• 제목/요약/키워드: Heat treatment condition

검색결과 968건 처리시간 0.027초

알루미늄 제련 폐기물(Red Mud)의 활성화 방법에 따른 수용상의 인산염 제거특성 (Phosphate Removal from Aqueous Solution according to Activation Methods of Red Mud)

  • 김이태;배우근;김우정
    • 한국물환경학회지
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    • 제20권5호
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    • pp.466-472
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    • 2004
  • Red mud is formed as a waste during bauxite refining known as Bayer's process. Its main constituents are iron, aluminium, sodium and silica. The disposal of large quantities of wasted red mud causes a serious ecological problem. In this study, the red mud wasted from the bauxite refinery was studied for phosphate removal from aqueous solution according to activation methods. The influence of heat treatment, and neutralization with sea water and acid treatment level for the optimum conditions for phosphate removal have been determined. Heat treatment combined with acid treatment is most suitable for the removal of phosphate from aqueous solution. The optimal condition was activated with 1 N HCl solution after heating in $600^{\circ}C$ during 4 hours. Acid and heat treatment causes sodalite compounds which hinder the phosphate adsorption to leach out. The adsorption data obtained followed a first-order rate expression and fitted well with the Freundlich Isotherm well.

열처리에 의한 작약의 Paeoniflorin 함량 변화 (Changes of Paeoniflorin Content in Peony Roots by Heat-treatment)

  • 김태강;김광중
    • 한국식품저장유통학회지
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    • 제4권1호
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    • pp.69-75
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    • 1997
  • Peony is a medicinal herb which have utilized widely as chineses medicine. The paeoniflorin is the predominant component In peony root, monoterpene glucoside containing pinane structure. The effective components were extracted with the cold water from the intact peony roots, and effectively extracted with 70% ethanol from the dry powder of peony roots. The changes of paeoniflorin contents were investigated during the drying process of peony roots and processing of peony extract by the heat-treatment. Air-drying was the best condition for the preservation of paeoniflorin content among the drying processes of peony roots. But convective drying at 6$0^{\circ}C$ was recommended for the drying process of peony roots in large scale. The paeoniflorin in peony extracts was not destroyed by the treatment at 6$0^{\circ}C$ and 8$0^{\circ}C$ for 5 hrs, but destroyed 30%, 28% and 40% of paeoniflorin by treatment at 10$0^{\circ}C$ for 5 hrs, 115$^{\circ}C$ and 121$^{\circ}C$ for 10 minutes, respectively. The paeoniflorin was continueously extracted for 4 hrs from the dry pieces of peony roots(0.5$\times$0.5$\times$0.5cm) in boiling water but destroyed gradually after 4 hrs at 10$0^{\circ}C$. Paeoniflorins in 70% ethanol extracts of peony root were not destroyed at all in the process of concentration to dry powder at 60"C on vacuum.cuum.

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독활지황탕으로 호전된 다발성 관절염 환자 치험 1례 (A Case Study of Polyarthritis Treated with Dokhwaljihwang-tang)

  • 이재욱;최현민;임은철
    • 사상체질의학회지
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    • 제29권4호
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    • pp.369-375
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    • 2017
  • Objectives The purpose of this study is to report a case of improving various symptoms such as polyarthritis, dyspnea, fatigue, heat sensation. In addition, the promising explanation on the perspective of the heat and cold syndrome could be elicited. Methods Dokhwaljihwang-tang was prescribed for an outpatient for 3 weeks without any other therapy such as acupuncture, moxibustion and Western medicine. To evaluate the results of this treatment, polyarthritis was assessed by Visual Analogue Scale(VAS). The patient's general condition such as digestion and defecation discomfort is assessed by the progress notes. Results&Conclusions Most of the various symptoms have improved by about 80 percent. It is more important to observe defecation, urine, cold symptoms and condition of hands and feet synthetically.

알루미늄 단조 Lower Arm 개발 (Development of Forged Aluminum Lower Arm)

  • 조용기;윤병은
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1995년도 제2회 단조심포지엄 단조기술의 진보
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    • pp.74-80
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    • 1995
  • Forged aluminum lower arm has been developed to provide weight reduction of suspension parts. It was utilized FEM analysis in design of parts. Prototype parts were producted to two shape & different forging condition. Difference of forging condition was manufacturing process of stock, forging press, forging die, heat treatment condition. As a result, weight reduction of 44%, 38% was achived. Strength and fatigue endurance of forged aluminum lower arm was excellent.

금형주조한 Mo-Ni-Cu계 구상흑연주철의 오스템퍼링 온도 및 시간에 따른 파괴특성 (Fracture Properties of Mo-Ni-Cu Austempered Ductile Iron Cast in Permanent Mold with Austempering Temperature and Time)

  • 이영상;강인찬
    • 한국주조공학회지
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    • 제11권4호
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    • pp.331-337
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    • 1991
  • Various test specimens were prepared by austempering low alloyed Mo-Ni-Cu ductile iron blocks of high graphite nodule count at 270, 320 or $370^{\circ}C$ for 0.5, 1, 3 or 9hrs. Tensile test, CVN impact test and plane-strain fracture toughness test(compact tension specimen of 50mm W) were done for each heat treatment condition at room temperature. X-ray diffractometer and optical microscope were used to investigate the change of microstructure and relationships between microstructure and test results. The highest retained austenite volume percent at each austempering temperature was corresponded to the highest mechanical property. The highest elongation value of 17%, U.T.S. value of 1,600 MPa or $K_{IC}$ value of 90MPa${\surd}$m were reached at each optimum condition. The best heat treatment condition for fracture toughness were 3hrs' holding time combined with the austempering temperature of 270 and $320^{\circ}C$, and 1hr's of $370^{\circ}C$.

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시차주사열량측정법에 의한 니켈기 초내열 합금의 열분석 (Thermal Analysis of Nickel-Base Superalloys by Differential Scanning Calorimetry)

  • 윤지현;오준협;김홍규;윤존도
    • 한국재료학회지
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    • 제26권5호
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    • pp.235-240
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    • 2016
  • Appropriate thermo-mechanical properties of nickel-based superalloys are achieved by heat treatment, which induces precipitation and solid solution hardening; thus, information on the temperature ranges of precipitation and dissolution of the precipitates is essential for the determination of the heat treatment condition. In this study, thermal analyses of nickel-based superalloys were performed by differential scanning calorimetry method under conditions of various heating rates of 5, 10, 20, or 40K/min in a temperature range of 298~1573K. Precipitation and dissolution temperatures were determined by measuring peak temperatures, constructing trend lines, and extrapolating those lines to the zero heating rate to find the exact temperature under isothermal condition. Determined temperatures for the precipitation reactions were 813, 952, and 1062K. Determined onset, peak, and offset temperatures of the first dissolution reaction were 1302, 1388, and 1406K, respectively, and those values of the second dissolution reaction were 1405, 1414, and 1462K. Determined solvus temperature was 1462K. The study showed that it was possible to use a simple method to obtain accurate phase transition temperatures under isothermal condition.

무연황동의 절삭 칩 형태에 미치는 절삭조건과 템퍼링 온도의 영향 (Cutting Chip Forms on the Cutting Condition and Tempering Temperatures of Lead-free Brass)

  • 주영석;이상봉;김시영;주창식;정병호
    • 열처리공학회지
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    • 제25권1호
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    • pp.14-21
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    • 2012
  • The effects of cutting condition and tempering temperature for the shape of cutting chip were investigated. For this purpose, a lead-free brass containing 1wt.% of Bi extruded at $750^{\circ}C$ in straight turning was used in this study. The cutting chip preferred was mainly found to be loose form of arc chips with curling discontinuity, and these were formed by shear fracture. However, some of fragmental element chip were found to be mixed when tempering temperature was as high as $500^{\circ}C$. The form and size of chip was more affected by feed rate than by tempering temperature and cutting rate. In addition, the cutting surface was observed to be formed more rough in the case of high feed rate and low cutting rate compared to low feed rate and high cutting rate.

사형 주조에서 바인더 젯 3D 프린터를 이용한 기계적 물성 향상을 위한 공정 연구 (A Study on the Process for Improving Mechanical Property of Sand Casting by Using the Binder Jetting Method)

  • 황정철;김태성
    • 대한안전경영과학회지
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    • 제25권1호
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    • pp.23-29
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    • 2023
  • Among the Additive Manufacturing (AM) technologies, the Binder-Jetting printing technology is a method of spraying an adhesive on the surface of powder and laminate layer by layer. Recently, this technique has become a major issue in the production of large casting products such as ship-building, custom vehicles and so on. In this study, we performed research to make actual mold castings and increase mechanical property by using special sand and water-based binders. For use as a mold, it has a strength of more than 3MPa and permeability. Various experiments were carried out to obtain suitable them. The major process parameters were binder jetting volume, binder types, layer thickness and heat treatment condition. As a result of this study, the binder drop quantity was measured to be about 60 pico-liter, layer thickness was 100㎛ and the heat treatment condition was measured about 1,000℃ and compressive strength were measured to be more than 5MPa. The optimum condition of this experiment was established through actual casting of aluminum. The equipment used in this study was a Freeforms T400 model (SFS Co., Ltd.), and the printing area of 420 * 300 * 250mm and resolution of 600dpi can be realized.

결정립 미세화된 Cu-Zn-Al 형상기억합금의 열처리 조건에 따른 변태거동 (Transformation Behavior on Heat Treatment Condition in Grain-Refined Cu-Zn-Al Shape Memory Alloy)

  • 강조원;장우양;양권승
    • 열처리공학회지
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    • 제4권4호
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    • pp.34-43
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    • 1991
  • A small amount of misch metal and/or Zr was added as a dopant to 70.5wt----Cu-26wt----Zn-3.5wt----Al shape memory alloy in order to study the effect of grain refinement and heat treatments on the transformation behavior, stabilization of martensite, and shape memory ability. It was found that the addition of misch metal and Zr was very effective for reducing the grain size. The fracture mode has been changed from intergranular brittle fracture to ductile fracture with void formation and coalescence by the addition of misch metal and Zr. Aging of the ${\beta}$-phase decreases the $M_s$ temperature, but that of the martensite phase increases the $A_s$ temperature. The hysteresis of transformation temperature ${\Delta}T(A_s-M_s)$ has an increasing tendancy by grain refinement. The crystal structure of martensite was identified as monoclinic structure. As the grain size decreased, martensite stabilization more easily occured and the shape, memory ability has been reduced by the grain size refined.

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알루미늄 합금(Al 7075) 절삭성 향상을 위한 열간단조 후처리 방법에 관한 연구 (A Study on the Improvement of Machinability in Hot-Forged Aluminum Alloy Product(Al 7075))

  • 김진복;임학진;강범수
    • 한국추진공학회지
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    • 제4권2호
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    • pp.46-53
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    • 2000
  • 알루미늄 제품은 열간단조하면 재료가 연화되어 있어 절삭가공시 연속적인 칩이 발생하여 공구와 피삭재를 감고 회전함으로서 가공면 손상, 공구파손 및 작업자의 안전을 초래함에 따라 가공이 어려워 단지 절삭성 개선목적만을 위해 중간공정으로 T-4열처리하여 절삭가공하고 다시 어닐링처리하여 냉간성형을 하고 최종열처 리를 한다. 따라서 본 연구는 열간단조후 제품을 급냉시키면 용체화처리의 효과를 얻어 재료가 경화됨으로서 절삭성이 개선될 수 있다는 이론에 근거하여 T4열처리를 대체할 수 있는 후처리방법에 대해 연구하였다. 최적의 후처리방법을 구하기 위해 열간단조후 수냉과 공냉처리를 비교분석하였고, 열간단조후 냉각처리까지 지연된 시간과 수냉과정에서의 유지시간에 따른 분식을 통해 최적의 작업조건을 설정하였다.

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