• 대한금속재료학회지
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• 제50권1호
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• pp.59-63
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• 2012

Studying the long-range ordering of nanopores on the anodic aluminum oxide (AAO) membranes under a hard anodization (HA) approach is crucial in producing well-aligned nanopores on the AAO membranes. Electro-polishing in a mixture of ethanol and perchloric acid for 5 min removed marks formed by rolling and produced flat surfaces on aluminum substrates. The AAO was formed by the first HA process, providing seeds for the subsequent production of uniform AAO nanopores. The second HA process carried out on the seeds produced well-aligned, uniform AAO nanopores. The AAO nanopores, varying in size and shape, were observed with voltages applied for HA. This study provides a route for controlling the size and shape of AAO nanopores by changing the applied voltages.

• 한국정보전자통신기술학회논문지
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• 제16권5호
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• pp.217-222
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• 2023

본 논문은 제조공정이 단순하고, 공정시간도 매우 짧아 제조원가를 절감할 수 있는 고분자 유기하드마스크를 합성하는데 목적을 두었다. 승화 정제 장치를 통한 잔류금속을 측정한 결과, 9-Naphthalen-1-ylcarbazole(9-NC)은 4th zone에서 101.75ppb, 2-Naphthol(2-NA)은 5th zone에서 306.98ppb, 9-Fluorenone(9-F)는 4th zone에서 5th zone 사이에서 129.05ppb로 측정되었다. 그리고 합성된 유기하드마스크를 필터 시스템을 거친 후 잔류금속을 측정한 결과 9 ~ 7ppb 측정되었다. 또 열분석 변화를 측정한 결과, 2.78%로 감소하였고 분자량은 942로 측정되었고 탄소 함량은 89.74%이고 수율은 72.4%로 나타났다. 에칭 속도는 평균 18.22Å/s로 측정되었고 코팅 두께 편차는 평균 1.19로 측정되었다. 유기하드마스크의 입자크기가 0.2㎛ 이하에서는 입자가 존재하지 않았다. 코팅 속도를 1,000, 1,500, 1,800rpm으로 변화를 주어 코팅 두께를 측정한 결과, 수축률은 17.9에서 20.8%까지 측정되었고 코팅 결과 SiON과 접착력이 우수하고 유기하드마스크가 균일하게 도포되었음을 알 수 있었다.

• 대한금속재료학회지
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• 제46권4호
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• pp.223-226
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• 2008

The comparison of sintering behavior and mechanical properties of ultra-fine WC-10wt.%Co and WC-10wt.%Fe hard materials produced by high-frequency induction heated sintering (HFIHS) was accomplished using ultra fine powder of WC and binders(Co, Fe). The advantage of this process allows very quick densification to near theoretical density and prohibition of grain growth in nano-structured materials. Highly dense WC-10Co and WC-10Fe with a relative density of up to 99% could be obtained with simultaneous application of 60 MPa pressure and induced current within 1 minute without significant change in grain size. The hardness and fracture toughness of the dense WC-10Co and WC-10Fe composites produced by HFIHS were investigated.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2003년도 춘계학술대회논문집
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• pp.160-163
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• 2003

For the purpose of rolling hard metals such as silicon steel and non-ferrous metals, the backup roll driven-type mill has been widely used in cold rolling industry. Since the backup roll drive results in horizontal bending of the work rolls and therefore exerted reciprocal action on the roll gap contour, the selection of slim work rolls is very restricted. In this paper, we present an analytic equation based scheme to determine a proper horizontal position of work roll minimizing the horizontal force subject to mechanical constraints.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2002년도 춘계학술발표회 초록집
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• pp.35-35
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• 2002

Atomic force microscopy was applied to study the formation and growth mechanism of thin chrome layers prepared under various pulse plating conditions. The chrome was electro-deposited from an electrolyte bath containing 250 gl-l of chromic acid, 25 gl-l of sulfuric acid using direct current density of $1.6{\;}mA.$\textrm{mm}^{-2} and pulse currents with on-off time from 5 to 900 ms. The higher current density enhanced nucleation rate which resulted in refining grain size. The chrome growth kinetics determining nodule size and shape significantly depends on the duration of on-time rather than duration of off-time and on/off time ratio.

• Journal of Welding and Joining
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• 제33권4호
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• pp.37-43
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• 2015

Characteristics of dissimilar metal welds between STS 316L and carbon steel ASTM A516 Gr.70 made with GTAW have been evaluated in terms of microstructure, ferrite content, chemical analysis, hardness and corrosion resistance. Three heat inputs of 9.00, 11.25, 13.00kJ/cm were employed to make joints of dissimilar metals with ER309 wire. Based on microstructural examination, the amount of vermicular type of ${\delta}$-ferrite was increased with increasing heat input due to the increase of Creq/Nieq in the second layer of welds. Based on the EDX analysis of weld metals, Cr and Ni content in the 2nd layer increased while those content in the first layer of welds decreased with heat inputs. Cellular solidification mode in the 1st layer and dendritic solidification mode in the 2nd layer due to different cooling rates were prevailed, respectively. Heat affected zone which formed hard microstructure showed higher hardness than the weld metal. The salt spray test of dissimilar metals weld joints showed that the carbon steel surfaces only corroded. The weight loss rate due to corrosion increased up to 100hours but it decreased above 100 hours. There was little difference in the weight loss caused by corrosion regardless of heat inputs.

• 한국주조공학회지
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• 제19권1호
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• pp.84-90
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• 1999

In this study, CV cast iron was reverse transformed to produce harder second phase surrounding graphite nodules, and then the microstructure and related mechanical properties of the reverse transformed CV cast iron were investigated by using optical microscopy and by carrying out hardness, tension and impact test. The formation of hard second phase surrounding graphite nodules increased the hardness in CV cast iron. The marked increase in hardness was resulted from the formation of martensite surrounding graphite nodule. It is expected from these results that the formation of martensite surrounding graphite nodule would improve the wear resistance of CV cast iron. The formation of both martensite and pearlite surrounding graphite nodule improved the tensile properties. Impact properties were decreased with increasing the volume fraction of hard second phase. However, the reduced impact properties could be recovered through phase transformation of martensite into pearlite and sorbite by tempering.

• 연구논문집
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• 통권28호
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• pp.59-71
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• 1998

The ELID(electrolytic in-process dressing) grinding method is a new precision grinding technique with the special electrolytic in-process dressing by metal bonded grinding wheel, fluid, and power supply. It is possible to make a efficient precision machining of hard and brittle materials such as ceramics, hard metals, and quenched steels by using this method, In this study, a new efficient precision grinding method with ELID was attempted for application to the machining and finishing processes of cylindrical structural components. And, we try to develop the cylindrical grinding technique for mirror surface of ceramics, tungsten carbide and SCM steel, and for the high efficiency grinding of machined parts, for example, ball screw shaft. Electrical characteristics of three different wheel grit sizes of #325, #2000 and #4000 were investigated experimentally. ELID grinding method is proved to be useful for mirror surface generation and efficient machining.

• 한국생산제조학회지
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• 제18권5호
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• pp.498-506
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• 2009

An experimental study was performed to select cutting parameters for better quality-products in hard metals such as steels. Usually, a hard metal can be cut with a rotary cutting knife and the process provides a good cutting quality result. However, the cutting machine is much sensitive in cutting conditions because of its complicated mechanism. By this reason, careful processing conditions must be taken to improve the quality of the products. This experimental study for better quality products with a rotary cutting knife was carried out with two main factors; cutting speeds and cutting and pooling forces. A two-dimensional profile measuring instrument is used to evaluate its cutting faces and the effects of processing factors are analyzed by a commercial software.

• 한국분말재료학회지
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• 제10권4호
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• pp.249-254
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• 2003

WC-6wt%Co hard metal powders were sintered by a 2.45 GHz multimode microwave applicator in Ar atmosphere. Microwave sintering of WC-6wt%Co powder lowered the sintering temperature and shortened the processing time in less than two hours than by a conventional method. Microstructures of the sintered specimen were studied with scanning electron microscope (SEM) and no abnormal grain growth was observed. Mechanical properties were similar to the values of the specimens sintered by a conventional method. Specimen sintered at 135$0^{\circ}C$ for 30 minutes ,hewed 99%, 20.5 GPa and 8.1 MPa$\sqrt{m}$ of theoretical density, hardness and fracture strength, respectively.