• Elastomers and Composites
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• 제19권1호
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• pp.13-31
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• 1984

The purposes of this dissertation are to demonstrate that DSC theromoanaytical methods of vulcanization can provide useful informations on the vulcanization characteristics of industrial formulations and also provides the potential basis for a rapid and complete method of sulfur and vulcanizing accelerator analysis for quality control. The influences of those factors such as heating rate, scan temperature, vucanizing accelerator's type and concentration upon vulcanization exotherm in NR and NBR compounds in the presence of vulcanizing accelerators such as TMTD,MBTS,DPG,TMTM,CBS, and MBT were evaluated by means of DSC. In order to examine the credibility in the DSC method, the same samples which were used for DSC method were studied to compare the DSC results with the ODR (Oscillating Disk Rheometer) data. The results obtained were as follows 1. In the DSC dynamic experiments, the observed enthalpy results from vulcanization depends upon the heating rate; In the range of 2 to $20^{\circ}C/min$ of heating rate, as the heating rate was increased the enthalpy change was also increased. However, over the heating rate of $30^{\circ}C/min$ it was observed that the enthalpy change was decreased as the heating rate was further increased. Without regard to the change of enthalpy, tremendous instantaneous heat evolving was observed in the range of high heating rates. 2. For the samples which are added with various vulcanizing accelerators, the activation energies of vulcanization were as follows; 3. Regarding to the influences of vulcanizining accelerator's types upon the characteristics of vulcanization exotherm, NR and NBR compounds in the presence of thiuramsulphide compounds type accelerators such as TMTD, TMTM, were exhibited sharper and higher vulclanization exotherm than others. From the resuts of DSC thermograms which was distributed in even shape in the broad temperature range, it was clearly shown that the guanidine compounds type accelerator such as DPG acts as a delayed acting accelerator. 4. In the comparison of DSC and ODR results, the dependency of temperature in the cure rate and the observed conversions show good agreements between two results. 5. In the same curatives, by the comparison of glass transition temperatures, it was possible to predict relative values of maximum torques. Consequently, from the present studies, it is shown that the DSC thermoanalytical method can provide an alternate new method for rapid and complete quality control analysis of rubber industry.

• 한국조리학회지
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• 제19권3호
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• pp.209-217
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• 2013

본 연구에서는 소스나 수프 등의 기본재료가 되는 홍합 육수를 제조함에 있어서 홍합의 각종 영양 성분을 적절하게 이용하여 홍합 육수를 만들고자 하였다. 수분함량은 가열시간이 증가함에 따라 유의적(p < 0.05)으로 낮아졌다. 색도측정 결과, L값은 MS1(35.48)이 가장 높았고, a값도 MS1(-2.39)이 가장 높았으며, b값은 MS5(-9.49)가 가장 높았다. pH는 MS5가 6.56으로 가장 낮아 가열시간이 증가 시 시료 간의 유의적(p < 0.001)인 차이를 보이며 낮아졌다. 당도는 MS3이 $4.03^{\circ}Brix$로 가장 높았고, MS1이 $3.37^{\circ}Brix$로 가장 낮았다. 염도는 MS1이 0.71%로 가장 낮았고, 가열시간이 증가 시 시료간의의 유의적인(p < 0.001) 차이를 보이며 염도가 높아졌다. 홍합육수의 특성차이검사 결과, 육수의 외관, 투명도, 비린냄새, 비린맛, 짠맛은 가열시간 증가 시 강하게 평가되었다. 감칠맛은 MS4가 4.33으로 가장 강하게 평가되었다. 홍합육수의 기호도 검사 결과, 맛, 전체적인 기호도 항목에서는 MS3이 가장 좋게 평가되었다. 이상의 결과로 볼 때, 가열시간 증가로 홍합육수의 기호도가 대체적으로 좋게 평가되었으며, 홍합육수 제조 시 가열시간이 15분일 때 기호도가 상승되는 것을 알 수 있었다.

• 마이크로전자및패키징학회지
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• 제30권1호
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• pp.90-94
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• 2023

금속 발열체는 높은 열손실과 화재 위험성 등의 문제점이 있어 우수한 열전도도와 전기전도도 특성을 갖는 탄소섬유가 대체소재로 각광받고 있다. 그러나 탄소섬유는 약 200℃ 이상에서 산화하여 단선되기 때문에 발열체 적용이 제한적이며, 현재 진공관 형태로 탄소섬유 발열체가 일부 사용되고 있다. 본 연구에서는 진공관을 사용하지 않고 대기 중탄소섬유 산화방지를 위해 전기영동증착법으로 탄소섬유 표면에 내열성이 높은 폴리이미드를 코팅하였으며 인가전압에 따른 코팅 두께와 내열성을 확인하였다. 폴리이미드를 코팅한 탄소섬유 발열체를 직렬 연결하여 만든 히터는 최대 292℃ 까지 안정적인 발열 특성을 보였으며 이는 열전달 시뮬레이션의 발열온도 결과와 유사하였다. 전기영동증착방법으로 코팅한 폴리이미드 층은 200℃ 이상에서 탄소섬유의 산화방지에 효과적이며 발열 안정성을 요구하는 2차전지, 우주항공, 전기자동차 등 다양한 발열 부품에 적용 가능할 것으로 기대된다.

• 한국안전학회지
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• 제14권3호
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• pp.84-92
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• 1999

The effects of air velocity and excess air on combustion characteristics were studied in a fluidized bed combustor. The domestic low-grade anthracite coal with heating value of 2010 kcal/kg and the imported bituminous coal from Australia with heating value of 6520 kcal/kg were used as coal samples. The combustion characteristics of mixed fuels in a fluidized bed combustor could be interpreted by pressure fluctuation properties, ash distribution and gas emission. The properties of the pressure fluctuations, such as the standard deviation, cross-correlation function, dominant frequency and the power spectral density function, were obtained from the statistical analysis. From this study, the combustion region increased with increasing air velocity but decreased with excess air due to combustion characteristics of anthracite and bituminous coal.

• 대한전기학회논문지:전기기기및에너지변환시스템부문B
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• 제52권3호
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• pp.133-139
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• 2003

In this paper, a new control scheme of Class-E inverter for Induction Heating (IH) Jar applications with clamped voltage characteristics using Pulse-Frequency-Modulation (PFM) is introduced. To reduce the voltage stress of switch, the proposed PFM control scheme doesn't need any auxiliary circuit in comparison to a family of Active Clamped Class-E (ACCE) inverter. It can decrease voltage stress of switch through modulation of switching frequency. The Class-E inverter using the proposed control scheme has the advantage of not only the same output power when it is compared with a Hybrid-Active Clamped Class-E (Hybrid-ACCE) inverter but also Zero-Voltage-Switching (ZVS), which are characteristics of conventional Class-E and ACCE inverter. The control principles and analysis of proposed method are explained in detail and its validity is verified through simulation and experimental results.

• 대한기계학회논문집B
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• 제20권3호
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• pp.979-987
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• 1996

A theoretical study for the laminar round jet diffusion flame impinging on the wall was carried out to predict the characteristics and structure of impinging jet flame and heat transfer to the wall. Finite chemistry via Arrhenius equation was adopted as the combustion model. All the transport properties were considered as the variable depending on the temperature and composition. For the parametric study, the distance from nozzle to perpendicular wall and Reynolds number at nozzle exit were chosen as the major parameters. As the results of the present study, the characteristics of flow field and the distributions of temperature, density and each chemical species were obtained. The heat transfer rate from flame to the wall and the effective heating area were calculated to investigate the influence of the major parameters on the heat transfer characteristics.

• 한국가구학회지
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• 제23권1호
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• pp.68-74
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• 2012

In this study domestic thinning and small diameter woods of Giant dogwood (Cornus controversa Hemsl) was used. To increase the utilizability of wood, the utilizability was proposed after manufacturing laminated wood by pressing and heating. The physical and mechanical characteristics of Laminated wood were investigated and the color change was measured, using a Chromaticity coordinates, after being pressed at 10% (45 mm), 20% (40 mm), 30% (35 mm) for 5 minutes, using Stopper, and then heated at $180^{\circ}C$ for 6, 12, 24 and 48 hours. The results were as follows. Wood density, compressive strength, MOR, MOE are increased with increasing pressing rate but decreased as heating time is increased after pressing. However, Color change is clear, dimensional stability is improved after pressing and heating.

• 대한전자공학회논문지
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• 제14권1호
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• pp.23-28
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• 1977

본논문은 고주파유도가열전원으로 주목을 끌고있는 SCR inverter의 실용적인 설계에 관한 것이다. 시간적으로 변화하는 부하에 대하여, 주파수제어방식에 의하여 출력과 역률을 일정하게 유지하도록 설계하여, 그특성을 측정검토한바, 만족스러운 결과를 얻었다. 시작시험한 inverter dir 3[KHz], 3[KW]의 것이었다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집D
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• pp.158-163
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• 2001

Performance of the water direct contact air conditioning system, in which heat and mass are transferred directly between air and water droplet, is simulated by semi-empirical method. This system improves transport efficiency compared to conventional indirect contact system and cooling, heating, dehumidification and humidification are attained with one unit. In this study, temperature and flowrate for air and water are measured in the various cooling and heating conditions, and correlations for $h_{c}A/c_{pm}$ are derived from these data. Cooling and heating characteristics of the water direct contact air conditioning system are investigated using correlations.

• 한국가구학회지
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• 제17권2호
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• pp.25-34
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• 2006

This experiment was carried out to investigate the high-frequency gluing characteristics of poly vinyl acetate emulsion adhesive(PVAc) on MDF edge-glued boards. The edge-glued boards were glued lengthwise with butt, scarf, or finger joint. The wastes of MDF boards were reused as board materials. The obtained results are summarized as follows; the bending strength of edge-glued MDF increased slightly with the HF heating time, but the economically desirable heating time was 6 minutes. The bending and tensile strength of edge-glued MDF were high with scarf, finger and butt joint, in order. The strength of finger jointed MDF showed 80% of scarf jointed MDF. The effects of location of finger joints on the bending strength of edge-glued MDF were larger than those of the numbers of finger joints. The bending strength of edge-glued MDF with one joint on the middle position showed 40% decrease in comparison with non-jointed MDF.