in the tangential direction while the pre-cracking did 8.0%.

Heating Values of Agricultural Wastes for Substitute Energy Development (농업부산물의 발열량 조사(지역환경 \circled2))

  • 홍성구
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 2000.10a
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    • pp.563-568
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    • 2000
  • Animal waste is a major agricultural waste or wastewater that requires appropriate treatment to prevent environmental pollution. In this presentation, it is examined if incineration of manure compost is an alternative to treatment of animal waste. Heating values of selected biomass including manure compost were obtained using a bomb calorimeter. Based on heating values of manure and manure compost, ranging from 1200 - 1500 kcal/kg on wet base, incineration could be an alternative for animal waste treatment if available land is limited for land application and sufficient reduction of water content in manure compost.

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The Clinical Effects of Heating-Conduction Acupuncture Therapy for Anterior Talofibular and Calcaneofibular Ligament Injury Induced by Acute Ankle Sprain (전열침(傳熱鍼)이 급성 족관절 염좌로 인한 전거비·종비 인대 손상에 미치는 임상적 효과)

  • An, Soon-Sun;Heo, Dong-Seok
    • Journal of Korean Medicine Rehabilitation
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    • v.20 no.3
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    • pp.119-129
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    • 2010
  • Objectives : The purpose of this study is to investigate the clinical effects of heating-conduction acupuncture therapy on ligament injury induced by acute ankle sprain. Methods : From september 16, 2008 to April 17, 2010, the 28 outpatients who had admitted to department of oriental rehabilitation medicine, Dae-Jeon oriental Medical hospital, Dae-Jeon university with acute ankle sprain were performed heating-conduction acupuncture therapy on anterior talofibular and calcaneofibular ligament injury. To evaluate the efficiency of heating-conduction acupuncture therapy, pain threshold with pressure algometer and visual analogue scale(VAS) were applied before treatment and after 1st, 2nd treatment. Results : 1. The pain threshold and the VAS score showed statistical significant improvement after 1st treatment on calcaneofibular and anterior talofibular ligament injury. 2. The VAS score after 2nd treatment on calcaneofibular and anterior talofibular ligament injury showed statistical significant improvement compared with that after 1st treatment. 3. The pain threshold after 2nd treatment on calcaneofibular and anterior talofibular ligament injury did not show statistical significant improvement compared with that after 1st treatment. 4. The difference between anterior talofibular and calcaneofibular ligament injury was not statistical significant in pain threshold and VAS score. Conclusions : Heating-conduction acupuncture therapy has clinical effects of pain reduction on patient with calcaneofibular ligament injury as well as anterior talofibular ligament induced by acute ankle sprain.

Monitoring on Heating Condition and Enzyme Treatment Condition for Manufacture of Oriental Melon Concentrate (참외 농축액 제조를 위한 가열 및 효소 처리조건 모니터링)

  • 이기동;권승혁;이명희;김숙경;주길재;권중호
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.33 no.5
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    • pp.905-910
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    • 2004
  • This study was carried out to observe the change of oriental melon juice quality during manufacture by heating condition and enzyme treatment. To use over-production oriental melon effectively, oriental melon juice was prepared with change of heating temperature and heating time. The heating conditions for minimum filtration time were 98.57$^{\circ}C$ and 11.29 min. The optimum conditions Predicted for separation ratio of clear solution, filtration time and browning color intensity of oriental melon juice were 98$^{\circ}C$, 13 min. In the pectin-degrading enzyme treatment test, turbidity showed minimum value in 4.40 mg%(pectin-degrading enzyme content), 39.72 mg% (gelatin content) and 24.09 min (treatment time).Browning color intensity showed minimum value in 9.33 mg% (pectin-degrading enzyme content),44.70 mg% (gelatin content) and 115.56 min (treatment time). The optimum conditions predicted for turbidity and browning color intensity of oriental melon concentration Juice were 6.6 mg% (pectin-degrading enzyme content), 33.6 mg% (gelatin content) and 70 min (treatment time).

Change of Heating Value of Cow Manure According to Pre-treatment (전처리 방법 적용에 의한 우분의 열량값 변화)

  • Jeong, Kwang-Hwa;Kim, Jung-Kon;Lee, Dong-Jun;Lee, Dong-Hyun;Cho, Won-Mo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.23 no.4
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    • pp.63-73
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    • 2015
  • This study was carried out to evaluate the change of heating value of cow manure by applying pre-treatment process. Three types of treatment precess; Composting, Dry anaerobic digestion and Physical compression were applied as a pre-treatment method. Composting and anaerobic digestion of cow manure were cause of caloric value reduction of the cow manure. The heating value of cured compost was 5% lower than that of initial composting material. The heating value of dry anaerobic digestion residue was 25.7% lower than that of fresh cow manure. By physical compression of cow manure, heating value and VS/TS ratio (Volatile solids/Total solids ratio) of compressed cow manure were higher than that of fresh cow manure. On the other hand, heating value and VS/TS ratio of leachate generated by compression process were lower than those of fresh cow manure.