• Title/Summary/Keyword: Heat treatment time

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A Study On the Mechanical Properties of Isothermally Annealed after Elevated heating of drawn PP filaments (연신후 승온열처리한 PP filament의 역학적 성질에 관한 연구)

  • Lee, Eun-Woo
    • Journal of the Korean Society of Industry Convergence
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    • v.5 no.4
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    • pp.361-366
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    • 2002
  • The change of mechanical properties of drawn PP filaments which was treated by isothermally annealed after elevated heating. Measurements were carried out with UTM for mechanical properties. Isothermally heat treatment were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min, in silicon oil bath. And isothermally heat treatment after elevated heating from $20^{\circ}C$ were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min., with heating rate of $1^{\circ}C/min$., $5^{\circ}C/min$., $10^{\circ}C/min$. From the results of this study, it found the following facts. Initial modulus and tensile strength were increased with increasing of annealed temperature and time. Also initial modulus of tensile strength of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isothermally annealed samples.

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Surface modification of silica aerogel by surfactant adsorption and heat treatment methods (계면활성제 흡착 및 열처리를 이용한 실리카 에어로겔의 표면 개질)

  • Kim, Nam-Yi;Kim, Seong-Woo
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.3
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    • pp.282-289
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    • 2010
  • In preparation of silica aerogel-based hybrid coating materials, the combination of hydrophobic aerogel with organic polar binder material is shown to be very limited due to dissimilar surface property between two materials. Accordingly, the surface modification of the aerogel would be required to obtain compatibilized hybrid coating sols with homogeneous dispersion. In this study, the surface of silica aerogel particles was modified by using both surfactant adsorption and heat treatment methods. Four types of surfactants with different molecular weights and HLB values were used to examine the effect of chain length and hydrophilicity. The surface property of the modified aerogel was evaluated in terms of visible observation for aerogel dispersion in water, water contact angle measurement, and FT-IR analysis. In surface modification using surfactants, the effects of surfactant type and content, and mixing time as process parameter on the degree of hydrophilicity for the modified aerogel. In addition, the temperature condition in modification process via heat treatment was revealed to be significant factor to prepare aerogel with highly hydrophilic property.

Optimal Post Heat-treatment Conditions for Improving Bonding Strength of Roll-bonded 3-ply Ti/Al/Ti Sheets (롤 본딩된 Ti/Al/Ti 3-ply 다층금속 판재의 접합강도 향상을 위한 최적 후열처리 조건 도출)

  • Kim, M.H.;Bong, H.J.;Kim, J.H.;Lee, K.S.
    • Transactions of Materials Processing
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    • v.31 no.4
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    • pp.179-185
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    • 2022
  • The influence of post-roll bonding heat treatment conditions such as temperature and time on the variation in the diffusion layer, generated at the bonding interface and the subsequent mechanical properties of the roll-bonded Ti grade 1/Al1050/Ti grade 1 sheets, was systematically investigated. The intermetallic compound (IMC) phase generated by post heat treatment conditions adopted in this study was obviously indexed as monolithic TiAl3. Whereas the thickness of IMC layer generated by annealing at 500 ℃ was approximately 100 nm scale, it drastically increased above 1.5 ㎛ when annealed at 600 ℃. Uniaxial tensile and peel tests were then performed to compare mechanical properties. As a result, the bonding strength drastically increased above 7.9 N/mm by annealing at 600 ℃, which implies that proper annealing condition was a prerequisite, to improving interface bonding strength as well as global elongation properties for Ti/Al/Ti 3-ply sheet.

Mechanical and thermal properties of 3D printing metallic materials at cryogenic temperatures

  • Jangdon Kim;Jaehwan Lee;Seokho Kim
    • Progress in Superconductivity and Cryogenics
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    • v.26 no.2
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    • pp.24-30
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    • 2024
  • Metal 3D printing is utilized in various industrial fields due to its advantages, such as fewer restrictions on production shape and reduced production time and cost. Existing research on 3D printing metal materials focused on changes in material properties depending on manufacturing conditions and was mainly conducted in a room temperature environment. In order to apply metal 3D printing products to cryogenic applications, research on the properties of materials in cryogenic environments is necessary but still insufficient. In this study, we evaluate the properties of stainless steel (STS) 316L and CuCr1Zr manufactured by Laser Powder Bed Fusion (LPBF) in a cryogenic environment. CuCr1Zr is a precipitation hardening alloy, and changes in material properties were compared by applying various heat treatment conditions. The mechanical properties of materials manufactured using the LBPF method are evaluated through tensile tests at room temperature and cryogenic temperature (77 K), and the thermal properties are evaluated by deriving the thermal conductivity of CuCr1Zr according to various heat treatment conditions. In a cryogenic environment, the mechanical strength of STS 316L and CuCr1Zr increased by about 150% compared to room temperature, and the thermal conductivity of CuCr1Zr after heat treatment increased by about 6 to 10 times compared to before heat treatment at 40 K.

Study on Carbon Pick-up in molten iron (I);Effect of Crystallization heat treatment of Carbon-bearing materials on Carbon Pick-up in molten iron (용철(熔鐵)에서의 가탄(加炭)에 관(關)한 연구(硏究)(1);가탄(加炭)에 미치는 탄소재(炭素材)의 결정화열처리(結晶化熱處理)의 영향)

  • Cho, Won-Il;Lee, Jong-Nam
    • Journal of Korea Foundry Society
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    • v.3 no.3
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    • pp.159-166
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    • 1983
  • In order to develope domestic carburizers, the experiment was carried out by applying crystallization heat treatment to domestic anthracites and also to foreign products to compare with domestic anthracites.The present work was mainly concerned with the effect of their degree of crystallization of carbon-bearing materials on carbon pick-up in molten iron.Those effects were evaluated by the measurement of density, chemical composition, specific electric resistivity, and X-ray intensity of carbon-bearing materials. Experimental results thus obtained were summurized as follows. 1. The degree of crystallization of domestic anthracites and foreign products was increased with increasing heat treatment temperature. 2. The more degree of crystallization, the shorter the dissolving time of domestic anthracites in molten iron was obtained, while that of foreign products was remained constant. 3. As the degree of crystallization of domestic anthracites and foreign products was increased, the carbon content as well as carbon recovery in molten iron was increased.

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Effects of Mo on the Mechanical Properties of Ductile Cast Iron with Cu Austempered at 380℃ (Cu가 함유된 구상흑연주철의 380℃에서 오스템퍼링 시 Mo이 기계적 특성에 미치는 영향)

  • Kim, G.Y.
    • Journal of the Korean Society for Heat Treatment
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    • v.26 no.5
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    • pp.219-224
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    • 2013
  • In this study, we investigated effect of Mo addition on mechanical properties of Cu added ADI. Ductile cast iron specimens were austenitized at $900^{\circ}C$ for 150 min and then austempered at $380^{\circ}C$ for the various time periods from 15 min to 480 min. Mo added ADI had a higher volume fraction of retained austenite, and the volume fraction of retained austenite was determined by XRD analysis. As decreasing volume fraction of retained austenite, the elongation was also decreased as expected. But the UTS and yield strength were not decreased.

Prediction of Fracture Appearance Transition Temperature(FATT) to Steel by Ultrasonic and Barkhausen Noise Method (초음파와 Barkhausen Noise에 의한 강의 연.취성천이온도 예측)

  • Nam, Young-Hyun;Seong, Un-Hak
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.23 no.7 s.166
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    • pp.1215-1222
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    • 1999
  • It is advantageous to use an NDE method to assess the mechanical properties of materials since the conventional method is time-consuming and sometimes requires cutting of sample from the material/component. This paper shows that the ultrasonic and the Barkhausen noise(BHN) methods can be used to accurately characterize forged reactor vessels. The attenuation coefficient of the ultrasonic wave was changed with heat treatment temperature and condition[as-quenched, tempered, PWHT]. The RMS[root mean square] voltage of Barkhausen noise depended on heat treatment temperature and conditions. The fracture appearance transition temperature(FATT) can be predicted using nondestructive evaluation methods.

Analysis of Heat Treatment Process Conditions for Output Characteristics of Permalloy Core on Current Sensors using DOE (실험계획법을 이용한 퍼멀로이 전류 코어 센서의 출력특성에 관한 열처리 공정조건 분석)

  • Kim, Young Shin;Kim, Yoon Sang;Jeon, Euy Sik
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.4
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    • pp.16-23
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    • 2020
  • An electric vehicle operates at high currents and requires real-time monitoring of the entire system for ensuring efficiency and safety of the vehicle. Current sensors are applied to drive the motors, inverters, and battery control systems, and are the key components to ensure constant monitoring of the magnitude and waveforms of the operating current. In this study, a heat treatment process condition to influence the performance of Permalloy current sensors was developed; the correlation between the output capacity, low-temperature characteristics, and high-temperature characteristics of the current sensor was studied; and the process was optimized to meet the required output accuracy and temperature characteristics.

Studies on the Manufacturing of Ginseng Soft Drink II. Effect of pH and heat treatment on the stability of panaxadiol saponins (인삼청량음료 제조에 관한 연구 (제2보) pH 및 처리조건이 Panaxadiol Saponin의 안정성에 미치는 영향)

  • 양재원;도재호
    • Journal of Ginseng Research
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    • v.6 no.1
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    • pp.25-29
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    • 1982
  • This investigation was carried out to study the influence of pH and heat treatment on the ginsenosides in the white ginseng extract. Changes in ginsenosides (Rb1, Rb2, ,Rc, Rd) and free sugar were measured by the peak area variation of HPLC chromatogram during 25 hours heat treatment at the various level of pH. It was found that :(1) The peak areas of Rb1. Rb2, Rc and Rd on the HPLC chromatogram were decreased remarkably below pH 4.0 and more decrease was found as the temperature and heating time increased. (2) Those of glucose and arabinose were increased remarkably. It is considrered that the increase of glucose and the formation of arabinose result from the hydrolysis of ginsenoside( Rb1, Rb2, Rc, Rd) linked with sugars.

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The influence of post weld heat treatment on mechanical properties of stainless steel weldment (스테인리스강 용접부의 기계적 성질에 미치는 후열처리의 영향)

  • 한종만;한기형;이은배;허만주;한용섭
    • Journal of Welding and Joining
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    • v.14 no.3
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    • pp.75-85
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    • 1996
  • In this paper the influence of postweld heat treatment on mechanical properties of SMAW and FCAW stainless steel weldments was examined and the obtained results are as follows ; (1) The amount of $\delta$-ferrite formed by SMAW and FCAW process decreased with increasing holding temperature and time in post weld heat treatment(PWHT), and it was found that the reduced ferrite was transformed into sigma phase after $800^{circ}C{\times}50hr$ PWHT. This sigma phase, even though it was very small, resulted in brittleness of dissimilar weldment between carbon steel and stainless steel in bending test, however in similar weldment between stainless steel and stainless steel was not occured. (2) The chemical composition of sigma phase was measured to 28-30%Cr, 7-9%Mo, 4-6Ni in 316L weldment, and also 35-37%Cr, 0.9-1.0Mo, 6-8%Ni in 309L weldment by EDS analysis.

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