• Title/Summary/Keyword: Freezing characteristics

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Physicochemical Characteristics of Pumpkin(Cucurbita moschata Duch.) Powder with Different Treatment Conditions (처리 조건을 달리한 늙은호박 분말의 이화학적 특성)

  • Shin, Dong-Sun;Yoo, Yeon-Mi;Park, Bo-Ram
    • Korean journal of food and cookery science
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    • v.29 no.6
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    • pp.691-697
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    • 2013
  • This study determines the processing suitability of pumpkin powder by assessing, the physicochemical properties of pumpkin powder subjected to different treatments: steaming, freezing and roasting. Pumpkin powder containing 13.61-16.05% moisture, 39.40-9.53% protein, 1.35-1.43% lipid, 0.26-0.50% ash, 5.01-5.65% yield, and 9.40-10.50 mg% sugar was used. In terms of color values, the L-value of control, a-value of the steamed sample, and b-value of the roasted sample waere the highest. The steamed sampled had the highest DPPH radical-scavenging activity. Reduction in sugar concentration varied significantly by treatments conditions (p < 0.05). Carotenoid concentration was the highest in control (19.75 mg%), followed by steamed sample (17.91 mg%), frozen sample (15.17 mg%), and the roasted sample (14.04 mg%). On the basis of these results, steamed pumpkin powder was identified as the most suited for instant processing.

Acrosomal Changes and Survivability of Following Preservation of Dog Spermatozoa I. The Effects of Different Chilling Duration (개 정자의 보존방법에 따른 첨체 및 생존성의 변화 1. 저온보존에 따른 효과)

  • 정정란;유재규;양성렬;여현진;박종식;예은하;노규진;최상용
    • Journal of Embryo Transfer
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    • v.16 no.1
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    • pp.35-40
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    • 2001
  • Artificial insemination (AI) with frozen or cooled semen is widely used in commercial fields of cattle and pig. Little is known about characteristics of canine sperm after freezing or cooling. For both practical and commercial goal, the canine semen treated with cooling and freezing should be carried out to exam the fundamentals, including sperm motility, survivability and fertilizing capacity. The aim of this study, thus, was to identify the effects of extended exposure to 4$0^{\circ}C$ on canine semen by motility, survivability, acrosomal changes following different duration. Fifteen ejaculates collected by digital manipulation twice per week from 3 dogs (Shih-Tzu) were divided to 16 aliquots after adding Tris-egg yolk (TE) buffer formulated by our laboratory, and cooled from 37 to 4$^{\circ}C$, by ramp rate of 0.6$^{\circ}C$/min. Each sample was evaluated by their motility, survivability and the acrosomal status at 0h (control), 2h, 12h and 1 d~10 d, respectively. The motility of spermatozoa was graded to 6 levels using the modified method of Seager. The survivability of sperm was assessed using an epifluorescence microscope after Fert/Light (Mole-cular Probes Inc.) staining. To estimate the proportion of the spermatozoa of intact acrosome, 200 spermatozoa were assessed in randomly selected fields, using epifluorescence microscope after FITC/PSA (Sigma) staining. At 2 h after cooling, the motility of most spermatozoa were assessed to be grade 0 and 1. At 12 h, high number of sperm were in grade 0 to 1, however, it was significantly (P<0.05) lower than that of 2 h. From 1 d to 4 d, ~50% of sperm was assessed to grade 0 to 1. On day 7, a little sperm were in grade 0 to 1. No sperm showed motility on day 10. Sperm motility was rapidly reduced by the percent of 10% of grade 0 to 1. From 2 h to 6 h, the number of live sperm was 90% and the sperm chilled for 10 days lived>50%. Acrosomal intact of spermatozoa exposed to 4$^{\circ}C$ for 2 h was 51%, supposed the sperm of control was 100%. Our results suggest that 1) this is easy to transfer and preservation for short periods 2) AI can be used by semen chilled for 6-Day.

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Variations of Mechanical Properties of Hallasan Trachyte with respect to the Degree of Weathering (풍화진행에 따른 한라산조면암의 역학적 특성변화)

  • Cho, Tae-Chin;Lee, Sang-Bae;Hwang, Taik-Jean;Won, Kyung-Sik
    • Tunnel and Underground Space
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    • v.19 no.4
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    • pp.287-303
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    • 2009
  • Rock mass in Baekrokdam at the summit of Hallasan in Jeju island is composed of two volcanic rock types: Baekrokdam trachybasalt at the eastern region and Hallasan trachyte at the western region. On-going rockfall and subsequent collapse of Baekrokdam wall rock are closely linked to the weathering of trachyte distributed in the western region of Baekrokdam. Samples of Hallasan trachyte showing different weathering grades had been collected and the polarizing microscopic observation, X-ray diffraction analysis and analysis for chemical weathering had been conducted. Formation of secondary minerals, especially clay minerals, by chemical weathering has not been identified, but the change of chemical weathering indices indicated that chemical weathering process had been proceeded to the degree for increasing and decreasing the contents of some chemical components. Changes in physical and mechanical rock properties due to weathering has also been examined. Artificial weathering test of freezing-thawing reveals that the process of crack initiation and propagation deteriorated the mechanical characteristics of Hallasan trachyte and $D_B$ = 1.5 or porosity = $20{\sim}21%$ would be the ultimate limiting value induced by the mechanical weathering processes.

A Study on Long-Term Mechanical Properties and Durability in Metakaolin Concrete Bridge Deck (메타카올린 콘크리트 교량바닥판의 장기 역학적 특성 및 내구성에 관한 연구)

  • Yang, Eun Ik;Kim, Myung Yu;Yang, Joo Kyoung;Park, Hae Geun;Choi, Yoon Suk
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.15 no.3
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    • pp.125-133
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    • 2011
  • The requirement for durability of concrete bridge deck is increasing as the deterioration for the concrete bridge deck exposed to severe environment has been increased. For this reason, the concern about high-durable concrete is being high. Recently, a metakaolin is highly spotlighted as new admixture because its strength and durability are equivalent to silica fume. On the other hands, there are few researches for the metakaolin concrete bridge deck in domestic. So many various long-term data on the mechanical property and durability is needed to apply metakaolin concrete at the concrete bridge deck construction field. This study is aim to evaluate the long-term mechanical properties and durability of metakaolin concrete bridge deck with curing age. Mechanical properties are estimated by the compressive and flexural strength, and the drying shrinkage, the chloride resistance, the scaling, and freezing and thawing characteristics are compared with curing age. According to the results, when the metakaolin concrete is used, the development of compressive and flexural strength proceed in both the early and old ages. It is also improved the resistance of chloride penetration, freezing and thawing in concrete. It was showed that replacement of metakaolin was efficient for the reduction of the drying shrinkage.

Physical Properties of $LiPF_6/PC+EC+DEC$ Electrolyte by the Variation of PC Fraction and Initial Electrochemical Properties of Carbon Anode in the Electrolyte (PC 비율에 따른 $LiPF_6/PC+EC+DEC$ 전해액의 물리적 특성 및 탄소분극과의 초기 전기화학적 특성)

  • Doh Chil-Hoon;Moon Seong-In;Yun Mun-Soo
    • Journal of the Korean Electrochemical Society
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    • v.3 no.4
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    • pp.224-231
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    • 2000
  • The exfoliation of graphite (layer) was progressed due to the irreversible insertion of PC molecules between graphene layers, when propylene carbonate (PC) solvent was used as the organic solvents. The problem could be mitigated by the replacement of PC by ethylene carbonate (EC). But, the freezing point of EC-based electrolyte increased due to the high freezing point of $EC(36.2^{\circ}C)$. Therefore, EC+PC mixed electrolyte is expected as a good organic electrolyte for lithium ion battery. The EC-based organic electrolyte containing PC within pertinent quantity can be expected to have high molar conductivity and reduced exfoliation of graphite layer. The dielectric constant and molar conductivity of $LiPF_6/PC+EC+DEC$ electrolyte was investigated with a variation in the PC content. The electrochemical properties of carbon electrode in the electrolyte were also investigated. Molar conductivity and dielectric constant increased linearly by increasing the PC volume fraction in the electrolyte. The results of charge-discharge test for carbon/electrolyte/Li cell indicated that the initial irreversible specific capacity(IIC) of MCMB-6-28s and MPCF3000 decreased by the addition of $0.83 vol\%$ of PC, but increased with PC content over than $0.83 vol\%$. In the case of MPCF3000 and PCG100 having less than $10 vol\%$ PC, IIC was lower than 50 mAh/g. The discharge specific capacities varied with carbon material, but did not vary with PC content in the electrolyte.

An Experimental Study on Frost Heaving Pressure Characteristics of Frozen Soils (동결토의 동상팽창압 특성에 관한 실험적 연구)

  • 신은철;박정준
    • Journal of the Korean Geotechnical Society
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    • v.19 no.2
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    • pp.65-74
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    • 2003
  • Most of land reclamation projects are being implemented along the south and west coastal lines of the Korean Peninsula. The earth structures and in-ground LNG tank, and buildings can be constructed using artificial freezing method on the reclaimed land to control the uplift pressure caused by capillary forces. In this study, upon freezing a saturated soil in a closed-system from the top, a considerable frost heaving pressure was developed. Decomposed granite soils, silty soil, and sandy soil were used in the laboratory freeze test which is sometimes subjected to thermal gradients under closed-systems. A major concern has been the ability to predict the frost heaving pressure over the results of relatively short-term laboratory tests. The frost heaving pressure arising within the soil samples and the temperature of the samples inside were monitored with time elapse. The degree of saturation versus heaving pressure curve is presented for each soil sample and the maximum pressure is closely related to this curve. TDR apparatus was used to measure the volumetric water content by the measurement of unfrozen water contents of frozen soils. Unfrozen water increased in soils containing a high percentage of fine-grained particles. In fine-grained soils with strong attractive farces between soil grains and water molecules, additional water is attracted into the pores leading to further volume changes and ice segregation.

Prediction of Adfreeze Bond Strength Using Artificial Neural Network (인공신경망을 활용한 동착강도 예측)

  • Ko, Sung-Gyu;Shin, Hyu-Soung;Choi, Chang-Ho
    • Journal of the Korean Geotechnical Society
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    • v.27 no.11
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    • pp.71-81
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    • 2011
  • Adfreeze bond strength is a primary design parameter, which determines bearing capacity of pile foundation in frozen ground. It is reported that adfreeze bond strength is influenced by various affecting factors like freezing temperature, confining pressure, characteristics of pile surface, soil type, etc. However, several limited researches have been performed to obtain adfreeze bond strength, for past studies considered only few affecting factors such as freezing temperature and type of pile structures. Therefore, there exists a limitation of estimating the design parameter of pile foundation with various factors in frozen ground. In this study, artificial neural network algorithm was involved to predict adfreeze bond strength with various affecting factors. From past five studies, 137 data for various experimental conditions were collected. It was divided by 100 training data and 37 testing data in random manner. Based on the analysis result, it was found that it is necessary to consider various affecting factors for the prediction of adfreeze bond strength and the prediction with artificial neural network algorithm provides enough reliability. In addition, the result of parametric study showed that temperature and pile type are primary affecting factors for adfreeze bond strength. And it was also shown that vertical stress influences only certain temperature zone, and various soil types and loading speeds might cause the change of evolution trend for adfreeze bond strength.

Durability Characteristics in Concrete with Ternary Blended Concrete and Low Fineness GGBFS (삼성분계 콘크리트와 저분말도 슬래그를 혼입한 콘크리트의 내구 특성)

  • Kim, Tae-Hoon;Jang, Seung-Yup;Kwon, Seung-Jun
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.4
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    • pp.287-294
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    • 2019
  • GGBFS(Ground Granulated Blast Furnace Slag) has been widely used in concrete for its excellent resistance chloride and chemical attack, however cracks due to hydration heat and dry shrinkage are reported. In many International Standards, GGBFS with low fineness of 3,000 grade is classified for wide commercialization and crack control. In this paper, the mechanical and durability performance of concrete were investigated through two mix proportions; One (BS) has 50% of w/b(water to binder) ratio and 60% replacement ratio with low-fineness GGBFS, and the other (TS) has 50% of w/b and 60% replacement ratio with 4000 grade and FA (Fly Ash). The strength difference between TS and BS concrete was not great from 3 day to 91 day of age, and BS showed excellent performance for chloride diffusion and carbonation resistance. Two mixtures also indicate a high durability index (more than 90.0) for freezing-thawing since they contain sufficient air content. Through improvement of strength in low fineness GGBFS concrete at early age, mass concrete with low hydration heat and high durability can be manufactured.

Field Appliciability Evaluation of Eco-friendly Mixed Soil (친환경 혼합토의 현장적용성 평가)

  • Park, Kyungsik;Oh, Sewook;Bae, Wooseok
    • Journal of the Korean GEO-environmental Society
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    • v.15 no.2
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    • pp.17-25
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    • 2014
  • In the present study, it were performed an unconfined compression test and a field applicability test according to a mixed ratio of SS, soil type and curing period to analyze strength and deformation characteristic in order to evaluate engineering characteristics of soil mixed pavements using the eco-friendly soil stabilizer (SS). The test results revealed that SS mixed soil shows fast strength development at the initial curing time while 28-day strength amounted for 97% of the final strength. Furthermore, coarse-grained dredged sand (DS) and weathered granitic soil (WGS) have a larger ratio of deformation coefficient with respect to unconfined compressive strength than fine-grained dredged clay (DC) and organic soil (OS). Moreover, a comparison test between natural and forced drying conditions was conducted and test result showed 54% to 67% of strength degradation while having 55% to 63% of strength degradation in the freezing and thawing test result. Finally, a repeated loading test result showed that DS experiences up to 35% of strength reduction compared to initial strength under 10,000 times loading in maximum. Thus, it was validated that an appropriate amount of fine-grained sand is necessary to secure resistance capability to repeated loading.

Experimental Assessment and Specimen Height Effect in Frost Heave Testing Apparatus (동상시험장비의 실험적 검증 및 시료크기의 영향에 관한 연구)

  • Jin, Hyunwoo;Ryu, Byunghyun;Lee, Jangguen
    • Journal of the Korean GEO-environmental Society
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    • v.20 no.1
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    • pp.67-74
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    • 2019
  • Frost heave is one of the representative engineering characteristics in cold regions. In South Korea, which is located in seasonal frost area, structural damage caused by frost heave and thaw happens and the need for research on the frost heave is increasing. In this paper, newly developed transparent temperature-controllable cell is used to focus on the frost heave. Frost susceptible artificial soil is used to analyze water intake rate which is one of the important factors in frost susceptibility criteria. Frost heave rate and water intake rate have similar behavior after heave by freezing of pore water converges. O-ring installed in the upper pedestal to measure water intake rate generates side friction between the inner wall of the freezing cell and O-ring, thereby hindering frost heave. Therefore, the frost susceptibility criteria using the water intake rate is not reliable. It is appropriate to use frost heave rate which has similar behavior with water intake rate. Frost heave tests were performed under two different specimen heights. Overburden pressure, temperature gradient and dry unit weight were set under similar state. Based on laboratory testing results, frost heave is independent on the specimen height.