• 한국재료학회지
• /
• 제24권11호
• /
• pp.591-598
• /
• 2014

In this research, magnesium powder was prepared by gas atomizing. Refinement behaviors of magnesium powder produced under different conditions were investigated using a mechanical milling (attrition milling) process. Analyses were performed to assess the characterization and comparison of milled powder with different steel ball sizes and milling times. The powders were analyzed by field emission scanning electron microscope, apparent density and powder fluidity. The particle morphology of the Mg powders changed from spherical particles of feed metals to irregular oval particles, then plate type particles, with an increasing milling time. Because of the HCP structure, deformation occurs due to the existence of the easily breakable C-axis perpendicular to the base, which results in producing plate-type powders. An increase in ball size and the impact energy of the magnesium powder maximizes the effect of refinement. Furthermore, it is possible to improve the apparent density and fluidity according to the smoothness of the surface of the initial powder.

• 한국진공학회:학술대회논문집
• /
• 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
• /
• pp.222.2-222.2
• /
• 2015

A $Ge_2Sb_2Te_5$ nanowire (GST NW) phase change memory device is investigated with Joule heating electrodes. GST is the most promising phase change materials, thus has been studied for decades but atomic structure transition in the phase-change area of single crystalline phase-change material has not been clearly investigated. We fabricated a phase change memory (PCM) device consisting of GST NWs connected with WN electrodes. The GST NW has switching performance with the reset/set resistance ratio above $10^3$. We directly observed the changes in atomic structure between the ordered hexagonal close packed (HCP) structure and disordered amorphous phase of a reset-stop GST NW with cross-sectional STEM analysis. Amorphous areas are detected at the center of NW and side areas adjacent to heating electrodes. Direct imaging of phase change area verified the atomic structure transition from the migration and disordering of Ge and Sb atoms. Even with the repeated phase transitions, periodic arrangement of Te atoms is not significantly changed, thus acting as a template for recrystallization. This result provides a novel understanding on the phase-change mechanism in single crystalline phase-change materials.

• 열처리공학회지
• /
• 제21권5호
• /
• pp.235-243
• /
• 2008

Ni-C composite films were prepared using a combination of microwave plasma CVD and ion beam sputtering deposition working in a codeposition way. The structure of these films was characterized by energy-dispersive X-ray diffraction (EDXRD), transmission electron microscopy (TEM) and Raman spectroscopy. It was found that a nickel carbide phase, $Ni_3C$ (hcp), formed as very fine crystallites over a wide temperature range when Ni-C films were deposited at low $CH_4$ flow rates. The thermal stability of this nonequilibrium carbide $Ni_3C$ was also studied. As a result, the $Ni_3C$ carbide was found to decompose into nickel and graphite at around $400^{\circ}C$. With high $CH_4$ flow rates (> 0.2 sccm), the structure of the Ni-C films became amorphous. The formation behavior of the carbide and amorphous Ni-C phases are discussed in relation to the electrical resistivity of the films.

• 한국콘텐츠학회:학술대회논문집
• /
• 한국콘텐츠학회 2007년도 추계 종합학술대회 논문집
• /
• pp.153-159
• /
• 2007

미래 유망연구 및 기술과제의 선정을 위한 방법론의 개발과 이를 통한 구체적인 아이템 선정을 위한 연구가 추진되고 있다. 본 논문은 과학기술연구분야의 미래 유망분야를 선정하기 위한 조사로 과학계량학이라는 객관적인 지표를 이용한다. 스커퍼스(Scopus)라는 과학기술정보 데이터베이스를 이용하여 건설교통분야의 고인용 및 클러스터링 정보분석을 수행한다. 정보분석을 통하여 각 국가간의 기술동향을 비교하고, 건설교통분야의 유망연구 영역을 선정하였다.

• 한국주조공학회지
• /
• 제30권2호
• /
• pp.76-82
• /
• 2010

Effect of reaction time and sludge formation on the thickness of die soldering reaction layer has been studied in Al-9Si-0.3Mg casting alloy. Ternary ${\alpha}_{bcc}-Al_8Fe_2Si$ and ${\alpha}_{hcp}-Al_8Fe_2Si$ intermetallic compounds formed at the interface of SKD61 tool steel by interaction diffusion of Al, Fe and Si atoms after 0.5hr and 6hr immersion time, respectively. Binary ${\eta}-Fe_2Al_5$ additionally formed at the interface of SKD61 tool steel after 10hr immersion time. Thickness of soldering reaction layer in die surface increased as immersion time increased from 0.5hr to 24hr. Sludge formation was ascertained in the samples which were immersed in the melts more than 10hr. Reaction of die soldering after sludge formation was more accelerated than that of before sludge formation due to a decrease in Fe content, followed by higher diffusion rate of Al in the melt by sludge formation.

• Journal of Nutrition and Health
• /
• 제39권5호
• /
• pp.444-450
• /
• 2006

In this study, we investigated antimicrobial and cytotoxicity effects to each· fraction extracted from Hizikiafusifonnis (HF), which were extracted methanol (HFM) and then the extract was fractionated into four different types: hexane (HFMH) , methanol (HFMM) , bulanol (HFMB) and aquous (HFMA) partition layers. We determined the cytotoxic effect of these layers on human cancer cells by MIT assay. Among various partition layers of HF, the HFMB and HFMM were showed the strong cytotoxic effects on cancer cell lines we used. The quinone reductase (QR) induced activity of the HFMB on HcpG2 cells at $150\;{\mu}g/mL$ concentration was 2.63 times more effective compared to the control value of 1.0. Although further studies are needed, the present work suggests that HF maybe a chemopreventive agent for the treatment of human cancer cells.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2006년도 추계학술대회 논문집 Vol.19
• /
• pp.201-201
• /
• 2006

영구자석은 크게 Hard ferrite와 희토류계 자석, 그리고 Alnico 주조자석으로 구별되어진다. 그동안 Hard ferrite는 산업적으로 전자기 응용제품 또는 각종 구동 모터에 응용되어 왔지만, 최근 Nd계 희토류 자것이 고성능 모터의 소재로 급격히 대체되고 있다. 하지만, 희토류계 원료에 비해 동일 중량 대비 40~60배 가량 저렴한 Hard ferrite의 사용은 현재까지도 꾸준히 유지되고 있으며, 최근 자동차 고성능 모터용 Sr ferrite의 개발이 연구 중이다.[2] 본 연구에서는 제일원리 전산모사를 통하여 HCP 구조의 기본 Unit Cell 64개 원자를 가진 Sr-ferrite의 격자상수를 계산하여 기존 연구결과와 비교하였으며, 자화에너지와 자기모멘트를 계산하였다. 또한 향후 각종 첨가물의 영향에 대한 연구를 위해 기본 구조 및 치환 구조에 대해 고찰하였다. 그 결과 가장 안정한 에너지를 갖는 격자상수는 a=5.88, b=23.03으로 계산되어 Kimura et al의 측정 결과와 유사한 결과를 얻을 수 있었으며, $E_F$가 3.9171, $M_B$는 46.6481로 계산되었다. 항후 Sr-ferrite의 구조에서 Fe atom의 일부를 동일주기 원소인 Cr, Mn, Co, Ni, Cu로 치환하여 자기적 특성을 계산하여 본 연구결과와 비교하고자 한다.

• 소성∙가공
• /
• 제27권5호
• /
• pp.301-313
• /
• 2018

In this paper, tensile test was performed on pure titanium sheet (CP Ti sheet) with HCP structure in each direction to evaluate mechanical and surface properties and analyze microstructural changes during plastic deformation. We also evaluated forming limits of Ti direction in dome-type punch stretching test using a non-contact three-dimensional optical measurement system. As a result, it was revealed the pure titanium sheet has strong anisotropic property in yield stress, stress-strain curve and anisotropy coefficient according to direction. It was revealed that twinning occurred when the pure titanium sheet was plastic deformed, and tendency depends differently on direction and deformation mode. Moreover, this seems to affect the physical properties and deformation of the material. In addition, it was revealed the pure titanium sheet had different surface roughness changes in 0 degree direction and 90 degree direction due to large difference of anisotropy, and this affects the forming limit. It was revealed the forming limit of each direction obtained through the punch stretching test gave higher value in 90 degree direction compared with forming limit in 0 degree direction.

• 소성∙가공
• /
• 제23권8호
• /
• pp.495-500
• /
• 2014

Magnesium alloys are currently expected to be widely used for weight reduction of cars and as high efficient materials in the automotive and electronics industries. Although the specific strength of magnesium is excellent, it cannot be easily formed at room temperature due to its HCP structure. However in order to improve the formability of magnesium, it is necessary to investigate its formability in the warm temperature range. In the current study, the aim was to add to the magnesium property database so that the mass production of a magnesium car body can be accomplished. Warm tensile tests were conducted and the forming limit diagram was determined to confirm formability characteristics of magnesium AZ31B alloy sheet. In addition the bending formability and the magnesium damping capacity were evaluated for AZ31B and compared to SPRC440E which is a sheet steel used for car bodies.

• 동력기계공학회지
• /
• 제5권2호
• /
• pp.63-70
• /
• 2001

To obtain the optimal condition of heat treatment of wear-resistant alloy, hardness and Charpy V-notch test have been performed with Co-based Stellite No.4, No.6 and Tribaloy 800 alloys, following by heat treatment at the various conditions. Heat treatment at $1250^{\circ}C$ for 1 hours caused the as-casted Tribaloy 800 with FCC crystal structure to transform to HCP structure and lamellar eutectic structure was disappeared, which did not influence on the hardness. Aging at $800^{\circ}C$ for 20 hours, following by $1250^{\circ}C$ for 2 hours heat treatment has enhanced hardness significantly, which is due to the precipitation of large amounts of Laves-phase. The hardness of Stellite alloys was increased by the aging at $800^{\circ}C$ to 5 hours, and was nearly constant by the aging over 5 hours. The toughness of Stellite alloys was a few influenced by the aging treatment.