• Title/Summary/Keyword: GIC

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THE EFFECTS OF NANO-SIZED HYDROXYAPATITE ON DEMINERALIZATION RESISTANCE AND BONDING STRENGTH IN LIGHT-CURED GLASS IONOMER DENTAL CEMENT (광중합형 글라스아이오노머 시멘트의 탈회 저항성과 결합 강도에 대한 나노미터 입자의 하이드록시아파타이트의 효과)

  • Kim, Ji-Hee;Lee, Yong-Keun;Kim, Seong-Oh;Song, Je-Seon;Choi, Byung-Jai;Choi, Hyung-Jun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.37 no.1
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    • pp.24-34
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    • 2010
  • The aim of this study was to evaluate the effect of incorporated nano HA on the demineralization resistance and bonding strength of LC GIC in comparison with micro HA. Fuji II LC GIC was used as the control group and a base material for experimental groups. Two experimental groups were prepared. One was prepared by adding 15% micro HA to LC GIC by weight ratio (Exp. 1), and the other was prepared by adding 15% nano HA instead (Exp. 2). According to the results, the following conclusions could be obtained. 1. Observing under the CLSM, the control group showed thicker enamel demineralization layer than in the experimental groups, and the Exp. 2 group showed the thinnest demineralization layer. 2. In SEM analysis, there was greater enamel demineralization in the control group. The Exp. 2 group was more resistant to demineralization compared to the Exp. 1 group. 3. The bonding strength was found to be in the increasing order of control, Exp. 1, and Exp. 2 group (p < 0.05). 4. Observing the fractured surfaces under SEM after the bonding strength test was performed, there were bone-like apatite particles formed in HA-added experimental groups, and a greater number of bone-like apatite particles were formed in the Exp. 2 group compared to the Exp. 1 group.

The Study on the Structure and Energy State of Potassium-Graphite Intercalation Compounds (칼륨-흑연 층간화합물의 구조와 에너지 상태에 관한 연구)

  • 오원춘;백대진;고영신
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.3 no.1
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    • pp.66-74
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    • 1993
  • Potassium-Graphite Intercalation Compounds(K-GICs) have been prepared from purified natural graphite by transformed two-bulb method with variations of reaction temperature ($T_g:450^{\circ}C$, $400^{\circ}C$, $350^{\circ}C$, $300^{\circ}C$, $250^{\circ}C$).Prepared K-GICs were identified to stage transition process by X-ray diffraction data. At these results, d values of (00l) diffraction at 1 stage and 2 stage were corresponded to $5.35\AA$ and $8.73\AA$ respectively. The stage stability and energy states of K-GlCs were obtained by UV /VIS Spectrophotometric data. We found that the minimum value of reflectance was 2.67 eV(465nm) at $250^{\circ}C$and it's moved to higher energy than original graphite's. And X-ray diffraction and UV /VIS spectrophotometric datas suggest that K-GICs were formed lower stage and many charge carriers exist between C atoms of graphite. And then, these results also provide informations on the electrical and other physical properities of K-GICs.Especially, according to studied reports, d values differ from them of each author, but accurate values were established through this study.

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Effect of the restorative technique on load-bearing capacity, cusp deflection, and stress distribution of endodontically-treated premolars with MOD restoration

  • da Rocha, Daniel Maranha;Tribst, Joao Paulo Mendes;Ausiello, Pietro;Dal Piva, Amanda Maria de Oliveira;Rocha, Milena Cerqueira da;Di Nicolo, Rebeca;Borges, Alexandre Luiz Souto
    • Restorative Dentistry and Endodontics
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    • v.44 no.3
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    • pp.33.1-33.12
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    • 2019
  • Objectives: To evaluate the influence of the restorative technique on the mechanical response of endodontically-treated upper premolars with mesio-occluso-distal (MOD) cavity. Materials and Methods: Forty-eight premolars received MOD preparation (4 groups, n = 12) with different restorative techniques: glass ionomer cement + composite resin (the GIC group), a metallic post + composite resin (the MP group), a fiberglass post + composite resin (the FGP group), or no endodontic treatment + restoration with composite resin (the CR group). Cusp strain and load-bearing capacity were evaluated. One-way analysis of variance and the Tukey test were used with ${\alpha}=5%$. Finite element analysis (FEA) was used to calculate displacement and tensile stress for the teeth and restorations. Results: MP showed the highest cusp (p = 0.027) deflection ($24.28{\pm}5.09{\mu}m/{\mu}m$), followed by FGP ($20.61{\pm}5.05{\mu}m/{\mu}m$), CR ($17.62{\pm}7.00{\mu}m/{\mu}m$), and GIC ($17.62{\pm}7.00{\mu}m/{\mu}m$). For load-bearing, CR ($38.89{\pm}3.24N$) showed the highest, followed by GIC ($37.51{\pm}6.69N$), FGP ($29.80{\pm}10.03N$), and MP ($18.41{\pm}4.15N$) (p = 0.001) value. FEA showed similar behavior in the restorations in all groups, while MP showed the highest stress concentration in the tooth and post. Conclusions: There is no mechanical advantage in using intraradicular posts for endodontically-treated premolars requiring MOD restoration. Filling the pulp chamber with GIC and restoring the tooth with only CR showed the most promising results for cusp deflection, failure load, and stress distribution.

Impact behavior on temperature effect of nano composite materials (온도변화에 따른 나노 복합재료의 충격거동)

  • KIM, Hyung-Jin;LEE, Jung-Kyu;KOH, Sung Wi
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.51 no.4
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    • pp.561-566
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    • 2015
  • In this study, the effect of temperature effect of the rubber matrix filled with nano sized silica particles composites with silica volume fraction of 19-25% was investigated by the Charpy impact test. The Charpy impact test was conducted in the temperature range from $-40^{\circ}C$ to $0^{\circ}C$. The critical energy release rate GIC of the rubber matrix composites filled with nano sized silica particles was considerably affected by temperature and it was shown that the maximum value was appeared at higher temperature between temperature tested and it was shown that the value of GIC increases as temperature tested increases. The major fracture mechanisms were matrix deformation, silica particle debonding and delamination, microcrack between particles and matrix, and/or pull out between particles and matrix which is ascertained by SEM photographs of Charpy impact surfaces fracture.

THE EFFECT OF GLASS IONOMER CEMENT ON THE DOG'S EXPOSED DENTAL PULP (글라스 아이오노머 세멘트가 가견(家犬) 노출(露出) 치수조직(齒髓組織)에 미치는 영향(影響))

  • Kim, Jae-Han;Cho, Kyew-Zeung
    • Restorative Dentistry and Endodontics
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    • v.12 no.2
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    • pp.73-80
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    • 1987
  • The present study was designed to help elucidate the effect of glass ionomer cements on the exposed dental pulp by means of histologic examination. A total of 40 cavities of class V were prepared on the teeth of 4 dogs with exposure of 1mm in diameter on the bases of them. 20 cavities were filled with glass ionomer cement as the experimental group and the other 20 cavities were filled with zinc oxide eugenol cement as the control group. The dogs were sacrificed at one, two, three, and four weeks after filling, and the specimens were routinely prepared and stained with Hematoxylin-Eosin. The obtained microscopic findings were as follows: Inflammatory cell infiltrations were observed in control in 1 week, which decreased markedly with time. In all control groups, hemorrhage around exposed pulp tissue and coagulation change of pulp were observed. Secondary dentin formation and thickened predentin were observed in 4 week cases, and the recovery of pulp tissue was favorable on the whole. Inflammatory cell infiltration was observed in all GIC groups. Proliferation of blood vessel and congestion were observed with coagulation changes around the exposed pulp tissue. Secondary dentin formation and thickened predentin were observed in 3 weeks. In the experimental 4 week case, secondary dentin formation was evident. On the whole, pulpal irritation of glass ionomer cement was relatively severe. Recovery of pulp tissue in GIC groups was less favorable compared with that of ZOE groups.

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COMPARISON OF MARGINAL LEAKAGE OF CLASS 5 GIC RESTORATIONS ACCORDING TO CAVITY DESIGNS (와동 형태에 따른 5급 글라스 아이오노머 시멘트 수복물의 변연누출 비교)

  • Lee, Seon-Hwa;Hur, Bock;Lee, Hee-Joo
    • Restorative Dentistry and Endodontics
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    • v.23 no.1
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    • pp.296-303
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    • 1998
  • The purpose of this study was to assess the effects of cavity designs on the marginal leakage of class 5 glass ionomer restorations. The five cavity designs were as follows ; notch shape(A group), notch shape with groove(B group), combined lesion(C group), combined lesion with groove and deep chamfer margin(D group) and combined lesion with groove and shoulder(E group), and each design had 10 cavities. After the cavities were restored with GIC, they were immersed in 0.5% basic fuchsin solution for 6 hours. The specimens were washed thoroughly and sectioned longitudinally in a buccolingual direction through the center of the restorations. The degree of marginal leakage was measured as the extent of dye penetration under the stereoscope. The results of this study were as follows 1. The enamel margins of all groups showed lesser leakage than dentin/cementum margins(p<0.05). 2. The combined lesion(C group) showed more leakage than notch shape(A group), but there was no siginificant difference(p>0.05). 3. In the notch shape, there was no influence on the marginal leakage by the groove preparation. 4. In the combined lesion, marginal leakage was decreased by the groove preparation and marginal modification.

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A STUDY ON THE BOND STRENGTHS BETWEEN GLASS IONOMER CEMENT BASES AND COMPOSITE RESINS (글래스 아이오노머 이장재와 복합레진간의 결합강도에 관한 연구)

  • Kim, Min-Hee;Kim, Shin;Jeong, Tae-Sung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.26 no.3
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    • pp.520-527
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    • 1999
  • For the purpose of providing some suggestions in selection of filling materials used in 'sandwich technique', the bond strengths between glass ionomer cement bases and composite resins were investigated and compared. For lining materials, 'Vitrebond' and 'Ketac-fil' were used. Using these two as bases, 10 of each following resins were built up on the top ; Z-100 (light curing resin) Clear-fil (chemical curing resin), Bis-core (dual cure resin), Dyract (compomer), therfore 10 specimens of each group and total of 80 specimens were made. After storing specimens in $37^{\circ}C$ deionized water for 24 hours, the shear bond strengths were measured under universal testing machine with 50 kg of full load scale and 1mm/min of cross-head speed and obtained the results as follows : 1. Over Vitrebond base, Z-100 showed the lowest bond strength but the other three did not show any difference in bond strength. 2. Over Ketac-fil base, Clear-fil showed the highest bond strength followed by Dyract, Bis-core, and Z-100 showed the lowest bond strengths. 3. Whereas Clear-fil showed the similar bond strengths on the Vitrebond base as other resins, it showed the highest bond strength on Ketac-fil base, which showed some difference in bond strength by differing GIC bases. 4. The bond strengths between base materials and composite resin showed a stronger resin-dependence tendency in cases with Ketac-fil bases rather than with Vitrebond bases.

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The Optimum Addition Ratio of Nano Hydroxyapatite to Glass Ionomer Dental Cement (Changes in Demineralization Resistance and Bonding Strength of Light Cured Glass Ionomer after the Addition of Nano Hydroxyapatite in Various Ratio) (글래스아이오노머에 대한 나노 하이드록시아파타이트의 최적 첨가 비율(나노 하이드록시아파타이트의 첨가 비율에 따른광중합형 글래스아이오노머의 결합강도와 탈회저항성의 변화 비교))

  • Kim, Nam Hyuk;Kim, Seong Oh;Song, Je Seon;Lee, Jae Ho;Son, Heung Kyu;Choi, Byung Jai;Choi, Hyung Jun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.40 no.3
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    • pp.159-167
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    • 2013
  • The aim of this study was to evaluate changes in demineralization resistance and bonding strength of light cured glass ionomer after the addition of nano hydroxyapatite in various ratios. Fuji II LC GIC (GC Co., Japan) was used as the control group and also as a base material for experimental group. HA was mixed into the RMGIC at various ratio to create a HA-LC GIC mixture, preparing six experimental groups, i.e. 5%, 10%, 15%, 20%, 25%, 30% HA-LC GIC. According to the results, the bonding strength increased due to the addition of HA, showing the maximum value at the 15% nano HA group (p < 0.05). Under CLSM observation after 4 days of demineralization, the HA groups were more resistant to demineralization compared to the control group. No significant difference was observed between HA groups. In analysis through SEM, the HA groups showed attachment of granular materials and decreased demineralized tooth surfaces under influence of HA particles.