• Annual Conference of KIPS
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• 2017.11a
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• pp.560-561
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• 2017

작품명은 Hazardous Gas Alarm System이다. 이는 현재 가스 검출기에 대한 단점을 보완하여 현장 근로자가 편안하게 사용할 수 있도록 한다. 주된 기술은 센서를 이용한 수치 측정 및 수집이며 이를 활용하여 근로자에게 대기오염 정도를 알려주고 위험수치를 넘으면 근로자가 쉽게 알 수 있게 할 수 있는 작품이다. 현재 시중에 나와 있는 제품들에 비해 값싸고 사용하기 쉽게 제작 하였다.

• Bulletin of the Korean Chemical Society
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• v.25 no.6
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• pp.806-808
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• 2004

A gas chromatography/mass spectrometric assay method has been developed for the simultaneous determination of icing inhibitors, ethylene glycol monomethyl ether and diethylene glycol monomethyl ether in ground water contaminated with JP-8. Ethylene glycol monobutyl ether and ethylene glycol monoethyl ether were used as the internal standard and surrogate, respectively. 100 mL of ground water was extracted twice with 20 mL of methylene chloride. The extract was concentrated to dryness, dissolved with 100 ${\mu}$L of methanol and analyzed by GC-MS (SIM). The use of an Innowax column gave the peaks good chromatographic properties, and the extraction of these compounds from samples gave recoveries of about 50% with small variations. The method detection limits of the target compounds were in a range of 0.5-0.8 ng/mL in ground water.

• Archives of Pharmacal Research
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• v.19 no.6
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• pp.566-569
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• 1996

A sensitivity method has been developed for the detection and determination of niflmic acid(NA) in human urine. Samples were extracted with diethylether. Flunixin (FN) was added to the sample prior to extraction as an internal standard. Niflumic acid was converted to its methyl derivative and analyzed by capillary gas chromatography/negative chemical isonization mass spectrometry. Using selected ion monitoring (SIM), the levels of NA down to 5 pg/ml could be detected in 5 ml spiked urine sample. Calibration curve was linear over the range of 0.5 ppm-50 ppm. The recovery of niflumic acid from urine at 40 pg/ml was to be $91.7{\pm}3.8(n=3)$ and the coefficient of variation was 4.1%.

• YAKHAK HOEJI
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• v.37 no.4
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• pp.356-361
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• 1993

A sensitive method for the determination of methamphetamine(MA) and amphetamine(AM) in hair was developed by gas chromatography/mass spectrometry using stable isotope-labeled internal standards, amphetamine-d$_{5}$ and methamphetamine-d$_{5}$. Hair sample was washed with MeOH, incubated with MeOH(I% HCI) overnight at $37^{\circ}C$ while stirring and extracted using solid phase extraction column on a vacuum manifold. The extract obtained was pentafluoropropionated, and applied to GC/MS. The calibration curves of MA and AM were linear from 2.5 to 250 ng (r>0.99 for both). The limit of detection was 0.1 ng/mg in hair and cut-off level was set at 0.25 ng/mg for both. Hair samples of 27 MA abusers showed positive results in the range 0.7 to 106.8 ng/mg. AM, its metabolite, was detected in 20 out of 27 samples. The ratio of MA versus AM was 4.6~38.3 in specimens. Hair analysis for methamphetamine by GC/MS is an effective method for identifying long-term drug abusers.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1994.05a
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• pp.79-82
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• 1994

We have manufacture Copper-tetra-tert-butylphalocyanine (CuTBP)Langmuir-Blodgett(LB) films, which is known be sensitive to NO$_2$ gab. A response of these films to the NO$_2$ gab was studied. A surface pleasure of 25mN/m was obtained as a proper one for a film deposition. A deposited film status was identified with Uv/visible absorption spectra, ellipsometry measurements, and current-voltage(I-Y) characteristics. The NO$_2$ gas response experiments under 200ppm conducentration show that there are increment of electrical conductivity by 12 times, 5 seconds of response time, and 5 seconds of response time, and 90 seconds of recovery time.

• Journal of Electrical Engineering and Technology
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• v.9 no.2
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• pp.615-621
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• 2014

Power transformer is one of the most important equipments in electrical power system. The detection of certain gases generated in transformer is the first indication of a malfunction that may lead to failure if not detected. Dissolved gas analysis (DGA) of transformer oil has been one of the most reliable techniques to detect the incipient faults. Many conventional DGA methods have been developed to interpret DGA results obtained from gas chromatography. Although these methods are widely used in the world, they sometimes fail to diagnose, especially when DGA results falls outside conventional method codes or when more than one fault exist in transformer. To overcome these limitations, fuzzy inference system (FIS) is proposed. 250 different cases are used to test the accuracy of various DGA methods in interpreting the transformer condition.

• Journal of the Korea Institute of Military Science and Technology
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• v.17 no.4
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• pp.510-520
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• 2014

Metal-Organic Frameworks(MOFs) are attracting attentions from various fields including chemistry, materials science, physics and medical science because of its exceptionally large pore volumes and surface areas which far exceed those of zeolites. The possibilities of applications of MOFs for gas separation, catalysts, drug delivery, and high explosives detections have already been verified. In these review the author describes the structures, synthetic methods and applications of MOFs based on the literatures published during last 15 years to give the readers general pictures of MOF itself as well as the global research trends of these materials.

• Bulletin of the Korean Chemical Society
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• v.19 no.1
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• pp.45-50
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• 1998

Most organophosphorus pesticides may be metabolized to yield some common phosphates in human or in animals, and these metabolites may be used as the exposure biomarkers to pesticides. In this study, we developed the extraction method of four phosphate metabolites from the spiked human urine in high recovery by the solid phase extraction with a reverse-phase cartridge (cyclohexyl silica) followed by the elution with methanol. The extracted urinary metabolites were derivatized with hexamethyldisilazane/trimethyl-chlorosilane/pyridine (2 : 1 : 10, v/v/v) and identified by gas chromatography/mass spectrometry. Calibration curve obtained from each metabolite standard using by GC/MS/SIM has shown good linearity and detection limits of metabolites were the range of 0.05-0.1 ㎍/㎖ in urine. Phenthoate, one of the organophosphorus pesticides, was orally administrated to rats. Four metabolites were detected in the rat urine. The results of this study may be applied to development of exposure biomarkers for monitoring of environmental pollutants.

• Journal of Magnetics
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• v.18 no.3
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• pp.357-360
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• 2013

A modified SQI method using magnetic leakage flux (MFL) signal for underground gas pipelines' defect detection and characterization is presented in this paper. Raw signals gathered using MFL signals include many unexpected noises and high frequency signals, uneven background signals, signals caused by real defects, etc. The MFL signals of defect free pipelines primarily consist of two kinds of signals, uneven low frequency signals and uncertain high frequency noises. Leakage flux signals caused by defects are added to the case of pipelines having defects. Even though the SQI (Self Quotient Image) is a useful tool to gradually remove the varying backgrounds as well as to characterize the defects, it uses the division and floating point operations. A modified SQI having low computational complexity without time-consuming division operations is presented in this paper. By using defects carved in real pipelines in the pipeline simulation facility (PSF) and real MFL data, the performance of the proposed method is compared with that of the original SQI.

• KSII Transactions on Internet and Information Systems (TIIS)
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• v.12 no.12
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• pp.6079-6097
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• 2018

Safety-related systems (SRSs) has widely used in shipbuilding and power generation to prevent fatal accidents and to protect life and property. Thus, SRS performance is a high priority. The safety integrity level (SIL) is the relative performance level of an SRS with regard to its ability to operate reliably in a safe manner. In this article, we proposed an optimal design procedure to achieve the targeted SIL of SRSs. In addition, a more efficient failure mode and effects diagnostic analysis (FMEDA) process and optimization model were developed to improve cost efficiency. Based on previous IEC 61508 diagnostic analyses that revealed unnecessary costs associated with excessive reliability, the new approach consists of two phases: (i) SIL evaluation by FMEDA, and (ii) solution optimization for achieving the target SIL with minimal cost using integer-programming models. The proposed procedure meets the required safety level and minimizes system costs. A case study involving a gas-detection SRS was conducted to demonstrate the effectiveness of the new procedure.