• Applied Microscopy
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• v.26 no.4
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• pp.447-456
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• 1996

Fracture surfaces of materials contain useful information ranging from crack path to the mechanism of fracture. Since limitation of electron transparency requires a sample in the form of thin foil for TEM observations, it is impossible to extract such information directly from the fracture surfaces. In this study, the method of surface replication from the ceramic fracture surface is employed to characterize the process of crack propagation in ceramic matrix composites using TEM analysis. The surface replica from the fracture surface in ceramic materials provides detailed surface morphology and more importantly, loosened particles on the fracture surface are collected. Electron diffraction and chemical composition analyses of these particles reveal crack path in the specimen. Furthermore, one can determine the mode of fracture by observing the fracture surface morphology from the image of replica. Two examples are given to illustrate the potential of the surface replication technique. In the first example, apparent toughness increase in $B_{4}C-Al$ composites at high strain rate is investigated by surface replication to elucidate the mechanism of fracture at different strain rates. The polytypes of SiC formed during the sintering of SiC-AlN composite and their effect on the fracture behavior of SiC-AlN composite are analyzed in the second example.

• Journal of Mechanical Science and Technology
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• v.15 no.10
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• pp.1417-1422
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• 2001

Since fracture surface presents clear evidence to describe the circumstances of material failure event, analysis of fracture surface should provide plenty of useful information for failure prevention. Thus if we extract proper information from the fracture surface, the safety evaluation, for plant component could be more accurate. In general, the chaotic morphology of fracture surface is determined by the degree of material degradation as well as by other factors such as type of load, geometry of specimen, notch condition, microstructure of material and environment. In this research, we developed a fractal analysis technology for the fracture surface of aged turbine rotor steel based on the slit-island technique using an image analyzer. Moreover the correlation between the fractal dimension and the aging time was studied.

• Journal of Ocean Engineering and Technology
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• v.10 no.4
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• pp.84-91
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• 1996

A fractal analysis on fracture surface of aluminium-particulate SiC composites was attempted. As the volume fraction of SiC in composites increases, the fractal dimension tends to increase. However, no correlation between the fractal dimension and the fracture toughness in terms of critical energy release rate was observed. Since the fractal dimension represents the roughness of fracture surface, the fracture toughness would be a function of not only fracture surface roughness but also additional parameters. Thus the applicability of fractal analysis to the estimation of fracture toughness must depend on the proper choice and interpretation of additioal paramerters. In this paper, the size of characteristic strctural unit for fracture was considered as an additional parameter. As a result, the size appeared to be a function of only volume fraction of SiC. Finally, a master curve for fracture toughness of aluminium-particulate SiC composites was proposed as a function of fractal dimension and volume fraction of SiC.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.20 no.1
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• pp.95-102
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• 2021

Analysis of the fracture surface is one of the most important methods for determining the cause of equipment structural failure. Whether structural failure is caused by impact or fatigue is necessary information in industrial fields. For ferrous and non-ferrous metal materials, two fracture phenomena are generated on the fracture surface: ductile and brittle fractures. In this study, machine learning predicts whether the fracture is based on ductile or brittle when structurural failure is caused by impact. The K-means algorithm calculates this ratio by clustering the brittle and ductile fracture data from a photograph of the impact fracture surface, unlike the existing method, which calculates the fracture surface ratio by comparison with the grid type or the reference fracture surface shape.

• The Journal of Korean Academy of Prosthodontics
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• v.39 no.6
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• pp.682-697
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• 2001

This investigation evaluated the fracture toughness($K_{IC}$) of eight currently available core materials, and relate the fracture toughness value to fractography analysis and surface characteristics using a atomic force microscope (AFM). Single-edge notched (SEN) test specimens (n=10) and compact tension (CT) test specimens (n=10) were prepared conforming to the ASTM Standard E-399 for a high copper amalgam, three composite core materials (Core-Max II, Core Paste, Bisfil Core), two reinforced composite core materials (Ti-Core, Ti-Core Natural), a resin-modified glass ionomer core material (Vitremer), and a conventional glass ionomer core material (Ketac-Molar). The specimens were tested with an Instron Universal Testing Machine. The maximum loads were measured to calculate the fracture toughness ($K_{IC}$). Thereafter, fracture surfaces of SEN specimens of each material were investigated for fractography analysis using scanning electron microscope. And, disc-shaped specimens with 1mm thickness were fabricated for each material and were investigated under AFM for surface morphology analysis. The results were as follows: 1. Bisfil Core showed the highest mean fracture toughness regardless of test methods. 2. For the tooth-colored materials, Ti-Core Natural exhibited the highest fracture toughness. 3. Ketac Molar showed a significantly low fracture toughness when compared with the amalgam and the composite resin core materials(p<0.05). 4. The fracture toughness values obtained with the single-edge notched test, except Ketac Molar, were higher than those obtained in the compact tension test. 5. SEM revealed that the fracture surface of high fracture toughness material was rougher than that of low fracture toughness material. 6. AFM revealed that the surface particles of the composite resins were smaller in size, with a lower surface roughness than the glass ionomer core materials.

• Journal of the Korean Ceramic Society
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• v.26 no.5
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• pp.645-654
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• 1989

Specimens of WC-Co were indented to measure the resulting crack size and unindented samples were fractured in 3-point flexure to obtain the strength and to measure characteristic features on the fracture surface. Fracture toughness was determined using fractography and compared to those determined using identation techniques. We show that principles of fracture mechanics can be applied WC-Co composites and can be used to analyze the fracture process. The fracture surfaces were examined by scanning electron microscopy and optical microscopy. Characteristic feature observed in glasses, single crystals and polycrystalline materials known as mirror, mist, hackle, and crack branching were identified for these composites. We discuss the importance of fracture surface analysis in determining the failure-initiating sources and the failure behaviorof WC-Co composites.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.31 no.4
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• pp.432-440
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• 2007

In this study, we have investigated the closure behavior of fatigue cracks in SAPH440 steel plates under a mixed-mode I+II loading. A crack image capturing system as a direct measuring method was used to measure the closure levels at a crack tip. The crack closure levels in the fluctuation and stable sections were increased with the increase of the mode mixture ratio. The mode mixture ratio independent fatigue crack propagation rates equation was calculated by considering mixed-mode crack closure levels. The equation was examined according to the application method of crack opening ratio. The fracture surface analysis by C-scan method was also performed in order to investigate the closure mechanism and propagation mode of crack under the mixed-mode I+II loading. The crack closure under the mixed mode I+II is confirmed as a surface roughness closure by the quantitative analysis of fracture surface using the proposed surface roughness parameter.

• Journal of the Korean Society for Heat Treatment
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• v.26 no.4
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• pp.178-184
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• 2013

The effects of thickness and surface grinding condition on the fracture strength of Si wafer with a thickness under $100{\mu}m$ were investigated. Fracture strength was measured by ball breaker test for about 330 dies (size: $4mm{\times}4mm$) per each wafer. For statistical analysis of the fracture strength, scale factor was determined from Weibull plot. Ball breaker fracture strength was observed to increase with decreasing thickness of silicon die. For the silicon dies of different surface conditions, ball breaker fracture strength was high in the order of polished, ground (#4800), and ground (#320 grit) specimen. Probabilistic fracture strength (i.e., scale factor) increased with decreasing surface roughness of silicon die.

• Nuclear Engineering and Technology
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• v.54 no.5
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• pp.1726-1746
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• 2022

This paper presents fracture mechanics analysis results for various cracks located at pressurized water reactor pressure vessel nozzle crotch corners taking into consideration constraint effect. Technical documents such as the ASME B&PV Code, Sec.XI were reviewed and then a fracture mechanics analysis procedure was proposed for structural integrity assessment of various nozzle crotch corner cracks under normal operation conditions considering the constraint effect. Linear elastic fracture mechanics analysis was performed by conducting finite element analysis with the proposed analysis procedure. Based on the evaluation results, elastic-plastic fracture mechanics analysis taking into account the constraint effect was performed only for the axial surface crack of the reactor pressure vessel outlet nozzle with cladding. The fracture mechanics analysis result shows that only the axial surface crack in the reactor pressure vessel outlet nozzle has the stress intensity factor exceeding the low bound of upper-shelf fracture toughness irrespectively of considering the constraint effect. It is confirmed that the J-integral for the axial crack of the outlet nozzle does not exceed the ductile crack initiation toughness. Hence, it can be ensured that the structural integrity of all the cracks is maintained during the normal operation.

• Journal of the Korean Ceramic Society
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• v.47 no.5
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• pp.365-372
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• 2010

This paper was to evaluate the influence of kiln process parameter(kiln angle, kiln rotating speed) of lightweight aggregate using waste glass and bottom ash with industrial by-products on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis. In the results of surface plot and contour plot, it has verified that kiln residence time of lightweight aggregate increase as kiln angle and rotating speed decreases. For this reason, pore size and quantity tend to increase by active reaction of forming agent. It seems to be that increase in pore size and quantity have caused decreasing density, fracture load and thermal conductivity, and increasing water absorption. In conclusion, optimization of kiln process parameter on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis are kiln angle 2.4646%, kiln rotating speed 40.7089 rpm.