• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2004년도 춘계학술대회 논문집
• /
• pp.127-130
• /
• 2004

In the recent years, lightweight components fabricated with aluminum alloys have been applied into building the automobiles. Among the several competing fabrication methods, hot forging is taken as the most reliable technique to produce suspension parts such as control arms. Generally, Al forging products have been used widely for the aircraft building with the extruded stock as a starting material. For the economical base, however, the cast stocks turn to be as the forging stocks recently after a continuously casting technique was developed to produce quite a uniform microstructure enough to use for the forging process. Even more, there is a tendency to omit the homogenization step before forging, which is considered to be an indispensable process for all kinds of Al alloy, In the present study, a series of compression test was carried out to find out how the cast structure and the following heat treatments influence the deformation behavior, that is, forging characteristic.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2006년도 춘계학술대회 논문집
• /
• pp.285-287
• /
• 2006

Ultra-fine grained and high hardened Al sheet was obtained by Equal channel angular pressing (ECAP). During this process the microstructure, the hardness and the texture of AA 1050 Al alloy sheet are changed by a severe shear deformation. The plastic strain ratio after the ECAP and subsequent heat-treatment condition has been investigated in this study. It was found that the average r-value of the ECAPed and subsequent heat-treated specimen was 1.7 times higher than those of the initial Al sheet. This could be attributed to the various texture formations through the ECAP and subsequent heat-treatment of AA 1050 Aluminum alloy sheet.

• 열처리공학회지
• /
• 제11권3호
• /
• pp.207-215
• /
• 1998

13%Cr martensitic stainless steel was microalloyed with 0~1.5%Mo, and the mechanical properties were tested at the various heat treated conditions. Mo addition increased austenitization temperature(Ac1), and had little influence on the hardness and tensile properties at the annealed condition. The higher the austenitizing temperature, the higher the hardness and tensile strength, but Mo addition decreased those properties. The impact energy after austenitization increased with addition of Mo. The decrease of mechanical properties and increase of impact energy of Mo-alloyed steel after austenitization are thought to be caused by formation of ductile ${\delta}$-ferrite phase in the microstructure.

• 한국소성가공학회:학술대회논문집
• /
• 한국소성가공학회 2006년도 제5회 박판성형 SYMPOSIUM
• /
• pp.88-91
• /
• 2006

Ultra-fine grained and high hardened Al sheet was obtained by Equal Channel Angular Pressing (ECAP). During this process the microstructure, the hardness and the texture of AA 1050 Al alloy sheet are changed by a severe shear deformation. The plastic strain ratio after the ECAP and subsequent heat-treatment condition was investigated in this study. It was found that the average r-value of the equal channel angular pressed and subsequent heat-treated specimen was 1.7 times higher than that of the initial Al sheet. This could be attributed to the various texture formations through the ECAP and subsequent heat-treatment of AA 1050 Aluminum alloy sheets.

• 열처리공학회지
• /
• 제5권4호
• /
• pp.195-200
• /
• 1992

SCM 415 has been vacuum carburized in the carburizing pressure of 60-65kpa and the carburizing temperature of 1233k and 1273k after varied to 0-20 in the ratio of $N_2/C_3H_8$ and then diffusion treated for various times at 1123k. The results obtained from the experiment are as follows. 1. With increasing from 0 to 20 in ratio of $N_2/C_3H_8$ the sooting formation of surface after carburizing considerably decreased. 2. The hardness control and surface carbon content of carburizing surface has been modified by the addition of nitrogen to the propan. 3. The appoximate value of k is indirectry calculated at 1123k which results are obtained to $0.58{\times}10^{-2}(wt.%.S^{-1/2})$. 4. A great deal of propan by addition of nitrogen gas in carburizing gas was possible to saving without considerable change in case hardening depth. 5. The effective carburizing depth range is obtained to 0.8-1.1mm by diffusion temperature of 1123k after carburization at 1273k-3.6ks, and the surface hardness is increased as the increasing of $T_D/T_c$ in our experimental condition, and the maximum hardness as reachin distance from surface is decreased.

• 한국분말재료학회지
• /
• 제21권5호
• /
• pp.349-354
• /
• 2014

This study is a basic research for repair material production which manufactured a Cu repair coating layer on the base material of a Cu plate using kinetic spray process. Furthermore, the manufactured material underwent an annealing heat treatment, and the changes of microstructure and macroscopic properties in the Cu repair coating layer and base material were examined. The powder feedstocks were sphere-shaped pure Cu powders with an average size of $27.7{\mu}m$. The produced repair coating material featured $600{\mu}m$ thickness and 0.8% porosity, and it had an identical ${\alpha}$-Cu single phase as the early powder. The produced Cu repair coating material and base material displayed extremely high adhesion characteristics that produced a boundary difficult to identify. Composition analysis confirmed that the impurities in the base material and repair coating material had no significant differences. Microstructure observation after a $500^{\circ}C/1hr$. heat treatment (vacuum condition) identified recovery, recrystallization and grain growth in the repair coating material and featured a more homogeneous microstructure. The hardness difference (${\Delta}H_v$) between the repair coating material and base material significantly reduced from 87 to 34 after undergoing heat treatment.

• 자원리싸이클링
• /
• 제11권6호
• /
• pp.31-37
• /
• 2002

폐알루미늄 캔으로 제조된 2차지금과 신지금의 혼합비율에 따라 캔용 소재를 주조하고 미세조직을 조사하였다. 또한 주조후 열처리에 따른 상변화의 거동을 조사하였다. 2차지금의 혼합비율(20, 30, 40, 50, 60%)에 따라 캔용 소재를 전기로로 용해하고, ceramic filter를 사용하여 주조하였다. 주조후에는 주조조직 제어를 위해 균질화 열처리($615^{\circ}C$$\times$10hrs)를 하였다. 주조상태에서는 $\alpha$ 상($Al_{12}$ $(Fe,Mn)_3$Si), $\beta$상($Al_{6}$/(Fe,Mn)), 그리고 미세한 $Mg_2$Si상이 알루미늄 기지에 존재하며, 특히 가공성에 나쁜 영향을 미치는 것으로 알려진 $\beta$상이 많이 존재하였다. 그러나 균질화 열처리에 의해 이러한 $\beta$상은 유해성이 없는 $\alpha$상으로의 상변태가 일어났다. 기지내의 미세한 $Mg_2$Si상도 열처리에 의해 $\alpha$상으로 변화하였다. 주조시 여과된 조직을 분석한 결과 Fe, Cu, Si 등의 금속간화합물이 검출되었다.

• Journal of Microbiology and Biotechnology
• /
• 제31권4호
• /
• pp.570-583
• /
• 2021

Pyrococcus furiosus α-amylase can hydrolyze α-1,4 linkages in starch and related carbohydrates under hyperthermophilic condition (~ 100℃), showing great potential in a wide range of industrial applications, while its relatively low productivity from heterologous hosts has limited the industrial applications. Bacillus subtilis, a gram-positive bacterium, has been widely used in industrial production for its non-pathogenic and powerful secretory characteristics. This study was conducted to increase production of P. furiosus α-amylase in B. subtilis through three strategies. Initial experiments showed that co-expression of P. furiosus molecular chaperone peptidyl-prolyl cis-trans isomerase through genomic integration mode, using a CRISPR/Cas9 system, increased soluble amylase production. Therefore, considering that native P. furiosus α-amylase is produced within a hyperthermophilic environment and is highly thermostable, heat treatment of intact culture at 90℃ for 15 min was performed, thereby greatly increasing soluble amylase production. After optimization of the culture conditions (nitrogen source, carbon source, metal ion, temperature and pH), experiments in a 3-L fermenter yielded a soluble activity of 3,806.7 U/ml, which was 3.3- and 28.2-fold those of a control without heat treatment (1,155.1 U/ml) and an empty expression vector control (135.1 U/ml), respectively. This represents the highest P. furiosus α-amylase production reported to date and should promote innovation in the starch liquefaction process and related industrial productions. Meanwhile, heat treatment, which may promote folding of aggregated P. furiosus α-amylase into a soluble, active form through the transfer of kinetic energy, may be of general benefit when producing proteins from thermophilic archaea.

• KSBB Journal
• /
• 제20권1호
• /
• pp.50-54
• /
• 2005

셀룰로오스의 탄화과정에서는 셀룰로오스의 pyrolysis에 의 해 생산된 타르에 의해 탄화 후, 셀룰로오스 탄화물의 섬유구조를 저해시키는 문제점이 존재한다. 이와 같은 결과는 $800^{\circ}C$이상의 탄화온도와 건조 셀룰로오스를 toluene에 침지하고 초음파 처리 후 탄화한 탄화물에서 감소되지만, 섬유구조만의 탄화물을 얻을 수 없었다. 그러나 셀룰로오스의 탄화에서 타르의 생산을 감소시키는 HCI vapor flow 조건에서의 열처리 과정의 적용과 탄화과정 중 생성된 타르의 제거를 통해서 탄화 후, 대부분의 영역에서 섬유 구조를 갖는 탄화물을 얻을 수 있었다.

• 열처리공학회지
• /
• 제4권1호
• /
• pp.30-36
• /
• 1991

Effects of aging treatment on the mechanical properties of a 18 Ni maraging steel were investigated by considering the reverted austenite. Specimens were heat treated by austenitizing at $840^{\circ}C$ for 1 hr and then aged for various times at $480^{\circ}C$ and $520^{\circ}C$. The main results obtained are as follows : 1) The amounts of reverted austenite are increased up to about 4% at $480^{\circ}C$ and about 22% at $520^{\circ}C$ with 1 to 48 hrs aging time. 2) Decreasing tendencies of impact energy and fracture toughness with increasing aging time are diminished after aging for 2 hrs at two aging temperatures of $480^{\circ}C$ and $520^{\circ}C$. 3) Peak hardness and yield strength are obtained after aging for 4 hrs at $480^{\circ}C$ and 2 hrs at $520^{\circ}C$ respectively. From the above results, it was concluded that the optimum aging condition with which showed good strength and toughness combination are given to be $480^{\circ}C$ for 4 hrs and $520^{\circ}C$ for 2 hrs.