• Title/Summary/Keyword: HV%

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Effect of Heat Treatment Environment on the Densification of Cold Sprayed Ti Coating Layer (저온 분사 공정으로 제조된 티타늄 코팅층의 치밀화에 미치는 열처리 분위기의 영향)

  • Yu, Ji-Sang;Kim, Hyung-Jun;Oh, Ik-Hyun;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.19 no.2
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    • pp.110-116
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    • 2012
  • This study investigated the effects of annealing environment for the densification and purification properties of pure titanium coating layer manufactured by cold spraying. The annealing was conducted at $600^{\circ}C$/1 h and three kinds of environments of vacuum, Ar gas, and $5%H_2+Ar$ mixture gas were controlled. Cold sprayed Ti coating layer (as sprayed) represented 6.7% of porosity and 228 HV of hardness, showing elongated particle shapes (severe plastic deformation) perpendicular to injection direction. Regardless of gas environments, all thermally heat treated coating layers consisted of pure ${\alpha}$-Ti and minimal oxide. Vacuum environment during heat treatment represented superior densification properties (3.8% porosity, 156.7 HV) to those of Ar gas (5.3%, 144.5 HV) and $5%H_2+Ar$ mixture gas (5.5%, 153.1 HV). From the results of phase analysis (XRD, EPMA, SEM, EDS), it was found that the vacuum environment during heat treatment could be effective for reducing oxide contents (purification) in the Ti coating layer. The characteristic of microstructural evolution with heat treatment was found to be different at three different gas environments. The controlling method for improving densification and purification in the cold sprayed Ti coating material was also discussed.

Estimation of Secondary PM10 Concentrations and Their Diurnal Variations Using Air Quality Monitoring Data in Seoul (지상 대기질 측정 자료를 이용한 서울 지역 2차 미세먼지 생성량 및 그 일변화 추정)

  • Kim, Ji-A;Jin, Hyung-Ah;Kim, Cheol-Hee
    • Journal of Korean Society for Atmospheric Environment
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    • v.24 no.4
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    • pp.393-403
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    • 2008
  • In an effort to estimate secondary $PM_{10}$ concentrations and their diurnal variations at different photochemical activities, $PM_{10}$, CO, and $O_3$ concentrations obtained from the ambient air quality network located in Seoul are analyzed for the period from 2000 to 2005. In order to classify the photochemical activities on a daily basis, measured ${\Delta}O_{3,\;max-min}$ (maximum $O_3$-minimum $O_3$) and ${\int}(hv)dt$ which represents accumulated daily insolation, were used to classify each day into three regimes: 1) low photochemical reactivity; ${\Delta}O_{3,\;max-min}\;{\leq}\;40\;ppb$, and ${\int}(hv)dt\;{\leq}\;4000\;W/m^2$, 2) moderate photochemical reactivity; $40\;ppb\;<\;{\Delta}O_{3,\;max-min}\;{\leq}\;60\;ppb$, and $4000\;{\leq}\;{\int}(hv)de\;{\leq}\;6000\;W/m^2$, and 3) high photochemical reactivity; ${\Delta}O_{3,\;max-min}\;>\;60\;ppb$, and ${\int}(hv)dt\;{\geq}\;6000\;W/m^2$. The ratio of ($PM_{10}$/CO) obtained at low photochemical activity regime was used as an index of tracer for the estimation of secondary $PM_{10}$ at higher photochemical activity regimes. The results show that the estimated secondary $PM_{10}$ concentrations for moderate and high photochemical regimes are found to be 18.8% ($10.9\;{\mu}g/m^3$), and 35.0% ($26.2\;{\mu}g/m^3$), respectively. Diurnal variation of secondary $PM_{10}$ for the moderate photochemical regime shows weak but noticeable patterns. However, the highly activated photochemical regime shows strong diurnal variations of secondary $PM_{10}$ concentrations with the maximum value of $35.1\;{\mu}g/m^3$ at 1300LST.

Preparation of Biodegradable PHBV Devices Containing Gentamicin Sulfate (PHBV를 이용한 황산겐타마이신 서방성 제형의 제조와 방출거동)

  • 최학수;김상욱;윤덕일;강길선;이종문;김용식;이해방
    • Polymer(Korea)
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    • v.25 no.3
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    • pp.334-342
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    • 2001
  • Gentamicin sulfate (GS)-loaded poly(3-hydroxybutyrate-co-3-hydroxyvalerate)(PHBV) devices were prepared for controlled-release of antibiotics. In this study, the effects of thickness, hydroxyvalerate (HV) content, initial drug-loading ratio, and additive content on the release profile have been investigated. The morphology of devices was examined with scanning electron microscope (SEM) before and after in vitro release; their highly porous surface and cross-sectional were observed. It could be suggested that device would be affected by the packing of the HV and additive content, which would depend on their structure. A high performance liquid chromatography (HPLC) was used to detect and quantify the release of GS from the device. The drug release from all the devices showed biphasic release patterns, and some matrices released the incorporated antibiotic throughout 30 days with a near zero-order release rate. The release patterns were shown to be changed by altering the thickness, copolymer ratio, and additive content.

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Changes in the Cross-Sectional Area of the Abductor Hallucis During the Toe-Spread-Out Exercise at Different Ankle Positions (다양한 발목각도에 따른 발가락벌리기 운동이 엄지벌림근 단면적에 미치는 영향)

  • Kang, Seong-Tae;Kang, Sun-Young;Kim, Ki-Song;Jeon, In-Cheol;Choung, Sung-Dae
    • Journal of the Korean Society of Physical Medicine
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    • v.15 no.2
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    • pp.121-128
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    • 2020
  • PURPOSE: This study examined the changes in the cross-sectional area (CSA) of the abductor hallucis muscle during various ankle positions while performing toespread-out (TSO) exercise. METHODS: Thirty subjects with an average age of 22.1 years were recruited for this study. All subjects were firstly measured for the angle of their first metatarsophalangeal joint using a goniometer. Those with angles greater than 15° were allocated to the HV group. The remaining subjects were placed in the normal group. The CSA of the abductor hallucis was measured by ultrasound in the resting position with no movement and three ankle positions: neutral (0°), plantarflexion (30°), and dorsiflexion (30°). All data were analyzed using a two-way mixed analysis of variance between the groups (normal and HV group) and within the groups (resting, neutral, plantarflexion, and dorsiflexion) to determine the group x position interaction effects. RESULTS: During TSO exercise in the normal group, the CSA of the abductor hallucis was significantly greater in both the plantarflexion and neutral positions compared to the resting position (padj < .01), and plantarflexion was significantly greater than the dorsiflexion position (padj < .01). During the TSO exercise in the HV group, the CSA of the abductor hallucis for plantarflexion was significantly greater than it was for the resting, neutral, and dorsiflexion positions (padj < .01). CONCLUSION: Based on the above results, the TSO exercise in plantarflexion is an effective rehabilitation exercise for subjects with HV.

Electron beam weldability of titanium alloy (타이타늄합금의 전자빔용접성)

  • Lee, Chae-Hun;Yun, Jong-Won;Park, No-Gwang
    • Laser Solutions
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    • v.10 no.4
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    • pp.13-17
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    • 2007
  • Electron beam weldability was investigated for 1mm thick cold rolled sheets of commercially pure grade titanium and Ti-6Al-4V alloy. Accelerating voltage of 40kV, beam current of 6mA, and weld speed of 0.8m/min was used and focal position of focused electron beam was just on the surface of workpiece. Microstructure of weld metal, the heat affected zone and base metal was observed using optical microscope. Vickers hardness was measured across the welds and the transverse tensile test was carried out. Hydroformability test was also carried out for the butt welded coupons of commercially pure grade titanium. For the electron beam welded C P Ti, the average grain size was equiaxed $\alpha(15{\sim}25{\mu}m)$ for base metal, coarse equiaxed $\alpha(80{\sim}200{\mu}m)$ for weld metal and annealed and enlarged grain($40{\sim}120{\mu}m$) for the HAZ. The vickers hardness of C P Ti was $180{\sim}200Hv$ for base metal, and $160{\sim}180Hv$ for the weld metal and the HAZ. For the electron beam welded Ti-6Al-4V alloy, the vickers hardness was 360Hv for the base metal, abd $400{\sim}425Hv$ for the weld metal and the HAZ. All the failure occurred at the base metal, when the transverse weld tensile test was carried out for both electron beam welded C P Ti and Ti-6Al-4V alloy. The formability of electron beam welded C P Ti was decreased compared with that of C P Ti base alloy.

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Hardening Characteristics of Aluminum Alloy Surface by PTA Overlaying with Metal Powders (II) -Hardening charactersteristics and wear resistance of thicker surface alloyed layer- (플라즈마분체 오버레이법에 의한 알루미늄합금 표면의 경화특성에 관한 연구( II ) -후막 표면 합금화층의 경화특성과 내마모성-)

  • ;中田一博;;;松田福久
    • Journal of Welding and Joining
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    • v.12 no.4
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    • pp.102-109
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    • 1994
  • The thick and hard alloyed layer was formed on the surface of Aluminum Cast Alloy(AC2B) by PTA overlaying process with Cr, Cu and Ni metal powders under the condition of overlaying current 150A, overlaying speed 150mm/min and different powder feeding rate 5-20g/min. The characteristics of hardening and were resistance of alloyed layer have been investigated in relation to microstructure of alloyed layer. As a result, it was made clear that Cu powder was the most superier one in three metal powders used due to an uniform hardness distribution of Hv 250-350, good wear resistance and freedom from cracking in alloyed layer of which microstructure consisted of hypereutectic. On the contrary, irregular hardness distribution was usually obtained in Cr or Ni alloyed layers of which hardness was increased as Cr or Ni contents and reached to maximum hardness of about Hv 400-850 at about 60wt% Cr or 40wt% Ni in alloyed layer. However the cracking occurred in these alloyed layers with higher hardness than Hv 250-300 at more than 20-25wt% of Cr or Ni contents in alloyed layer. Wear rate of alloyed layer was decreased to 1/10 in Cu alloyed layer and 1/5 or 1/3 in Cr or Ni alloyed layer with same hardness of about Hv 300 in comparison with that of base metal at higher sliding speed.

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A Study on the high Temperature Properties of the Graded Thermal Barrier Coatings by APS and PAS (APS법으로 제조된 열장벽 피막과 PAS법으로 제조된 열장벽 성형체의 고온 물성에 관한 연구)

  • 강현욱;권현옥;한주철;송요승;홍상희;허성강;김선화
    • Journal of the Korean institute of surface engineering
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    • v.32 no.2
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    • pp.144-156
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    • 1999
  • Thermal Barrier Coating with Functional Gradient Materials (FGM-TBC) can play an important role to protect the parts from harmful environments in high temperatures such as oxidation, corrosion, and wear and to improve the efficiency of aircraft engine by lowering the surface temperature on turbine blade. FGM-TBC can increase the life spans of product and improve the operating properties. Therfore, in this study the evaluations of mechanical and thermal properties of FGM-TBC such as fatigue, oxidation and wear-resistance at high temperatures have been conducted. The samples of both the TBC with 2, 3, 5 layers (YSZ/NiCrAlY) to be produced by Air Plasma Spray method (APS) and the bulk TBC with 6 layers to be produced by Plasma Assisted Sintering method (PAS) were used. Furthermore, residual stress, bond strength, and thermal conductivity were evaluated. The average thickness of the APS was 500$\mu\textrm{m}$ to 600$\mu\textrm{m}$ and the average thickness of the PAS was 3mm. The hardness number of the top layer of APS was 750 Hv to 810Hv and that of PAS was 950 Hv to 1440Hv. The $ZrO_2$ coating layer of APS was composed of tetragonal structure after spraying as the result of XRD analysis. As shown in the results of the high temperature wear test, the 3 layer coating of APS had the best wear resistance at $800^{\circ}C$ and the 5 layer coating of APS had the best wear resistance at $600^{\circ}C$. But, these coatings had the tendency of the low-temperature softening at $300^{\circ}C$. The main mechanism of wear was the adhesive wear and the friction coefficient of coatings was increased as increasing the test temperatures. A s results of thermal conductivity test, the ${\Delta}T$ of the APS coating was increased as number of layer and the range of thermal conductivity of the PAS was $800^{\circ}C$ to $1000^{\circ}C$.

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A Study on the Comparison of hardness, Strength and Microstructure of dental Non-precious Metal Alloys Colored Goldish Yeller (Goldish Yellow Color인 수종(數種)의 치과용(齒科用) 비귀금속합금(非貴金屬合金) 경도(硬度), 강도(强度) 및 미세조직(微細組織)의 비교(比較)에 관(關)한 연구(硏究))

  • Kim, Jae-Do
    • Journal of Technologic Dentistry
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    • v.14 no.1
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    • pp.55-65
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    • 1992
  • The purpose of this study was to investigate the comparison of physical properties of nonprecious metal alloys colored goldish yellow. The experimental groups were copper based dental alloy and control group was Ni-Cr based dental alloy used crown and bridges frameworks. Hardness was tested by vickers hardness tester, tensile strength was tested by universal tension tester. After testing the tensile strength of castings, the microstrucure and the pattern of fracture were investigated by scanning electron microscope and metallurgical microscope. The results were as follows : Hardness of Ni based alloy was higher than Cu based alloys. Hardness number of A group was 200.41$\pm$16.10 Hv, B group was 194.33$\pm$1.69 Hv, C group was 139.29$\pm$2.19 Hv and D group was 293.81$\pm$27.17 Hv, respectively. Tensile strength of D group was 56.42$\pm$6.17 $kg/m^2$, A group was 50.39$\pm$5.68 $kg/m^2$, C group was 45.13$\pm$4.53 $kg/m^2$, B group was 45.25$\pm$9.25 $kg/m^2$, in order, and D group was maximum tensile strength. The fractured surfaces of tensile specimens in the all groups showed the tendency to form large voids in the center of specimens. Thus the ductile fracture was changed into the brittle fracture with the fine grain size.

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Evaluation on Soil Characterization in Paddy Treated with Different Green Manure Crops and Tillage Method by Ordination Technique

  • Kim, Kwang Seop;Park, Ki Do;Kim, Suk-Jin;Choi, Jong-Seo;Lee, Yong Bok;Kim, Min-Tae
    • Korean Journal of Soil Science and Fertilizer
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    • v.48 no.4
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    • pp.285-294
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    • 2015
  • Ordination has been recognized useful method to analyze the effects of multiple environmental factors on dozens of species in vegetation ecology because of summarizing community data by producing a low-dimensional graphics. Main objective of this study was the application of ordination method, especially principal components analysis (PCA), to analyze the soil characterization on paddy treated by different green manure crops and tillage methods. Treatments included the three tillage treatments and two green manure crops as the following; (i) moldrotary + rotary tillage without green manure crop (Con), with (ii) hairy vetch (ConHv), and (iii) hairy vetch + green barely (ConHvGb), (iv) rotary tillage without green manure crop (Rot), with (v) hairy vetch (RotHv), and (vi) hairy vetch + green barly (RotHvGb), and (vii) no-tillage (Notill). Vectorial distance result from PCA of soil properties including physical, chemical, and microbial properties showed the two main difference. Firstly, soil properties among plots without green manure were strongly affected by tillage strength [Vectorial distance: Con-Notil (5.88) > Rot-Notill (4.58)] at PC1 (35.0%) axis. But it was difficult to find the fixed trend among plots when green manure crop was added in plot. Nevertheless, two groups were separated by adding green manure crop at PC2 (29.2%) axis. These results show that PCA ordination methods could be used the research for change of soil characterization.

Reflection Symmetry of PALSAR Quad-Pol Imagery in the Amazon Rainforest (아마존 지역 PALSAR 다중편파 자료의 반사대칭성 특성)

  • Kim, Jae-Hun;Yoon, Sun Yong;Won, Joong-Sun
    • Korean Journal of Remote Sensing
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    • v.34 no.6_1
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    • pp.969-979
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    • 2018
  • This paper presents reflection symmetry of polarimetric SAR over the Amazon rainforest in terms of correlation coefficients between the pairs of HH- and HV-pol and VV- and VH-pol data by ALOS PALSAR. The reflection symmetry is defined as a non-zero correlation between HH- and HV-pol and VV- and VH-pol over natural distributed targets, and is a fundamental assumption for cross-talk calibration coefficient computation and for three-component decomposition for polarimetric SAR data. The Amazon rainforest is especially one of the common global reference sites for the reflection symmetry. The correlation coefficients for the pairs of reflection symmetry obtained in this study range from 0.018 to 0.097. The results imply that there exists a non-negligible dependency between co-pol and cross-pol in the distributed natural targets, and consequently the non-zero correlation must be considered as a potential contribution to errors of spaceborne SAR polarimetry to some extent.