• Title/Summary/Keyword: Heat treatment conditions

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Sliding Wear Characteristics of plasma Sprayed $8\%Y_{2}O_3-ZrO_2$ Coating for Post-spray Heat Treatment

  • Chae Young-Hun;Kim Seock-Sam
    • KSTLE International Journal
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    • v.6 no.2
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    • pp.45-50
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    • 2005
  • Plasma ceramic spray that is applied on a machine part under severe work conditions has been investigated for tribological behavior. The application of ceramic coatings by plasma spray has become essential in tribosystems to produce wear resistance and long life in severe conditions. The purpose of this study was to investigate the wear characteristics of $8\%Y_{2}O_3-ZrO_2$ coating, in view of the effect of post-spay heat treatment. The plasma-sprayed $8\%Y_{2}O_3-ZrO_2$ coating was studied to know the relationship between phase transformations and wear behavior related to post-spray heat treatment. Wear test was carried out with ball on disk type on normal loads of 50N,70N and 90N under room temperature. The phase transformation of phase and the value of residual stress were measured by X-ray diffraction method(XRD). Tribological characteristics and wear mechanisms of coatings were observed by SEM. The tribological wear performance was discussed in the focusing of residual stress. Consequently, post-spray heat treatment plays an important role in decreasing residual stress. Residual stress in the coating system has a significant influence on the wear mechanism of coating.

Physicochemical and antioxidant properties of garlic (A. sativum) prepared by different heat treatment conditions

  • Kim, Il-Doo;Park, Yong-Sung;Park, Jae-Jeong;Dhungana, Sanjeev Kumar;Shin, Dong-Hyun
    • Korean Journal of Food Science and Technology
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    • v.51 no.5
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    • pp.452-458
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    • 2019
  • The objective of this study was to investigate the physicochemical characteristics and antioxidant potential of garlic processed using different heat treatments conditions, which is an effective method for removing the unpleasant odor and taste of raw garlic. The pH and soluble solid content of raw garlic (pH 6.07, $7.7^{\circ}Bx$) were almost equal or slightly higher than that of processed garlic samples (pH 5.06-6.09, $7.1-7.4^{\circ}Bx$). The color of processed garlic was also significantly affected. The amounts of amino acids such as ${\gamma}$-amino-n-butyric acid and few essential amino acids also increased after the thermal treatment of garlic. The antioxidant potentials of red and black garlic were higher than that of raw garlic. The polyphenol content of processed garlic ($38.51-81.51{\mu}g$ gallic acid equivalent/g sample) was significantly higher than that of raw garlic ($30.66{\mu}g$ gallic acid equivalent/g sample). These results indicated that heat treatment for different durations under a controlled environment enhanced the nutritional and functional properties of garlic.

Effect of Cooling Rate and Temperature on Intercritical Annealing of Medium-Carbon Cr-Mo Alloy for High Strength Cold Heading Quality Wire Rod (고강도 냉간압조용 중탄소 Cr-Mo 합금강의 임계간 어닐링시 냉각속도 및 온도의 영향)

  • JongHyeok Lee;ByoungLok Jang
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.4
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    • pp.230-236
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    • 2023
  • The current study deals with the effect of cooling rate and temperature for annealing on medium-carbon Cr-Mo alloy steel, especially for cold heading quality wire rod, to derive the optimum micro-structures for plastic deformation. This is to optimize the spheroidization heat treatment conditions for softening the material. Heat treatment was performed under seven different conditions at a temperature between Ac1 and Ac3, mostly within 720℃ to 760℃, and the main variables at this time were temperature, retention time and cooling rate. Microstructure and phase changes were observed for each test condition, and it was confirmed that they were greatly affected by the cooling rate. It was also confirmed that the cooling rate was changed in the range of 0.1℃/min to 5℃/min and affected by phase deformation and spheroidization fraction. The larger the spheroidization fraction, the lower the hardness, which is associated with the increasing connection of ferrite phases.

Effect of Heat Treatment Conditions on the Microstructure and Mechanical Properties of Asymmetrically Cold Rolled OFC Sheet (비대칭 냉간압연된 무산소동 판재의 열처리 조건이 미세조직과 기계적 성질에 미치는 영향)

  • Kim, S.T.;Kwon, S.C.;Kim, D.V.;Lee, J.K.;Seo, S.J.;Yoon, T.S.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.29 no.1
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    • pp.5-10
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    • 2020
  • Heat treatment conditions of 88.5% asymmetrically cold rolled oxygen free copper (OFC) sheets have been studied to obtain an equiaxed fine microstructure with a grain size of less than 10 ㎛. The commercial OFC sheets with the thickness of 10 mm were asymmetrically cold rolled by using equal speed asymmetric rolling (ESAR) processes and total rolling reduction. The thickness of the rolled sheets were 88.5% and 1.15 mm, respectively. An equiaxed fine microstructure of OFC sheets with a grain size of 6.0 ㎛ were obtained when the asymmetrically cold rolled OFC sheets were heat treated at 180℃ for 40 minutes. The tensile strength of the asymmetrically cold rolled specimen increased from 217.6 MPa to 396.1 MPa, while the elongation of the specimen asymmetrically cold rolled and heat treated increased from 29.0% to 66.9% along with an 8% increase of the tensile strength.

Crystalline Phases and Superconductor Characteristics of the Plasma Sprayed YBa2Cu$\chi$O7-y High Tc Superconductor Thick Film (플라즈마 용사법에 의해 제조된 YBa2Cu$\chi$O7-y(X=3, 3.5, 4) 고온초전도체 후막층의 결정상 및 초전도 특성)

  • 한명섭;서동수
    • Journal of the Korean Ceramic Society
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    • v.29 no.2
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    • pp.152-160
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    • 1992
  • High-Tc superconductor thick films of YBa2Cu$\chi$O7-y (X=3, 3.5, 4) of which thickness varies from 100 $\mu\textrm{m}$ to 200 $\mu\textrm{m}$ were successfully prepared by plasma spraying method, and the characteristics of thick film depending on copper content and heat treatment conditions were investigated. Regardless of heat-treated temperature, the specimens with X=3 were composed of YBa2Cu$\chi$O7-y, Y2BaCuO5 and BaCuO3 phases. The specimens with X=4, however, were composed of YBa2Cu$\chi$O7-y phase at all heat treatment conditions. The specimens with X=4 composition showed the best superconducting characteristics after heat treatment at 925$^{\circ}C$, and the superconducting transition temperature with zero resistivity (Tc,zero) was 87K. The thick film lost superconductivity when the specimens were heat-treated at 950$^{\circ}C$ because of interdiffusion between superconductor elements and bond coating elements and Y2BaCuO5 phase was found was found to be main phase at the interface.

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Construction of Abalone Sensory Texture Evaluation System Based on BP Neural Network

  • Li, Xiaochen;Zhao, Yuyang;Li, Renjie;Zhang, Ning;Tao, Xueheng;Lee, Eung-Joo
    • Journal of Korea Multimedia Society
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    • v.22 no.7
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    • pp.790-803
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    • 2019
  • The effects of different heat treatments on the sensory characteristics of abalones are studied in this study. In this paper, the sensory evaluation of abalone samples under different heat treatment conditions is carried out, and the evaluation results are analyzed. The three-dimensional (3D) scanning and reverse engineering are used in tooth modeling of the sensory evaluation of abalone samples under different heat treatment conditions. Besides, the chewing movement models are simplified into three modes, including the cutting mode, compressing mode and grinding mode, which are simulated using finite element simulation. The elastic modulus of the abalone samples is obtained through the compression testing using a texture analyzer to distinguish their material properties under different heat treatments and to obtain simulated mechanical parameters. Finally, taking the mechanical parameters of the finite element simulation of abalone chewing as input and sensory evaluation parameters as the output, BP neural network is established in which the sensory texture evaluation model of abalone samples is obtained. Through verification, the neural network prediction model can meet the requirements of food texture evaluation, with an average error of 9.12%.

Characteristics of Tantalum Powder by Conditions of After Treatment (후처리 조건에 따른 탄탈륨 분말의 특성)

  • 윤재식;박형호;배인성;김병일
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.344-347
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    • 2003
  • Pure tantalum powder has been produced by combining Na as a reducing agent, $K_2$TaF$_{7}$ as feed material, KCl and KF as a diluent in a stainless steel (SUS) bomb, using the method of metallothermic reduction. And we examined various types of after-treatment that affect the high purification of powder. A significant amount of impurities contained in recovered powder was removed in various conditions of acid washing. In particular, 20% (HCl + HNO$_3$) was effective in removing heavy metal impurities such as Fe, Cr and Ni, 8% H$_2$SO$_4$ + 8% $Al_2$(SO$_4$)$_3$ in removing fluorides such as K and F from non-reactive feed material, and 2% $H_2O$$_2$ + 1 % HF in removing oxides that formed during reaction. Significant amounts of oxygen and part of light metal impurities could be removed through deoxidation and heat treatment process. On the other hand, because it is difficult to remove completely heavy metal impurities such as Fe, Cr, and Ni through acid washing or heat treatment process if their contents are too high, it is considered desirable to inhibit these impurities from being mixed during the reduction process as much as possible.

Determination of Heat Treatment Condition for Hot Press Formed Automotive Flex Plate (자동차용 플렉스 플레이트 제조를 위한 핫프레스 포밍 열처리 조건 최적화)

  • Park, I.H.;Lee, M.G.;Kim, S.J.;Jeong, W.C.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.186-189
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    • 2008
  • The flex plate, an automotive part which mounts to the automotive engine to transfer torque to transmission, should have considerable hardness and shape accuracy. As a way to produce the flex plate, the hot press forming technology which takes advantages of high formability at elevated temperature, enhanced strength and shape stability was introduced. Therefore, as one of major process parameters the heat treatment condition should be determined to obtain appropriate hardness in the range of manufacturer's specifications. In this study, two heat treatments, austempering and quenching and tempering (QT), were compared as feasible conditions fur the hot press forming of high-carbon tool steel and the hardness and toughness after heat treatments were evaluated. The study showed that both heat treatments resulted in improved hardness but only quenching and tempering showed practicable range of toughness.

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Computer Simulation of Quench-Hardening of Alloy Steel for Structural Purposes by the Modified Finite Difference Method (개량차분법에 의한 임의의 형상의 열처리제품의 급냉경화 해석)

  • Kim, K.S.;Song, Y.B.;Hong, C.P.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.11-16
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    • 1989
  • Understanding and control of thermal history of heat-treated components are very important in heat treating process. A computer program was developed for prediction of thermal history in quenching process with various cooling media and agitation conditions. Computer simulation of heat flow in quenching treatment of spur gear of SCM 22 H was carried out by two and three dimensional finite difference method. Distributions of microstructure and hardness in heat-treated spur gear were predicted by computer simulation, and the results showed a good agreement with the experiments. It was concluded that the

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Effects of Heat-Treatment Conditions on the Properties of Cu-Be-Co Alloy (Cu-Be-Co합금의 물성에 미치는 열처리 조건의 영향)

  • Jung, Woon-Jae;Kyoung, Shin-Ho;Kim, Ki-Tae;Kim, Jong-In
    • Journal of Korea Foundry Society
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    • v.14 no.3
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    • pp.233-239
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    • 1994
  • The effects of solid solution treatment and aging in the properties of Cu-0.32wt%Be-1.35wt%Co alloy was gravity die casted and forged were investigated in order to examine the optimum heat treatment conditions for production of high conductivity mold material. The optimum properties for mold material were obtained under the conditions which were solid solution treated at $930^{\circ}C$ for 1 hour and aged at $430^{\circ}C$ for 2hours.

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