• 제목/요약/키워드: Heat Treatment Technique

검색결과 356건 처리시간 0.027초

SnO$_2$박막의 전기적 특성에 미치는 불소 doping및 열처리 효과 (Effect of fluorine doping and heat treatment for SnO$_2$ thin films on electrical properties)

  • 류득배;이수완;박정일;박광자
    • 한국표면공학회지
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    • 제33권2호
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    • pp.87-92
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    • 2000
  • Transparent and electrical conducting tin oxide thin films were fabricated on soda lime silicate glass by thermal chemical vapour deposition technique. Thin films were deposition from mixtures of tetramethyltin (TMT) as a precursor, oxygen or oxygen containing ozone as an oxidant and 1,1,1,2-tetrafluoroethane as a doping material. Electrical properties of fabricated tin oxide films were changed depending on substrate temperature, and the amount of dopant. Resistivity of tin oxide films was reduced by doping fluorine or heat treatment. Thin films can be optimized at TMT flow rate of 8sccm, oxygen flow rate of 150sccm, 1,1,1,2-tetrafluoroethane floe rate of 300sccm and substrate temperature $380^{\circ}C$. In this conditions, the lowest resistivity of tin oxide films were $9$\times$10^{-4}$ $\Omega$cm.

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퀜칭과정에서 상변태를 고려한 탄소성 열응력의 유한요소해석(I) -오스테나이트에서 퍼얼라이트로의 변태- (An Analysis Finite Element for Elasto-Plastic Stresses Considerating Phase Transformation at the Quenching Process(I) - From Austenite to Pearlite -)

  • 김옥삼;구본권
    • 열처리공학회지
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    • 제7권4호
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    • pp.233-243
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    • 1994
  • Constitutive relation of thermoelasto-plastic material undergoing phase transformation during quenching process were developed on the basic of continuum thermodynamics. The metallic structure, temperature and residual stresses distributions were numerically calculated by the finite element technique. The metallic structure were defined by transformation from austenite to pearlite and characterized as a fuction of thermal history and mixture rule of phase. On the distribution of thermal stress along the radial direction, axial and tangential stresses are compressive in the surface, and tential in the inner part. Radial stress is tensile in the whole body. The reversion of residual stress takes plase at 11.5~15.5mm from the center.

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디젤엔진 피스톤용 SCM440의 레이저 표면경화부의 잔류응력 (Residual Stress Distribution of Laser Hardened SCM440 for Diesel Engine Piston)

  • 이동석;유웅재;김재도
    • 열처리공학회지
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    • 제8권3호
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    • pp.182-186
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    • 1995
  • SCM440, which is widely used as the diesel engine piston of vessel, has been hardened by a $CO_2$ laser with the wavelength of $10.6{\mu}m$. Laser hardening experiment has been carried out for the condition of a laser power 1kW, the travel speed between 0.4 and 1.5m/min, and a rectangular-Gaussian beam. Residual stress has been measured by using middle point technique of half value width of X-ray diffraction method. It was found that the compressive residual stress with the range between 400 and 600MHz has distributed in the laser hardening zones and the tensile residual stress between 100 and 200MHz has distributed in the boundary of hardening zones.

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용접부 잔류응력의 이완에 관한 해석 (Numerical Analysis for Residual Stress Relaxation of Weld Zone)

  • 서정원;구병춘;이동형;정홍채
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 춘계학술대회
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    • pp.43-48
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    • 2003
  • The problem of welding stresses and fatigue behavior is the main concerns of welding research fields. The residual stresses and distortion of structures by welding is exert negative effect on the safety of mechanical structures. That is, expansion of material by high temperature and distortion by cooling during welding process is caused of tensile and compressive residual stresses on welding material, and this residual stresses reduce fracture and fatigue strength of welding structures. The accurate prediction of residual stress and relaxation due to loading and post weld heat treatment of weld zone is very important to improve the quality of weldment. In this study, a finite element modeling technique is developed to simulate the relaxation of residual stresses due to loading and post weld heat treatment of weld zone. The accuracy of finite element models is evaluated based on experimental results and the results of the analytical solution.

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준위상정합된 리튬탄탈레이트 광도파로에서의 청색 광파 생성 (Blue Light Generation in a Quasi-Phase-Matched $LiTaO_3$ Optical Waveguide)

  • 이상윤;신상영;진용성
    • 전자공학회논문지A
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    • 제32A권12호
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    • pp.173-183
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    • 1995
  • Blue light of 0.15mW at 417.6nm is generated in a quasi-phase-matched LITaO$_{3}$ optical waveguide. A new heat-treatment technique using a metal-oxide mask is proposed to fabricate the periodic domain-inverted grating with less degraded optical properties. The mask promotes the proton indiffusion by inhibition of the proton outdiffusion during the heat treatment. It reduces the amount of the initial proton exchange for the domain inversion and prevents the formation of crystal defects on the surface accompanied by the proton outdiffusion. Consequently, it minimizes the degradation of nonlinear coefficient and scattering loss caused by the initial proton exchange.

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감광성유리를 이용한 마이크로머시닝 기술 (Micromachining technology using photosensitive glass)

  • 조수제
    • 한국레이저가공학회지
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    • 제14권1호
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    • pp.25-29
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    • 2011
  • Micromachining of photosensitive glass by UV exposure, heat treatment, and etching processes is reported. Like photoresist, the photosensitive glass is also classified into positive and negative types by development characteristics. For the positive type, the exposed area is crystallized and etched away during the etching process in HF solution, whereas the unexposed area is crystallized and etched away for the negative type. The crystallized area of the photosensitive glass has an etch rate approximately 30~100 times faster than that of the amorphous area so that it becomes possible to fabricate microstructures in the glass. Based on the unique properties of glass such as high optical transparency, electrical insulation, and chemical/thermal stability, the glass micromachining technique introduced in this work could be widely applied to various devices in the fields of electronics, bio engineering, nanoelectonics and so on.

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반응성 이온빔 스퍼터링법에 의해 제조된 ATO박막 (ATO Thin Films Prepared by Reactive lout Beam Sputtering)

  • 구창영;김경중;김광호;이희영
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
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    • pp.361-364
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    • 2000
  • Antimony doped tin oxide (ATO) thin films were deposited at room temperature by reactive ion-beam sputter deposition (IBSD) technique in oxidizing atmosphere utilizing Sb and Sn metal targets. Effect of Sb doping concentration, film thickness and heat treatment on electrical and optical properties was investigated. The thickness of as-deposited films was controlled approximately to 1500 $\AA$ or 2000$\AA$, and Sb concentration to 10.8 and 14.9 wt%, as determined by SEM and XPS analyses. Heat treatment was performed at the temperature from 40$0^{\circ}C$ to 80$0^{\circ}C$ in flowing $O_2$or forming gas. The resulting ATO films showed widely changing electrical resistivity and optical transmittance values in the visible spectrum depending on the composition, thickness and firing condition.

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Effect of silane activation on shear bond strength of fiber-reinforced composite post to resin cement

  • Kim, Hyun-Dong;Lee, Joo-Hee;Ahn, Kang-Min;Kim, Hee-Sun;Cha, Hyun-Suk
    • The Journal of Advanced Prosthodontics
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    • 제5권2호
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    • pp.104-109
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    • 2013
  • PURPOSE. Among the surface treatment methods suggested to enhance the adhesion of resin cement to fiberreinforced composite posts, conflicting results have been obtained with silanization. In this study, the effects of silanization, heat activation after silanization, on the bond strength between fiber-reinforced composite post and resin cement were determined. MATERIALS AND METHODS. Six groups (n=7) were established to evaluate two types of fiber post (FRC Postec Plus, D.T. Light Post) and three surface treatments (no treatment; air drying; drying at $38^{\circ}C$). Every specimen were bonded with dual-curing resin cement (Variolink N) and stored in distilled water for 24 hours at $37^{\circ}C$. Shear-bond strength (MPa) between the fiber post and the resin cement were measured using universal testing device. The data were analyzed with 1-way ANOVA and by multiple comparisons according to Tukey's HSD (${\alpha}$=0.05). The effect of surface treatment, fiber post type, and the interactions between these two factors were analyzed using 2-way ANOVA and independent sample T-tests. RESULTS. Silanization of the FRC Postec Plus significantly increased bond strength compared with the respective non-treated control, whereas no effect was determined for the D.T. Light Post. Heat drying the silane coupling agent on to the fiberreinforced post did not significantly improve bond strength compared to air-syringe drying. CONCLUSION. The bond strength between the fiber-reinforced post and the resin cement was significantly increased with silanization in regards to the FRC Postec Plus post. Bond strength was not significantly improved by heat activation of the silane coupling agent.

A COMPARATIVE STUDY OF THE PROTECTION OF DHAINCHA (Sesbania aculeata) SEED MEAL AND FISH MEAL FROM RUMEN DEGRADATION USING NYLON BAG TECHNIQUE

  • Hussain, M.;Chowdhury, B.;Siddiqua, A.;Routh, C.K.;Saadullah, M.
    • Asian-Australasian Journal of Animal Sciences
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    • 제6권2호
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    • pp.197-203
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    • 1993
  • The protection of dry matter and nitrogen from rumen degradation of dhaincha seed (Sesbania aculeate) meal was studied using nylon bag technique. The dhaincha seed meal was subjected to various heat treatments that included oven drying, autoclaving and boiling. Similar experiment was conducted with fish meal as reference for comparison. The oven-dried dhaincha meal was found to retain more dry matter and nitrogen than was found boiled or autoclaved meal. While autoclaving appeared to improve nitrogen and dry matter retention to some extent, boiling seemed to cause more loss of dry matter from nylon bag. Heat treatment caused high retention of nitrogen by fish meal. The calculated effective protein degradation was 80.4% and 83.2% for the oven dried fish meal and dhaincha seed meal whereas same values were 74.2% and 86.7% for autoclaved fish and dhaincha seed meal respectively at the outflow rate of 4.4% per hour. The in vitro study revealed higher digestibility for heat treated samples by pepsin. The dry matter, nitrogen and ash content of dhaincha seed meal were 85.93%, 5.93% and 7.31% respectively.

수승화강(水升火降) 조절법(調節法)(수화조절법(水火調節法))에 대한 제언 -약침을 이용하여- (Proposal on the Method of Regulating Ascending Kidney Water and Descending Heart Fire -through pharmacopuncture technique-)

  • 권기록
    • 대한약침학회지
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    • 제10권3호
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    • pp.149-155
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    • 2007
  • Objectives The purpose of this study is aimed at diagnosing and suggesting treatment plans for commonly seen clinical manifestation of heat symptom in the upper body and coldness in the lower body, also known as hot above, cold below syndrome. Methods Various reasons attribute to the presence of hot above, cold below syndrome, but mainly contributed by blockage of normal Qi flow by abnormality of heart-kidney root, spleen-stomach axis, and liver-lung axis. Diagnosing these abnormalities and timely alleviation to the healthy state is presented in the study. Results 1For heat in the upper body, Huang Lian Jie Du Tang(黃連解毒湯), CF, or JsD pharmacopuctures are injected on GB21, GB20. Qi stagnation in the thoracic area is treated with BUM injection on CV17. For impairment of transportation and transformation in the middle energizer, BUM pharmacopuncture is injected on CV12. Coldness in the lower energizer was relieved by bee venom or Sweet BV(Bee Venom free from enzymes) on CV6. Conclusion Above proposed methods of regulating water-fire were effective in treating hot above, cold below syndrome in clinical manifestations. But once the symptom subsides, treatment focused on eliminating innate cause should be rendered to achieve more successful results.