• 한국기계가공학회지
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• 제21권1호
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• pp.56-65
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• 2022

The electrochemical corrosion properties of austenitic AISI 304 steel subjected to a long-term-aging heat treatment were investigated. AISI 304 steel was aged at 700 ℃ for up to 10,000 h. The variation in the microstructure of the aged specimens was observed by optical microscopy and scanning electron microscopy. Electrochemical polarization experiments were performed to obtain the corrosion current density (Icorr) and corrosion potential (Ecorr). Analyses indicated that the metastable intermetallic carbide M₂₃C₆ formed near the γ/γ grain boundary and coarsened with increasing aging time; meanwhile, the δ-ferrite decomposed into the σ phase and into M₂₃C₆ carbide. As the aging time increased, the current density increased, but the corrosion potential of the austenitic specimen remained high (at least 0.04 ㎛/cm²). Because intergranular carbide was absent, the austenitic annealed specimen exhibited the highest pitting resistance. Consequently, the corrosion resistance of austenitic AISI 304 steel decreased as the aging heat treatment time increased.

• Journal of the Korean Wood Science and Technology
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• 제44권3호
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• pp.370-380
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• 2016

제주도 지역에서 소나무재선충병 피해를 받은 곰솔 원목의 이용확대를 위하여 열처리를 수행하였다. 열처리는 처리 원목의 중심부가 소나무재선충의 사멸온도인 $56^{\circ}C$를 30분간 유지하여야 한다. 곰솔 원목의 초기함수율과 말구지름은 각각 46% ~ 141%, 180 mm ~ 500 mm의 범위이고, 기본비중과 전건비중은 각각 0.47, 0.52이었다. $105^{\circ}C$ 조건에서 함수율과 말구지름에 따라 열처리에 소요되는 시간은 7.7 h ~ 44.2 h의 범위로 측정되었다. 다양한 함수율 및 지름을 갖는 곰솔 원목의 열처리 소요시간을 예측하기 위하여 열처리 진행 중 처리목 내부의 온도분포를 유한차분법을 적용한 2차원 열전달 해석을 통하여 제시하였다. 열전달 해석을 위한 목재의 열적 특성은 함수율에 따른 열전도계수와 비열을 적용하였으며, 자연대류와 강제대류를 합한 형태의 혼합대류에 의한 혼합대류계수를 적용하였다. 실험값과 예측 값의 오차는 3 ~ 45%의 범위로 분석되었다. 곰솔 원목에서 초기함수율이 50%이고, 말구지름이 200 mm, 300 mm, 400 mm인 경우, 예측된 열처리 소요시간은 각각 10.9 h, 18.3 h, 27.0 h이었다. 초기함수율이 75%일 때, 지름에 따라 각각 13.6 h, 22.5 h, 32.8 h이고, 초기함수율이 100%일 때, 지름에 따라 각각 16.2 h, 26.5 h, 38.2 h이었다. 이러한 열처리 소요시간의 예측방법에 소나무와 잣나무 등 다른 소나무재선충병 피해목의 물리적 특성을 적용하면, 함수율과 말구지름에 따른 열처리 소요시간을 제시할 수 있을 것으로 판단된다.

• 한국주조공학회지
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• 제24권5호
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• pp.290-294
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• 2004

The effect of carbon equivalent on the fading behavior of hypoeutectic ductile cast iron was investigated. The carbon content was slightly increased right after graphite spheroidization treatment and remained almost constant with holding at $1,490^{\circ}C$ after 4 minute. The residual magnesium content was decreased slowly with holding. The empirical equation expressing the relationship between this and holding time was proposed ; $C=C_o-P{\times}t$. The proportionality constant, P, was inversely proportional to carbon content.

• 열처리공학회지
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• 제10권1호
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• pp.63-70
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• 1997

A study was performed to examine the aging behaviors of Al-2.1Li-2.9Cu alloy by differential scanning calorimetry and transmission electron microscopy. DSC measurements were conducted over the temperature range of $25{\sim}550^{\circ}C$ at a heating rate of $5^{\circ}C$/min. for the specimens aged at 130, 160, $190^{\circ}C$ and $220^{\circ}C$ for various times after solution treatment at $540^{\circ}C$ for 30 minutes. The peaks due to the formation of G.P.zone were not detected in the specimens aged at 130 and $160^{\circ}C$, but those at 190 and $220^{\circ}C$ appeared in DSC curves. The heat absorption due to the dissolution of ${\delta}^{\prime}$ phase was increased with increasing aging time at $130^{\circ}C$ aging. In contrast, those values for the specimens aged at 160 and $190^{\circ}C$ were initially increased and inversely decreased at the transition time of 72 and 1 hour, respectively. The heat evolution due to the formation of $T_1$ phase was nearly unchanged at $130^{\circ}C$ aging, but at $160^{\circ}C$ and $190^{\circ}C$ aging, drastically decreased after the transition time. It can be considered that the increase of $T_1$ phase results in the decrease of ${\delta}^{\prime}$ phase when aging time is longer than the transition time. The hardness of the specimen aged at $190^{\circ}C$ is initially higher compared with that at $160^{\circ}C$, however, the peak hardness shows the lower value than that at $160^{\circ}C$.

• Journal of Advanced Marine Engineering and Technology
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• 제8권2호
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• pp.81-87
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• 1984

The effect of heat treatment and mechanical stress on the dielectic strength of epoxy resin film is studied. The film with 30-210 .mu.m thickness are casted at room temperature for 8 hours and post cured at the range of temperature 60-180 .deg. C, and the heat setting time are two kind, ie, 2 and 10 hours. The samples are made with Stycast 1266 that the primary compound is diglycidyl ether of bisphenol A, and the hardner is denaturated polyamines. Under no mechanical stresses, the maximum dielectric strength of the sample is obtained for the sample heat treated for 2 hours at 150 .deg. C. However, the best dielectric strength characteristics under compressive stress is obtained for the sample heat treated at 90 .deg. C and 120 .deg. C. The dielectric strength of the sample are also affected significantly by the cooling velocity of the sample after post heat setting at given temperature.

• Journal of the Korean Wood Science and Technology
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• 제47권5호
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• pp.567-578
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• 2019

A common problem with fast-growing hardwoods is dimensional instability that limits use of their wood. In this study, we investigated the effects of pre-drying methods, temperatures, and heating duration on the specific gravity, water absorption, and dimensional stability of three tropical fast-growing hardwoods, jabon (Neolamarckia cadamba Roxb.), sengon (Falcataria moluccana Miq.), and mangium (Acacia mangium Willd.). Wood samples were pre-dried by two methods (fan and oven at $40^{\circ}C$), and heat treatments were performed at three temperatures (120, 150, and $180^{\circ}C$) for two different time periods (2 and 6 hours). The specific gravity, water absorption, dimensional stability, and structural changes of the samples were evaluated. The results revealed that heat treatments slightly reduced the specific gravity of all three wood species. In addition, the heat treatments reduced water absorption and significantly improved dimensional stability of the samples. Oven pre-drying followed by heat treatment at $180^{\circ}C$ for 6 hours resulted in good physical improvement of jabon and sengon wood. Fan pre-drying followed by heat treatment at $180^{\circ}C$ for 2 hours improved the physical properties of mangium wood. The heat treatment shows a promising technique for improving the physical characteristic of fast growing hardwoods.

• 보존과학회지
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• 제28권1호
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• pp.29-37
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• 2012

이 연구는 매장상태에서 출토되는 금동유물의 표면색이 고유한 금색 이외에 붉은 계열의 색들과 교반되어 나타나는 원인을 규명하고자 수은아말감도금법을 재현해 보고 완성품에 대하여 열처리 조건을 변화시켜 도금층의 표면색과 표면 및 단면의 상태변화를 알아보고자 하였다. 그 결과 높은 열처리 실험조건 일수록 도금층에 검은 산화물층이 넓게 생성되었으며, 산화물층을 제거한 부분에서는 붉은색의 도금 표면색이 표출되었다. 또한 표면이 노란색과 붉은색으로 교반된 시료의 미세 표면관찰에서는 색상에 따라 표면상태의 변화양상이 다르게 나타났으며 단면에서는 도금층 공극의 밀도와 크기가 점차 커지는 것으로 밝혀졌다. 열처리 실험 후 표면성분분석 결과 온도가 올라갈수록 Hg와 Au의 비율은 감소하였으나 Cu의 성분비는 증가하였다. 또한 단면분석 결과에서도 실험조건에 따른 층위별 Au와 Cu의 성분변화가 반비례하는 경향을 보였다. 이러한 실험결과들을 볼 때 아말감을 이용한 금동유물은 생산과정이나 생산 이후에 열이 도금층의 표면색에 영향을 미치는 것을 의미하며 도금층 상태에도 관계된다는 것을 확인할 수 있었다.

• 열처리공학회지
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• 제4권1호
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• pp.30-36
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• 1991

Effects of aging treatment on the mechanical properties of a 18 Ni maraging steel were investigated by considering the reverted austenite. Specimens were heat treated by austenitizing at $840^{\circ}C$ for 1 hr and then aged for various times at $480^{\circ}C$ and $520^{\circ}C$. The main results obtained are as follows : 1) The amounts of reverted austenite are increased up to about 4% at $480^{\circ}C$ and about 22% at $520^{\circ}C$ with 1 to 48 hrs aging time. 2) Decreasing tendencies of impact energy and fracture toughness with increasing aging time are diminished after aging for 2 hrs at two aging temperatures of $480^{\circ}C$ and $520^{\circ}C$. 3) Peak hardness and yield strength are obtained after aging for 4 hrs at $480^{\circ}C$ and 2 hrs at $520^{\circ}C$ respectively. From the above results, it was concluded that the optimum aging condition with which showed good strength and toughness combination are given to be $480^{\circ}C$ for 4 hrs and $520^{\circ}C$ for 2 hrs.

• 한국식생활문화학회지
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• 제36권5호
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• pp.484-491
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• 2021

This study investigated the effect of dry heat treatment (DHT) on the physicochemical properties of hard type (HR) and floury type (FR) rice to improve the processing aptitude of rice flour. The rice flour was heated at 130℃ for 0, 2 and 4 hours, and the color value, water absorption index (WAI), water soluble index (WSI), swelling power, solubility, pasting properties, particle shape and the X-ray diffraction were measured. After DHT, the L value of rice flour decreased, and the b value increased. The WAI, WSI, swelling power and solubility of HR and FR increased with the increase of treatment time. The cold viscosity and setback increased, while breakdown decreased. Cracks and lumps formed with fine particles were observed. The X-ray diffraction pattern was A-type, while the diffraction intensity decreased. According to the results of the two-way analysis of variance (ANOVA) test, the hydration and pasting properties were significantly different between HR and FR and were affected by DHT time. The results suggest that the properties of modified rice flour by DHT can be used in the food industry.

• 열처리공학회지
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• 제14권4호
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• pp.212-219
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• 2001

The fatigue test was carried out to evaluate the fatigue characteristics of fire resistance steel for frame structure and heat affected zone (HAZ) by the one side Gas Metal Arc Welding (GMAW). In this paper, the fatigue crack growth behavior was investigated with the compact tension specimen of base metal and the HAZ according to chemical composition and rolling end temperature, respectively. And the acoustic emission signals obtained from the fatigue test were analyzed by the time-frequency analysis method as a nondestructive evaluation. Main results obtained are summarized as follows; The hardness was appeared softening phenomenon that weld metal and HAZ are lower than that of base metal. Fatigue life of welded specimen was longer than that of base metal. m was 3~4.5 in base metal and 3.8~5.8 in HAZ. The main frequency range of acoustic emission signal analyzed from time-frequency method is different with the range by noise and crack. Also, it could be classified that it was also generated by fracture mechanics of dimple, inclusion etc.