• Polymer(Korea)
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• v.36 no.4
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• pp.448-454
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• 2012

A poly(amic acid) (PAA) was prepared by reaction of 4,4'-(hexafluoroisopropylidene)diphthalic anhydride (6FDA) and 2,2-bis[4-(4-aminophenoxy)phenyl]hexafluropropane (BAPP) in N,N-dimethylacetamide (DMAc). The cast films of the synthesized PAA were thermally treated at different temperatures to create polyimide (PI) films. The heat treatment temperature varied between 80 and $230^{\circ}C$ to investigate the imidization index in relation with the solvent evaporation rates. The progress of PAA imidization was examined using a thermogravimetric analyzer (TGA) and a Fourier transform infrared spectroscope (FTIR) at various time and temperature. The experimental results showed that the imidization index was fast at the initial stage in the presence of solvent, DMAc, reaching the final imidization. When the imidization temperature is high over $200^{\circ}C$, the imidization index decreased because the solvent was evaporated too fast.

• Korean Journal of Food Science and Technology
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• v.46 no.5
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• pp.588-592
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• 2014

Under optimized condition mild pressure in combination with specific temperature for heat treatment transform the 6-gingerol into 6-shogaol. The purpose of this study was to optimize the conditions used for heat treatment under pressure for increasing 6-shogaol content in ginger (Zingiber officinale Roscoe). A central composite experimental design was used to evaluate the effects of application temperature ($70-130^{\circ}C$) and temperature-holding time (95-265 min) on the transformation of 6-shogaol. The experimental values were shown to be in significantly good agreement with the predicted values (adjusted determination coefficient, $R^2{_{Adj}}=0.9857$). 6-Shogaol content increased as the application temperature and temperature-holding time increased. By analyzing the response surface plots, the optimum conditions of heat treatment (temperature and time) for increasing 6-shogaol content were found to be $127^{\circ}C$ and 109 min, respectively. Under these optimal conditions, the predicted 6-shogaol content was 3.98 mg/g dried ginger. The adequacy of the model equation for predicting the optimum response values was effectively verified by the validation data.

• Atmosphere
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• v.32 no.4
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• pp.395-409
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• 2022

A new soil moisture initialization scheme is applied to the Korea Meteorological Administration (KMA) Global Seasonal forecasting system version 6 (GloSea6). It is designed to ingest the microwave soil moisture retrievals from Soil Moisture Active Passive (SMAP) radiometer using the Local Ensemble Transform Kalman Filter (LETKF). In this technical note, we describe the procedure of the newly-adopted initialization scheme, the change of soil moisture states by assimilation, and the forecast skill differences for the surface temperature and precipitation by GloSea6 simulation from two preliminary experiments. Based on a 4-year analysis experiment, the soil moisture from the land-surface model of current operational GloSea6 is found to be drier generally comparing to SMAP observation. LETKF data assimilation shows a tendency toward being wet globally, especially in arid area such as deserts and Tibetan Plateau. Also, it increases soil moisture analysis increments in most soil levels of wetness in land than current operation. The other experiment of GloSea6 forecast with application of the new initialization system for the heat wave case in 2020 summer shows that the memory of soil moisture anomalies obtained by the new initialization system is persistent throughout the entire forecast period of three months. However, averaged forecast improvements are not substantial and mixed over Eurasia during the period of forecast: forecast skill for the precipitation improved slightly but for the surface air temperature rather degraded. Our preliminary results suggest that additional elaborate developments in the soil moisture initialization are still required to improve overall forecast skills.

• Proceedings of the KSME Conference
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• 2000.11a
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• pp.280-285
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• 2000

It is very important to evaluate the surface or subsurface microstructure because of their influences on mechanical properties of materials. Surface SH-wave which is horizontally polarized shear wave traveling along near surface and subsurface layer is an attractive technique for material evaluation. The destructive method is widely used for the estimation of material degradation but it has a great difficulty in preparing specimens from in-service industrial facilities. In this study, nondestructive evaluation for degraded structural materials used at high temperature though surface SH-wave method is discussed. 2.25Cr-1Mo steel specimens which were prepared by the isothermal aging heat treatment at $650^{\circ}$ were evaluated though ultrasonic nondestructive evaluation techniques investigating the change of sound velocity, attenuation coefficient and amplitude spectra. In addition, it has verified experimentally the frequency-dependence of attenuation coefficient though wavelet analysis method.

• Design & Manufacturing
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• v.2 no.2
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• pp.6-9
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• 2008

Injection molding is representative process of plastic production. Most of numerical analyses for injection molding have been based on the Hele Shaw's approximation: two-dimensional flow analysis. The present work covers numerical analyses of injection molding using three-dimensional solid elements. The accuracy of the analysis results has been verified through some numerical examples in comparison with the various conditions. In this study, moldflow software was used to analyze the cooling analysis. The results of cooling analysis and testing catapult were compared for plastic products.

• Journal of the Korean institute of surface engineering
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• v.38 no.2
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• pp.83-87
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• 2005

We enhanced the color of blue sapphires and rubies successfully by using a oxygen-propane torch flame annealing, which had not been employed so far. We confirmed that about 1 mm-thick de-coloring of the corundum samples were available with 60 minutes flame annealing through eye evaluation, color coordination characterization, and methylene iodide immersion observation. We also suggest that the color centers such as $[Fe_{Al}^{\cdot}]$ may transform into transparent $[Fe_{Al}^{x}],\;[Cr_{A1}^{x}]$ sites with $[V_o^']$ generation at the elevated temperature in oxygen-rich atmosphere by diffusion mechanism. Our results implied that the longer diffusion time and the higher oxygen partial pressure might lead to the better de-coloring enhancement in corundum gem stones.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.58 no.10
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• pp.1982-1988
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• 2009

$TiO_2$ films are fabricated using silk printing method. Heat treatment temperature of films is 600[$^{\circ}C$]. From the analysis of microstructure, grain size of $TiO_2$ films is about $0.2{\sim}0.3[{\mu}m]$. Thickness of films is 30.19[${\mu}m$] and surface uniformity of films is good. From the analysis of crystalline structure, $TiO_2$ films transform anatase phase to rutile phase. Capacitance of films increases according to increase relative humidity and decrease measuring frequency. Hysteresis characteristics of capacitance and impedance are best at 45[%RH] and 75[%RH] respectively. Impedance of films increases according to decrease measuring frequency.

• 연구논문집
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• s.24
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• pp.81-96
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• 1994

To investigate failure mechanisms observed in carbon-phenolic thermal insulators, differential equations which govern the decomposition process in a deformable anisotropic porous solid are derived for three-dimensional axisymmetric constructions. The governing equations not only couple the material deformation with pore pressure, but also couple pressure and temperature, which means that heat convected by the pyrolysis gases is properly accounted for. Then the Bubnov-Galerkin finite element method is applied to these equations to transform them into a semidescrete finite element system. A thermal insulation liner in the cowl region under typical operating conditions is analyzed to find a mechanism for plylift. The results from the structural analysis show across-ply failure in the cowl zone. The mechanism for plylift is hypothesized as a sequential procedure : 1) the across-ply failure which is the precursor to plylift and 2) the local fiber buckling caused by generation of excessive in-plane compressive stress. To prevent plylift, the across-ply stress can be reduced by using appropriate material ply angles in cowl zone design.

• Textile Coloration and Finishing
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• v.35 no.4
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• pp.221-230
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• 2023

Meta-aramid and polyamic acid were separated and the manufactured films were analyzed for their integration and logarithmic properties. The miscibility of meta-aramid and polyamic acid was analyzed by Fourier transform infrared spectroscopy and scanning electron microscopy. Using calorimetric analysis and differential scanning calorimetry, the storage of meta-aramid and polyamic acid, indicated on the right side of the column, was analyzed. It was confirmed that the initial thermal resistance occurs because the polyamic acid is accounted for in the meta-aramid, and the glass transition temperature and persistence phenomenon are explained.

• Steel and Composite Structures
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• v.51 no.1
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• pp.1-8
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• 2024

Transient dynamic behavior of a sandwich beam under thermal and impulsive loads has been researched in the context of higher-order beam theory. The impulse load of blast type has been enforced on the top exponent of the sandwich beam while it is in a thermal environment. The core of the sandwich beam is cellular with auxetic rectangular pattern, whereas the layers have been built with the incorporation of graphene oxide powder (GOP) and are micromechanically introduced through Halpin-Tsai formulization. Governing equations for the sandwich beam have been solved through inverse Laplace transform style for obtaining the dynamical deflections. The connection of beam deflections on temperature variability, GOP quantity, pulse load situation and core relative density has been surveyed in detail.