• Journal of Welding and Joining
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• 제29권1호
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• pp.65-73
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• 2011

Microstructural characteristics of two high strength (600 MPa & 800 MPa) weld metals produced by flux-cored arc welding process (FCAW) were evaluated. The 600 MPa grade weld metal was consisted of 75% acicular ferrite and 25% ferrite which was formed at relatively high temperature (grain boundary ferrite, widmanstatten ferrite, polygonal ferrite). However, the 800 MPa grade weld metal was composed of about 85% acicular ferrite and 15% low temperature forming phases (bainite, martensite). The prior austenite grain size of 800 MPa grade weld metal was decreased by solute drag force. The compositions and sizes of inclusions which are the dominant factors for the formation of acicular ferrite were analyzed by a transmission electron microscopy (TEM). In both 600 MPa and 800MPa grade weld metals, the inclusions were mainly consisted of Ti-oxide and Mn-oxide, and the average size of inclusions was $0.7{\mu}m$. The 800 MPa grade weld metal exhibited higher tensile strength and similar toughness compared with the 600 MPa grade weld metal. This result is mainly due to a higher fraction of low temperature products and a lower fraction of grain boundary ferrite in the 800 MPa grade weld metal.

• Journal of Welding and Joining
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• 제30권1호
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• pp.64-71
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• 2012

The characteristics of high heat input (342kJ/cm) EG (Electro Gas Arc) welded joint of EH36-TM steel has been investigated. The weld metal microstructure consisted of fine acicular ferrite (AF), a little volume of polygonal ferrite (PF) and grain boundary ferrite (GBF). Charpy impact test results of the weld metal and heat affected zone (HAZ) met the requirement of classification rule (Min. 34J at $-20^{\circ}C$). In order to evaluate the relationship between the impact toughness property and the grain size of HAZ, the austenite grain size of HAZ was measured. The prior austenite grain size in Fusion line (F.L+0.1 mm) was about $350{\mu}m$. The grain size in F.L+1.5 mm was measured to be less than $30{\mu}m$ and this region was identified as being included in FGHAZ(Fine Grain HAZ). It is seen that as the austenite grain size decreases, the size of GBF, FSP (Ferrite Side Plate) become smaller and the impact toughness of HAZ increases. Therefore, the CGHAZ was considered to be area up to 1.3mm away from the fusion line. Results of TEM replica analysis for a welded joint implied that very small size ($0.8\sim1.2{\mu}m$) oxygen inclusions played a role of forming fine acicular ferrite in the weld metal. A large amount of (Ti, Mn, Al)xOy oxygen inclusions dispersed, and oxides density was measured to be 4,600-5,300 (ea/mm2). During the welding thermal cycle, the area near a fusion line was reheated to temperature exceeding $1400^{\circ}C$. However, the nitrides and carbides were not completely dissolved near the fusion line because of rapid heating and cooling rate. Instead, they might grow during the cooling process. TiC precipitates of about 50 ~ 100nm size dispersed near the fusion line.

• 한국안전학회지
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• 제18권3호
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• pp.46-53
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• 2003

For the tensile tests of the F.E.M., microvoids are created by the boundary separation process at the martensite boundary or neighborhood and at inclusions within the fracture. to grow to the ductile dimple fracture. For the case of the M.E.F., microvoids created at the discontinuities of the martensite phase which exists at the grain boundary of the primary ferrite are grown to coalescence with the cleavage cracks induced at the interior of the ferrite, which as a result show the discontinuous brittle fracture behavior. In spite of their similar tensile strengths, the fatigue limit and the notch sensitivity of the M. E.F. is superior to those of the F.E.M., The M.E.F. is much more insensitive to notch than F.E.M. from the stress concentration factor($\alpha$).

• 한국재료학회지
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• 제31권3호
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• pp.139-149
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• 2021

In this study, three kinds of bainitic steels are fabricated by controlling the contents of vanadium and boron. High vanadium steel has a lot of carbides and nitrides, and so, during the cooling process, acicular ferrite is well formed. Carbides and nitrides develop fine grains by inhibiting grain growth. As a result, the low temperature Charpy absorbed energy of high vanadium steel is higher than that of low vanadium steel. In boron added steel, boron segregates at the prior austenite grain boundary, so that acicular ferrite formation occurs well during the cooling process. However, the granular bainite packet size of the boron added steel is larger than that of high vanadium steel because boron cannot effectively suppress grain growth. Therefore, the low temperature Charpy absorbed energy of the boron added steel is lower than that of the low vanadium steel. HAZ (heat affected zone) microstructure formation affects not only vanadium and boron but also the prior austenite grain size. In the HAZ specimen having large prior austenite grain size, acicular ferrite is formed inside the austenite, and granular bainite, bainitic ferrite, and martensite are also formed in a complex, resulting in a mixed acicular ferrite region with a high volume fraction. On the other hand, in the HAZ specimen having small prior austenite grain size, the volume fraction of the mixed acicular ferrite region is low because granular bainite and bainitic ferrite are coarse due to the large number of prior austenite grain boundaries.

• 한국전기전자재료학회논문지
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• 제16권6호
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• pp.538-548
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• 2003

We studied effects by Re$_2$O$_3$(R=Dy, Gd, Ho) addition on the properties of Mn-Zn ferrite. The doping concentration range from 0.05 wt% to 0.25 wt%. All samples were prepared by standard fabrication of ceramics. With increasing the rare earth oxides, specific density and initial permeability increased on the whole. But, the tendencies such as upper result had the measured value on limitation and characteristics saturated or decreased properties after that. In case of excessive addition of additive beyond some level, initial permeability properties of ferrite have gone down in spite of anomalous grain. With increasing the content of additive, both the real and imaginary component of complex permeability and the magnetic loss (tan$\delta$) increased. Because the increased rate of real component had higher than imaginary component, magnetic loss increased none the less for increasing the real component related with magnetic permeability. But, the magnetic loss of ferrite doped with the rare earth oxides was lower than that of Mn-Zn ferrite at any rate. The small amount of present rare earth oxides in Mn-Zn ferrite composition led to enhancement of resistivity in bulk, and more so in the grain boundary. It was seem to be due to the formation of mutual reaction such as between iron ions and rare earth element ions.

• Journal of Welding and Joining
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• 제14권1호
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• pp.68-74
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• 1996

The microstructure of HAZ and the mechanical properties in weldments such as hardness and toughness were studied for mild steel and AH36 grade TMCP steel, as increasing heat input with electrogas welding process. The results of this study can be summarized as follow: 1) In the HAZ of mild steel, the width of coarse grained zone was larger than that of the nomalized zone, however in the case of TMCP steel, the nomalized zone was wider than the coarse grained zone. 2) The grain size of HAZ become coarse with increasing heat input. And at the same heat input, the grain size of TMCP steel was more coarser than that of mild steel. 3) According to the change of heat input, the deviation of hardness values was not significant, and the maximum values of hardness was not in HAZ but in the weld metal. And the hardness values in root part was higher than in face part. 4) Even though the HAZ grain size of mild steel was larger than that of TMCP steel, the impact values for mild steel was higher than those for TMCP steel, and the impact values in face part was higher than those in root part.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 추계학술대회 논문집
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• pp.154-157
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• 2007

The austenite phase observed in low carbon HSLA steels is well known to be decomposed to various bainitic microstructures, such as granular bainite, acicular ferrite and bainitic ferrite during continuous cooling process. These bainitic microstructures have been usually identified by using either scanning electron microscope (SEM) or transmission electron microscope (TEM). However, SEM and TEM images do no exactly coincide, because of the quite different sample preparation method in SEM and TEM observations. These conventional analysis method is, thus, not suitable for characterization of the complex bainitic microstructure. In this study, focused ion beam (FIB) technique was applied to make site-specific TEM specimens and to identify the 3-dimensional grain morphologies of the bainitic microstructure. The morphological feature and grain boundary characteristics of each bainitic microstructure were exactly identified.

• Journal of Welding and Joining
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• 제11권4호
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• pp.57-69
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• 1993

In the present study, the microstructure and Charpy V notch toughness of multipass $CO_2$ FCA weldment in three different heat inputs(1-3KJ/mm)were investigated. The weldments using two different domestic FCAW wires(AWS E71T-1 and E71T-5 equivalent) in C-Mn steel were chemically analysed. The following conclusions can be inferred. 1. T-1 wire Showed a stable arc transfer, less spatter and harsh, a better bead spreading and easy slag removal, whereas T-5 wire suffered from the arc stability, which tended to increase spatter and produce a more convex bead. 2.The microsturctures of the top beads of the weldments in three different heat inputs consisted of coarse-grained boundary ferrite and Widmanstatten ferrite side plate with increasing heat inputs. The modest fraction of acicular ferrite in the two wire weldments was observed in the 2KJ/mm heat input. 3.The fine-grained reheated zones of both welds consisted of a duplex microstructure of polygonal ferrite and second phases. 4. The basic flux weldment of T-5wires showed a higher Charpy impact property than that of T-1 wires because of a higher fraction of acicular ferrite in the weld microstructure.

• Archives of Metallurgy and Materials
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• 제67권4호
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• pp.1497-1501
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• 2022

In-situ observation of the transformation behavior of acicular ferrite in high-strength low-alloy steel using confocal laser scanning microscopy was discussed in terms of nucleation and growth. It is found that acicular ferrite nucleated at dislocations and slip bands in deformed austenite grains introduced by hot deformation in the non-recrystallization austenite region, and then proceeded to grow into an austenite grain boundary. According to an ex-situ EBSD analysis, acicular ferrite had an irregular shape morphology, finer grains with sub-grain boundaries, and higher strain values than those of polygonal ferrite. The fraction of acicular ferrite was affected by the deformation condition and increased with increasing the amount of hot deformation in the non-recrystallization austenite region.

• 열처리공학회지
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• 제12권1호
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• pp.21-30
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• 1999

The present study were investigated changes of precipitation behaviour of laves phase in ferrite single phase and ferrite-martensite dual phase and precipitation of laves phase under stress. Hardness changes in ferrite phase appeared two hardness peaks by precipitation of initial fine precipitator and laves phase in 3Mo-0.3Si and 3Mo-0.3Si-C specimens, respectively. Hardness changes in martensite phase of 3Mo-0.3Si-C specimen was lower in the initial stage of aging by carbide precipitation and after this, increased by re-hardening due to precipitation of laves phase. In the ferrite phase, laves phase was mainly precipitated, whereas in the martensite phase, carbide was preferentially formed during the initial stage of aging and with increasing aging time, laves phase and carbide were simultaneously precipitated by precipitation of laves phase at around carbide. In the ferrite-martensite interface, laves phase was mainly precipitated and carbide was mainly formed at boundary of lath martensite than grain boundary. Adding the stress in aging, fine precipitator of inital precipitation of laves phase precipitated in (100) of perpendicular to tensile direction and has grown to only followed<010>direction and also, volume fraction of laves phase increased. Consequently, the stress added was accelerated initial precipitation of laves phase.