• 제목/요약/키워드: Hard metals

검색결과 117건 처리시간 0.028초

표면처리가 어려운 금속재료의 EBSD 분석을 위한 시편 준비 (Sample Preparation for EBSD Analysis: Tips for Metals with Delicate Surfaces)

  • 강주희;김수현
    • 대한금속재료학회지
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    • 제48권8호
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    • pp.730-740
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    • 2010
  • Aluminum, magnesium, titanium and high Mn steel are difficult to use in electron backscatter diffraction (EBSD) sample preparation due to the formation of an oxidation layer under conventional polishing. Alcohol-based polishing with colloidal silica suspension was introduced for these delicate samples. A hard particle-embedded sample was analyzed successfully using mechanical polishing. Ion-milling was effective in removing oxidized, deformed and transformed layers after mechanical polishing and was able to reduce artifacts significantly. The microstructure of a cross-section of a thin copper film was evaluated by attachment of a dummy to the film for mechanical polishing.

High Velocity Compaction : Overview of Materials, Applications and Potential

  • Dore, Florence;Lazzarotto, Ludovic;Bourdin, Stephane
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.20-21
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    • 2006
  • Through different projects, CETIM and its scientific and industrial partners have evaluated the potential of the High Velocityy Compaction Technology in terms of materials and component shape. Various kinds of powder materials were studied: metals, ceramics and polymers. The HVC process was used with success to manufacture gears, large parts and multilevel components. Due to the high density of HVC parts, the green machining process enables shapes to be produced that would otherwise be impossible to compact and components to be produced with very hard sintered and homogeneous materials.

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펄스 전류 활성 소결법을 이용한 WC-Mo2C-Co 소결체 제조 및 기계적 특성 평가 (Fabrication and Mechanical Properties of WC-Mo2C-Co Hard Materials by the Pulsed Current Activated Sintering Method)

  • 윤희준;방한서;방희선;오익현;박현국
    • 대한금속재료학회지
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    • 제50권12호
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    • pp.921-929
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    • 2012
  • The pulsed current activated sintering method (PCAS) is a new rapid sintering method that was developed recently for fabricating ceramics and composites. This method combines a high temperature for a short time with pressure application. In this work, PCAS was used to fabricate $WC-5wt%Mo_2C-5wt%$ Co hard material using WC, $Mo_2C$, and Co. The $WC-Mo_2C-Co$ was almost completely dense with a relative density of up to 100% after the simultaneous application of a pressure of 60 MPa and electric current for 11 min without grain growth. The average grain size of WC that was produced through PCAS was about $0.5-0.6{\mu}m$. The vickers hardness and fracture toughness of the $WC-5wt%Mo_2C-5wt%$Co hard materials were about $2453.5kg/mm^2$ and $7.9MPa{\cdot}m^{1/2}$, respectively, for 60 MPa at $11200^{\circ}C$.

물의 경도가 흰쥐의 신장, 간에서 중금속 축적에 미치는 영향 (Influence of Water Hardness on Accumulation of Heavy Metals in Kidneys and Livers of Rats)

  • 한돈희
    • 한국환경보건학회지
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    • 제14권2호
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    • pp.51-64
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    • 1988
  • It has been suggested that calcium is only one of many metals that compete with toxic metals in the body. Therefore, this study was carried out to determine the influence of water hardness on accumulation of heavy metals in rats. The seventy-five rats were divided into control and case groups. Case group was subdivided into four subgroups in proportion to the concentration of water hardness respectively, such as, 0, 250, 500, 1000ppm. Control group was fed on only deionized water, but case groups were fed on hard water with ionized heavy metals (Cd 150mg + Pb 300mg + Cu 300mg/l) for 20, 40, 60 days. The concentrations of cadmium, lead and copper were measured by atomic absorption spectrophotometry (Perkin Elmer 2380) in livers and kidneys. The results of the study are summarized as following 1. The concentration of cadmium accumulation showed the tendency of decrease in proportion to water hardness in both livers and kidneys of rats having been fed for only 60 days, respectively. 2. In only livers of rats having been fed for 60 days, essential metal, copper had the tendency of decrease according as hardness in water. 3. It was impossible to compare case with control about the tendency of lead accumulation because there was no difference between the two in livers and kidneys respectively.

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유기 벤토나이트에 의한 중금속 흡착특성 (Adsorption of Heavy Metals on Organobentonite)

  • 유지영;최재영;박재우
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2001년도 총회 및 춘계학술발표회
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    • pp.168-171
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    • 2001
  • Organobentonite modified with hexadecyltrimethylammonium (HDTMA) was used to quantify an adsorption of heavy metals. Based on preliminary experiments, optimal soil/solution ratio, a range of pH, and electrolyte were selected. Adsorption experiments of cadmium and lead were conducted to quantify an adsorption selectivity to bentonite and organobentonite. Adsorption of cadmium and lead to bentonite was increased with increasing a soil/solution ratio. Adsorption of cadmium and lead to bentonite was increased with increasing a soil/solution ratio. Adsorptions of heavy metal to organobentonite were slightly reduced relative to bentonite. This study used the principle of hard-soft-acid-base (HBAB) to interpretate an adsorption mechanism. Because of competition between cadmium and lead. adsorption of cadmium and lead was reduced in mixture of heavy metals. Adsorption selectivity.

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Hard, Wear Resistant Metal Surfaces for Industrial Applications through Laser Powder Deposition

  • Sears, James;Costello, Aaron
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.293-294
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    • 2006
  • Laser Powder Deposition (LPD) is a technology capable of modifying a metallic structure by adding the appropriate material to perform a desired function. LPD offers a unique fabrication technique that allows the use of soft (tough) materials as base structures. Through LPD a hard material can be applied to the base material with little thermal input (minimal dilution and heat-affected-zone {HAZ}), thus providing the function of a heat treatment or other surface modifications. These surface modifications have been evaluated through standard wear testing (ASTM G-65), surface hardness (Rc), micro-hardness (vickers), and optical microscopy.

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WC-Co 초경합금의 액상소결시 WC 입자형상에 미치는 탄소량의 영향 (Effect of Carbon Content on the Shape of WC Grains during Liquid Phase Sintering of WC-Co Hard Metals)

  • 한석희;박종구;허무영
    • 한국분말재료학회지
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    • 제6권4호
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    • pp.307-313
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    • 1999
  • The effect of carbon content on the shape of WC grains dispersed in the Co-rich matrix during liquid phase sintering of WC-35%Co hard metals has been determined. The shape of WC grains was observed using SEM stereography after removing cobalt matrix with boiling hydrochloric acid solution. The WC grains changed from hexagonal to trigonal prism as the carbon content increased in the two-phase region of(WC + $\beta$ - Co), while the morphology of WC grains changed from trigonal to hexagonal shape as the carbon content decreased. The morphology of WC grains changes reversibly along with carbon loss or carbon pick-up. Morphology change of WC grains is attributed to crystal structure of WC, which has an asymmetric array of carbon atoms. There are two types of prismatic planes having different numbers of broken W-C bonds in WC grains. It is scrutinized that as the carbon content increases, the high energy prism planes grow fast and the crystals change from hexagonal to trigonal shape. On the other hand, when the carbon content decreases, the high energy prism planes are dissolved accompanying split of (100) plane into (101) and (101) planes.

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유기 벤토나이트에 의한 카드뮴과 납의 흡착특성 (Adsorption of Cadmium and Lead on Organobentonite)

  • 유지영;최재영;박재우
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제6권3호
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    • pp.21-29
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    • 2001
  • 양이온성 계면활성제인 HDTMA를 이용하여 치환시킨 유기 벤토나이트의 중금속 흡착능을 알아보았다. 카드뮴과 납의 흡착량은 pH와 흡착제 대 용액 비가 증가함에 따라 증가하였다. 이 실험을 통해 적정 pH 범위와 흡착제 대 용액 비를 결정하였다. 유기 벤토나이로의 중금속 흡착은 벤토나이트에 비해 약간 감소하였으며, 두 가지 중금속이 함께 존재하는 경우 경쟁에 의해 흡착량은 더 감소하였다. 유기 벤토나이트의 경우 카드뮴에 비해 납의 흡착 감소량은 더 두드러지게 나타났다. 이러한 흡착 mechanism을 hard-soft-acid-base (HSAB) 원리를 사용하여 설명하였다.

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