• 대한치과기공학회지
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• 제21권1호
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• pp.27-41
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• 1999

치과용 Ag기 합금에서 30wt%Pd 및 10wt%Cu의 용질농도의 구성비가 3이 되는 3원 합금과 여기에 2wt% Au의 첨가에 미치는 석출상의 영향을 조사 분석하여 아래와 같은 결론을 얻었다. Ag-Pd-Cu 3원 합금은 $\alpha$ 단일상에서 Ag-rich ${\alpha}_2 $ 및 PdCu 규칙상에 의해서 경화반응이 진행되며 연속승온시효곡선에 의하면 100-$300^{\circ}C$의 저항증가와 300-$500^{\circ}C$의 저항감소라고 하는 2단계 변화에 의해서 경화곡선이 얻어졌다. 또한 본 합금의 시효과정에서는 ${\alpha}{\to}{\alpha}_2+PdCu{\to}$의 2상 분리반응에 의하여 경화원인이 되었다. 석출과정은 ${\alpha}{\to}{\alpha}_1+PdCu{\to}{\alpha}_2+PdCu$ 이고 Cu-rich인 ${\alpha}_2$상은 거의 나타나지 않으며 최고 경도값은 ${\alpha}_2$ 및 PdCu의 2상공존 구역에서 나타났다. 미량의 Au첨가에 의해서 경화는 다소 증가하지만 경화성보다는 내식성에 보다 크게 기여하였고 Pd/Cu=3인 합금은 Pd/Cu=1 또는 1.7의 합금보다도 전반적으로 경도값은 가장 낮게 나타나며 이것은 치과용 Ag기 합금의 시효경화성에는 Cu농도가 크게 기여하였다. 불연속석출물인 nodule 생성물은 입계에 우선 형성되어 $\alpha$ matrix로 진행되어 nodule 석출물은 부드러운 경계면을 가지고 $\alpha$ matrix주위에 strain matrix를 나타내므로 nodule 형성이 본 합금의 시효경화를 야기하였다. 내식성은 Pd 함량이 가장 높은 본 합금에서 매우 양호하게 나타났으며 Pd 함량이 증가가 내식성의 향상에 크게 기여하여 미량의 Au 첨가에 의해서 보다 현저히 효과를 얻었다. 본 합금의 시효열처리 조건은 $450^{\circ}C$ 적절하며 1-120min 시효시간에 걸쳐서 소정의 경도 값을 얻을 수 있고 시효경화성 및 내식성의 결과로부터 Ag-30wt%Pd-10wt%Cu합금 및 미량 Au 합금은 치과용 금속재료로 적합하였다.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2003년도 추계학술발표대회 논문집
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• pp.46-49
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• 2003

Cu have been widely used as signal transmission materials for electrical electronic components owing to its high electrical conductivity. However, it's size have been limited to small ones due to its poor mechanical properties, Until now, strengthening of the copper at toy was obtained either by the solid solution and precipitation hardening by adding alloy elements or the work hardening by deformation process. Adding the at toy elements lead to reduction of electrical conductivity. In this aspect, if carbon nanofiber is used as reinforcement which have outstanding mechanical strength and electric conductivity, it is possible to develope Cu matrix nanocomposite having almost no loss of electric conductivity. It is expected to be innovative in electric conduct ing material market. The unidirectional alignment of carbon nanofiber is the most challenging task developing the copper matrix composites of high strength and electric conductivity In this study, the unidirectional alignment of carbon nanofibers which is used reinforced material are controlled by drawing process in order to manufacture the intermediary materials for the carbon nanofiber reinforced Cu matrix nanocomposite and align mechanism as well as optimized drawing process parameters are verified via experiments and numerical analysis. The materials used in this study were pure copper and the nanofibers of 150nm in diameter and of $10~20\mu\textrm{m}$ In length. The materials have been tested and the tensile strength was 75MPa with the elongation of 44% for the copper it is assumed that carbon nanofiber behave like porous elasto-plastic materials. Compaction test was conducted to obtain constitutive properties of carbon nanofiber. Optimal parameter for drawing process was obtained by experiments and numerical analysis considering the various drawing angles, reduction areas, friction coefficient, etc Lower reduction areas provides the less rupture of cu tube is not iced during the drawing process. Optimal die angle was between 5 degree and 12 degree. Relative density of carbon nanofiber embedded in the copper tube is higher as drawing diameter decrease and compressive residual stress is occurred in the copper tube. Carbon nanofibers are moved to the reverse drawing direct ion via shear force caused by deformation of the copper tube and alined to the drawing direction.

• 한국재료학회지
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• 제10권5호
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• pp.335-342
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• 2000

리늄판의 미세경도를 압흔 하중 및 온도의 함수로 구하였다. 미세경도의 온도의존성은 상온에서 100$0^{\circ}C$까지의 범위에서 Vickers 압흔기가 내장된 고온 미세압흔기를 이용하여 연구되었다. 미세경도의 하중의존성은 Vickers와 Knoop 압흔기를 이용하여 검토되었다. 압흔 크기 영향은 표준화된 Meyers법칙에 위해 충분히 설명 되었다. 압흔도중 압흔기 아래에서의 가공경화 때문에 어닐링된 리늄판 경도값은 높은 압흔 하중에서 압련되 리늄판의 경도값에 접근하였다. 경도의 하중의존성으로부터 외삽하여 얻어진 하중 영에서의 경도값은 경도값이 다른 열활성을 나타내는 두 개의 다른 기구에 의해 제어됨을 제시하였다. 낮은 온도에서 활성화에너지는 0.02eV 였으며, 한편 높은 온도에서 활성화에너지는 0.15eV 였다. 이때 전이온도는 대략 $250^{\circ}C$ 이었다.

• 대한기계학회논문집A
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• 제26권12호
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• pp.2581-2589
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• 2002

In this research, fretting tests were conducted in air to investigate the wear characteristics of fuel cladding materials with the fretting parameters such as normal load, slip amplitude, frequency and the number of cycles. A high frequency fretting wear tester was designed for this experiment by KAERI. After the experiments, the wear volume and the shape of wear contour were measured by the surface roughness tester. Tribologically transformed structures(TTS) were analysed by means of optical and scanning electron microscopes to identify the main wear mechanisms. The results of this study showed that the wear volume were increased with increasing slip amplitude, and the shape of wear contour was transformed V-type to W-type. Also, it was found that the critical slip amplitude was 168${\mu}{\textrm}{m}$. These phenomena mean that wear mechanism transformed partial slip to gross slip to accelerate wear volume. The wear depth increased with an increase of friction coefficient due to increase of normal load and frequency. The fretting wear mechanisms were believed that, after adhesion and surface plastic deformation occurred by relative sliding motion on the contact between two specimens, TTS creation was induced by surface strain hardening and wear debris were detached from the contact surface which were produced by the micro crack propagation and creation.

• 대한기계학회논문집A
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• 제26권7호
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• pp.1317-1323
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• 2002

This paper describes the comparison of calculated effective stress with experimental one in austenitic heat resistant steels, STS310J1TB and STS310S with and without a small amount of Nb and N. Based on a solute atoms diffusion model, contribution from soluble nitrogen to the high-temperature strength was numerically examined for austenitic heat-resisting Fe-Cr-Ni-N(STS310J1TB) and Fe-Cr-Ni (STS310S) alloys. The solute atmosphere dragging stress of dislocation was calculated in optional dislocation velocity of STS310J1TB and STS310S at $650^{\circ}C$, $675^{\circ}C$ and $700^{\circ}C$. As a result of the numerical calculation, the solute atmosphere dragging stress of STS310J1TB was about 50 times larger than that of STS310S. When the temperature became high, the maximum value of solute atmosphere dragging stress was small and the velocity of moving dislocation was fast. From the relationship between the dislocation rate and the solute atmosphere dragging stress, the relation of both was proportional and the inclination is about 1 in the level with low velocity of moving dislocation. From above results, the mechanism of dislocation movement in STS310J1TB was the solute atmosphere dragging stress. The solute atmosphere dragging stress, which was calculated from the numerical calculation was close to the effect stress in stress relaxation tests.

• 대한기계학회논문집A
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• 제27권8호
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• pp.1398-1408
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• 2003

Tensile and LCF(low cycle fatigue) tests were carried out in air at wide temperature range 20$^{\circ}C$-750$^{\circ}C$ and strain rates of 1${\times}$10$\^$-4//s-1${\times}$10$\^$-2/ to ascertain the influence of strain rate on tensile and LCF properties of prior cold worked 316L stainless steel, especially focused on the DSA(dynamic strain aging) regime. Dynamic strain aging induced the change of tensile properties such as strength and ductility in the temperature region 250$^{\circ}C$-600$^{\circ}C$ and this temperature region well coincided with the negative strain rate sensitivity regime. Cyclic stress response at all test conditions was characterized by the initial hardening during a few cycles, followed by gradual softening until final failure. Temperature and strain rate dependence on cyclic softening behavior appears to result from the change of the cyclic plastic deformation mechanism and DSA effect. The DSA regimes between tensile and LCF loading conditions in terms of the negative strain rate sensitivity were well consistent with each other. The drastic reduction in fatigue resistance at elevated temperature was observed, and it was attributed to the effects of oxidation, creep and dynamic strain aging or interactions among them. Especially, in the DSA regime, dynamic strain aging accelerated the reduction of fatigue resistance by enhancing crack initiation and propagation.

• 자원리싸이클링
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• 제21권3호
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• pp.28-38
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• 2012

이 논문에서는 시멘트를 전혀 사용하지 않고 결합재로서 플라이애쉬를 100% 사용한 알칼리 활성 콘크리트를 개발할 목적으로 알칼리 활성화제의 화학적 변화에 따른 모르타르의 압축강도에 미치는 영향과 SEM/ EDS 및 XRD 등의 미세구조 분석을 검토하였다. 그 결과, 몰농도가 높을수록 초기강도에 큰 영향을 미치는 것으로 분석되었고, 압축강도의 크기에 비례하여 $Si^{4+}$ 및 $Al^{3+}$량이 용출되었다. 또한 SEM 및 EDS로 조직을 분석한 결과 모르타르의 조직구조에 큰 영향을 미치는 성분은 Al 및 Si 성분이었고, XRD 분석결과 활성화제 성분차이에 따른 세기(intensity)의 차이는 거의 없는 것으로 나타났다.

• 터널과지하공간
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• 제11권3호
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• pp.225-236
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• 2001

암반 절리면의 거칠기는 전단강도 및 변형거동에 가장 중요한 영향을 미치는 요소 중의 하나이다. 절리면은 전단변형이 발생하는 동안 손상을 받게 되고 이에 따라 거칠기각은 연속적으로 낮아진다. 절리면의 수직팽창성과 강도 경화 및 연화현상도 거칠기의 변화와 관련이 있는 것으로 이해되고 있다. 따라서 절리면의 거칠기의 변화를 효율적으로 반영시킬 수 있는 수치해석 모델의 개발이 중요하다. 이 연구에서는 탄소성이론을 바탕으로 거칠기 변화를 고려할 수 있는 탄소성 응력-변형 증분식을 유도하여 절리면 거질기 변화가 절리면 전단거동에 미치는 영향을 정량적으로 평가하는데 이용하였다. 유도된 탄소성 증분식을 검증하기 위하여 수치 주기전단시험을 실시하였다. 수치시험결과 개발된 탄소성 증분식은 거친 절리면의 주기전단시험에 나타나는 일반적인 현상들을 모사하는데 효과적임을 알 수 있었다.

• 소성∙가공
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• 제19권6호
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• pp.337-343
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• 2010

Current need of weight reduction in automotive part increases the application for high strength steel (HSS). The various types of high strength steels have been used to produce chassis part, control arms and trailing arms for weight reduction and increasing of fatigue durability such as dual phase steel (DP) and ferrite bainite steel (FB). But, DP and FB steels have proven to show inferiority in durability as well as press formability. Edge cracking occurred often in flange forming and hole expansion processes is the major failure encountered. This paper discussed the behavior of edge stretchability of high strength steel of DP and FB steels. Experimental works have been conducted to study the effect of punch clearance and burr direction on hole expansion ratio (HER). Also finite element simulation (FEM) has been preformed to clarify the mechanism of flange crack and support the experimental results on HER of DP and FB steels. It was simulated the whole process of blanking process following by hole expansion process and ductile fracture criterion named the modified Cockcroft-Latham model which was used to capture the fracture initiation. From the hole expansion tests and FEM simulation studies it was concluded that ferrite bainite steel showed better stretch-flangeability than dual phase steel. It was attributed to the lower work hardening rate of ferrite bainite steel than dual phase steel at the sheared edge.

• Clinical and Experimental Reproductive Medicine
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• 제22권2호
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• pp.183-189
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• 1995

In human IVF-ET, the development and morphology of the embryo have been known to affect implantation and pregnancy rates(PRs). Recently, pregnancy has been reported to related to the embryos with thick zona-pellucida, high levels of fragmentation, poor blastomere development and zona hardening. Although the mechanism of implantation is unclear, it is thought that the hatching process precedes implantation and that the hatching is related to implantation and PRs. This study was carried out to investigate the effect of assisted hatching(AHA) on the improvement of PRs in human IVF-ET. The results were as follows; 1. The PRs of the AHA group (40.8%) was significantly higher than that of control group(27.2%)(P<0.01). 2. According to the age of patients, the PRs of control and AHA groups were 33.9%(20/59), 44,4%(12/27) in <30 yrs, 26.1%(30/115), 38.3%(18/47) in 31-35 yrs, 22.4%(13/58), 41.4%(12/29) in >36 yrs, respectively. 3. According to the factors of infertility in AHA group, unexplained(immunologic factor) (40.0%) and male factors(41.9%) were higher than female(tubal obstruction, endometriosis, adhesion) factor (28.9%). As a result, it is suggested that AHA technique improve the PRs in poor prognosis patients. It is concluded that AHA method can be used to improve the PRs in human lVF-ET.