• Title/Summary/Keyword: Grain Structure

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Changes in Amylopectin Structure and Pasting Properties of Starch as Affected by Different Transplanting Dates in Rice

  • Kim, Sang-Kuk;Shin, Jong-Hee;Ahn, Deuk-Jong;Kim, Se-Jong
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.61 no.4
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    • pp.235-241
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    • 2016
  • Three different transplanting dates for two rice cultivars grown in Daegu, Republic of Korea, were examined to identify the changes in growth, rice quality, and characteristics of amylopectin. An early transplanting date caused a reduction in the number of panicles in both rice cultivars compared to that in the optimal and late transplanting dates. The 1000-grain weight in the two rice cultivars was significantly increased in the late transplanting date. The rice cultivar tolerant to high temperatures, Donganbyeo, exhibited the lowest milky grain rate in the late transplanting date. The highest rate of head grain was observed in the late transplanting date in both rice cultivars. Regarding the pattern of pasting properties, peak viscosity increased with delayed transplanting dates. With respect to changes in the amylopectin branch-chain length distribution, the amylopectin structure of the translucent Dongan rice cultivar transplanted on April 25 was characterized by a significant increase in A chains with DP > 12, and a decrease in long chains $DP{\geq}37$ compared to that transplanted on June 25. In contrast, the amylopectin structure of the chalky Dongan rice cultivar transplanted on April 25 exhibited further decrease in 13 < DP < 19 than that transplanted on June 25. In the Ungwang rice cultivar, the amylopectin structure of the translucent Ungwang rice cultivar transplanted on April 25 and June 25 was characterized by a significant decrease in the lengths of total amylopectin chains. Furthermore, the amylopectin structure of the chalky Ungwangbyeo rice cultivar transplanted on April 25 was characterized by a significant increase in 7 < DP < 30, while a significant decrease was observed in that transplanted on June 25. These results indicate that the amylopectin structure is altered by different transplanting dates depending on the characteristics of the rice cultivar.

Stretch-Flangeability of Harmonic Structure Material Manufactured by Powder Metallurgy Method (분말야금법으로 제조한 하모닉 구조재료의 신장플랜지 가공성)

  • Yoon, Jae Ik;Lee, Hak Hyeon;Park, Hyung Keun;Ameyama, Kei;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.24 no.2
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    • pp.128-132
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    • 2017
  • Harmonic structure materials are materials with a core-shell structure having a shell with a small grain size and a core with a relatively large grain size. They are in the spotlight because their mechanical properties reportedly feature strength similar to that of a sintered powder with a fine grain size and elongation similar to that of a sintered powder with a coarse grain size at the same time. In this study, the tensile properties, microstructure, and stretch-flangeability of harmonic structure SUS304L made using powder metallurgy are investigated to check its suitability for automotive applications. The harmonic powders are made by mechanical milling and sintered using a spark plasma sintering method at 1173 K and a pressure of 50 MPa in a cylindrical die. The sintered powders of SUS304L having harmonic structure (harmonic SUS304L) exhibit excellent tensile properties compared with sintered powders of SUS304L having homogeneous microstructure. In addition, the harmonic SUS304L has excellent stretch-flangeability compared with commercial advanced high-strength steels (AHSSs) at a similar strength grade. Thus, the harmonic SUS304L is more suitable for automotive applications than conventional AHSSs because it exhibits both excellent tensile properties and stretch-flangeability.

The study of Grain boundary diffusion effect in Tin/Cu by Xps (XPS를 이용한 TiN/Cu의 Grain boundary diffusion 연구)

  • 임관용;이연승;정용덕;이경민;황정남;최범식;원정연;강희재
    • Journal of the Korean Vacuum Society
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    • v.7 no.2
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    • pp.112-117
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    • 1998
  • TiN has been investigated as a good candidate for a diffusion barrier of Cu. Therefore, in this study, the grain boundary diffusion of Cu in TiN film was investigated by X-ray photoelectron spectroscopy(XPS). In general, TiN has a columnar grain structure. In the relatively lower temperature, less than 1/3 of the melting point, it was observed that Cu diffused into TiN mainly along the grain boundaries of TiN. The grain size of TiN was measured by atomic force microscope (AFM). In order to estimate the grain boundary diffusion constants, we used the modified surface accumulation method. The activation energy, $Q_b$ was 0.23 eV, and the diffusivity, $D_{bo}$ was $5.5\times10^{-12{\textrm{cm}^2$/sec.

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A multiple level set method for modeling grain boundary evolution of polycrystalline materials

  • Zhang, Xinwei;Chen, Jiun-Shyan;Osher, Stanley
    • Interaction and multiscale mechanics
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    • v.1 no.2
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    • pp.191-209
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    • 2008
  • In this paper, we model grain boundary evolution based on a multiple level set method. Grain boundary migration under a curvature-induced driving force is considered and the level set method is employed to deal with the resulting topological changes of grain structures. The complexity of using a level set method for modeling grain structure evolution is due to its N-phase nature and the associated geometry compatibility constraint. We employ a multiple level set method with a predictor-multicorrectors approach to reduce the gaps in the triple junctions down to the grid resolution level. A ghost cell approach for imposing periodic boundary conditions is introduced without solving a constrained problem with a Lagrange multiplier method or a penalty method. Numerical results for both uniform and random grain structures evolution are presented and the results are compared with the solutions based on a front tracking approach (Chen and Kotta et al. 2004b).

Computer simulation study for the effect of potential energy on the behavior of grain boundary using Molecular dynamics

  • Choi, Dong-Youl;Kim, Hyun-Soo;Kim, Young-Suk;Tomita, Yoshihiro
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.03b
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    • pp.173-178
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    • 1999
  • In this study MD simulations have been performed to observe the behavior of a grain boundary in an a-Fe plate under 2-dimensional loading. In MD simulation the acceleration of every molecule can be achieved from the potential energy and the force interacting between each molecule and the integration of the motion equation by using Verlet method gives the displacement of each molecule. Initially four a-Fe rectangular plates having different misorientation angles of grain boundary were modeled by using the Johnson potential and Morse potential We compared the potential energy of the grain boundary system with that of the perfect structure model. Also we could obtain the width of the grain boundary by investigating the local potential energy distribution. The tensile loading for each grain boundary models was applied and the behavior of grin boundary was studied. From this study it was clarified that in the case using Johnson potential the obvious fracture mechanism occurs along the grain boundary in the case of Morse potential the diffusion of the grain boundary appears instead of the grain boundary fracture.

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Electrical Fire Identification due to Conductor Structure Analysis of Electrical Wires (전선의 도체조직 분석에 의한 전기화재 감식)

  • Park, O-Cheol;Kim, Wang-Kon;Park, Nam-Kyu;Hong, Jin-Woong
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.11a
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    • pp.615-618
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    • 2003
  • To investigate the electrical fire identification due to conductor structure analysis of an electrical wire, we are studied by temperature heating test, over current test, short test and electric molten marks. And metal structure analysis of wire by short, we are found out increase in crystal grain with heating temperature. Structure of specimen at over current 300[%] occurred hardly structure formation and boundary of grain.

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A Study on Poly-Si Solar Cell of Novel Structure with the Reduced Effects of Grain Boundaries (결정입계 영향을 줄인 새로운 구조의 다결정 실리콘 모양전지에 관한 연구)

  • Lim, Dong-Gun;Lee, Su-Eun;Park, Sung-Hyun;Yi, Jun-Sin
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1738-1740
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    • 1999
  • This paper deals with a novel structure of poly-Si solar cell. A solar cell conversion efficiency was degraded by grain boundary effect in Polycrystalline silicon. To reduce grain boundary effect, we performed a preferential grain boundary etching, $POCl_3$ n-type emitter doping, and then ITO film growth on poly-Si. Among the various preferential etchants, Schimmel etch solution exhibited the best result having grain boundary etch depth about $10{\mu}m$. RF magnetron sputter grown ITO films showed a low resistivity of $10^{-4}\Omega-cm$ and high transmittance of 85%. With well fabricated poly-Si solar cells. we were able to achieve as high as 15% conversion efficiency at the input power of 20mW/$cm^2$.

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Asymmetric Rolling as Means of Texture and Ridging Control and Grain Refinement (집합조직과 이랑형표면결함의 제어 및 결정립 미세화 수단으로서의 비대칭압연)

  • Lee D.N.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.08a
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    • pp.11-18
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    • 2004
  • Asymmetric rolling, in which the circumferential velocities of the upper and lower rolls are different, can give rise to intense plastic shear strains and in turn shear deformation textures through the sheet thickness. The ideal shear deformation texture of fcc metals can be approximated by the <111> // ND and $\{001\}<110>$ orientations, among which the former improves the deep drawability. The ideal shear deformation texture for bcc metals can be approximated by the Goss $\{110\}<001>\;and\;\{112\}<111>$ orientations, among which the former improves the magnetic permeability along the <100> directions and is the prime orientation in grain oriented silicon steels. The intense shear strains can result in the grain refinement and hence improve mechanical properties. Steel sheets, especially ferritic stainless steel sheets, and aluminum alloy sheets may exhibit an undesirable surface roughening known as ridging or roping, when elongated along RD and TD, respectively. The ridging or roping is caused by differently oriented colonies, which are resulted from the <100> oriented columnar structure in ingots or billets, especially for ferritic stainless steels, that is not easily destroyed by the conventional rolling. The breakdown of columnar structure and the grain refinement can be achieved by asymmetric rolling, resulting in a decrease in the ridging problem.

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Study on the Structure of Expanded Rice with Deep-Frying for Salyeotgangjung (유탕처리된 쌀엿강정용 팽화쌀의 조직학적 연구)

  • Kim, Myoung-Ae
    • Journal of the Korean Society of Food Culture
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    • v.16 no.4
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    • pp.323-329
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    • 2001
  • This study was carried out to observe the character change of expanded rice grain for Salyeotgangjung at various gelatinization methods. The expansion and structure change of rice grain was different at conditions of heating methods and gelatinization, respectively. The boiling showed good expansion compared to other heating methods by electric rice-cooker, pressure cooker, and steam cooker. There was not difference in expansion of rice grain between the boiling and the boiling after soaking. Rice grain did greatly expand as the boiling time was extended. But the quality for Salyeotgangjung would be not good because of crack of expanded rice grain surface when the boiling time was too long.

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Preparation and characterization of Zinc Oxide films deposition by (PVD) (PVD 코팅법에 의한 ZnO제조 및 특성)

  • Kim, Sung Jin;Pak, Hunkyun
    • 한국신재생에너지학회:학술대회논문집
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    • 2010.06a
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    • pp.95.1-95.1
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    • 2010
  • Transparent conducting ZnO films were deposited to apply DSSC Substrate on glass substrates at $500^{\circ}C$ by ionbeam-assisted deposition. Crystallinity, microstructure, surface roughness, chemical composition, electrical and optical properties of the films were investigated as a function of deposition parameters such as ion energy, and substrate temperature. The microstructure of the polycrystalline ZnO films on the glass substrate were closely related to the oxygen ion energy, arrival ratio of oxygen to Zinc Ion bombarded on the growing surface. The main effect of energetic ion bombardment on the growing surface of the film may be divided into two categories; 1) the enhancement of adatom mobility at low energetic ion bombardment and 2) the surface damage by radiation damage at high energetic ion bombardment. The domain structure was obtained in the films deposited at 300 eV. With increasing the ion energy to 600 eV, the domain structure was changed into the grain structure. In case of the low energy ion bombardment of 300 eV, the microstructure of the film was changed from the grain structure to the domain structure with increasing arrival ratio. At the high energy ion bombardment of 600 eV, however, the only grain structure was observed. The electrical properties of the deposited films were significantly related to the change of microstructure. The films with the domain structure had larger carrier concentration and mobility than those with the grain structure, because the grain boundary scattering was reduced in the large size domains compared with the small size grains. The optical transmittance of ZnO films was dependent on a surface roughness. The ZnO films with small surface roughness, represented high transmittance in the visible range because of a decreased light surface scattering. By varying the ion energy and arrival ratio, the resistivity and optical transmittance of the films were varied from $1.1{\times}10^{-4}$ to $2.3{\times}10^{-2}{\Omega}cm$ and from 80 to 87%, respectively. The ZnO film deposited at 300 eV, and substrate temperature of $500^{\circ}C$ had the resistivity of $1.1{\times}10^{-4}{\Omega}cm$ and optical transmittance of 85% in visible range. As a result of experiments, we provides a suggestition that ZnO thin Films can be effectively used as the DSSC substrate Materials.

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