• Journal of Advanced Marine Engineering and Technology
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• 제31권4호
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• pp.377-384
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• 2007

A backscatter Kikuchi diffraction attachment to an SEM enables the convenient investigation of grain orientations on bulk or micro surface. Their relation to micro structural features gives insight into many aspects of anisotropic materials properties. In micro area such as Micro Electro Mechanical Systems(MEMS) devices is required in order to improve understanding of how they may be expected to perform upon the micro scale. Electro Back Scatter Diffraction (EBSD) helps us to find uniform area as MEMS material. The ${\gamma}-TiAl$ has two different lamellar structures ${\gamma}/{\alpha}2-Ti_3Al$ phase which have shows $\{111\}{\gamma}//\{0001\}{\alpha}2$ plane indexing. The micro size testing specimen was successfully made by this structural relation. Interlamellar structure specimen averagely show $20{\sim}25%$ lower fracture toughness value compare with translamellar specimens Moreover micro fracture surface and micro crack progress were observed.

• Nuclear Engineering and Technology
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• 제44권7호
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• pp.791-798
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• 2012

Since standardized fracture test specimens cannot be easily extracted from in-service components, several alternative fracture toughness test methods have been proposed to characterize the deformation and fracture resistance of materials. One of the more promising alternatives is the local approach employing the SP(Small Punch) testing technique. However, this process has several limitations such as a lack of anisotropic yield potential and tediousness in the damage parameter calibration process. The present paper investigates estimation of ductile fracture resistance(J-R) curve by FE(Finite Element) analyses using an anisotropic damage model and enhanced calibration procedure. In this context, specific tensile tests to quantify plastic strain ratios were carried out and SP test data were obtained from the previous research. Also, damage parameters constituting the Gurson-Tvergaard-Needleman model in conjunction with Hill's 48 yield criterion were calibrated for a typical nuclear reactor material through a genetic algorithm. Finally, the J-R curve of a standard compact tension specimen was predicted by further detailed FE analyses employing the calibrated damage parameters. It showed a lower fracture resistance of the specimen material than that based on the isotropic yield criterion. Therefore, a more realistic J-R curve of a reactor material can be obtained effectively from the proposed methodology by taking into account a reduced load-carrying capacity due to anisotropy.

• 대한기계학회논문집A
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• 제30권3호
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• pp.269-278
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• 2006

This paper proposes slip line fields for bending of unequally notched specimens in plane strain that have a sharp crack in one side and a sharp V-notch in the other side. Depending on the back angle, two slip line fields are proposed, from which the limit moment and crack tip stress fields are obtained as a function of the back angle. Excellent agreement between slip line field solutions with those from detailed finite element limit analysis based on non-hardening plasticity provides confidence in the proposed slip line fields. One interesting point is that, for the unequally notched specimen, the difference between the crack tip triaxial stress for tension and that for bending increases significantly with increasing the back angle. This suggests that such a specimen could be potentially useful to investigate the crack tip constraint effect on fracture toughness of materials. In this respect, the possibility of designing a new toughness testing specimen with varying crack tip constraint is discussed.

• Journal of Welding and Joining
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• 제34권6호
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• pp.16-19
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• 2016

Needs for structural integrity procedure such as BS 7910, the nuclear industry document R6 Rev.4 and the European FITNET procedure are being increased in industry. Especially, BS 7910 allows metallic structures to be assessed on the basis of fracture mechanics analysis rather than strict adherence to design and fabricated codes. This study is to propose the flaw assessment to judge the toughness level of welding consumables at the development stage. The FCA welding consumables with YP 690MPa and CTOD over 0.25 mm have been developed and its allowable weld flaw size considering actually applied environment has been evaluated. Since the estimated allowable defect size is sufficiently detectable in nondestructive testing, the toughness of the developed material is judged to be appropriate and no problem in securing the structural integrity.

• 폴리머
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• 제24권3호
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• pp.326-332
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• 2000

유리섬유/불포화 폴리에스터 복합재료에서 섬유에 처리된 사이징제가 복합재료의 최종 물성에 미치는 영향을 상온에서의 접촉각 측정을 통해 고찰하였다. 본 연구에서는 폴리비닐알코올, 폴리에스터, 그리고 에폭시계 사이징제를 사용하여 유리섬유의 표면을 처리하였으며 각각의 물성을 비교하였다. 유리섬유의 접촉각은 증류수와 diiodomethane을 젖음액으로 사용하여 Washburn식을 기본으로 한 wicking법으로 측정하였다. 결과적으로 접촉각 측정에 의해 구한 표면자유에너지는 에폭시계 사이징제로 치리된 유리섬유에서 최대값을 나타내었다. 복합재료의 층간 전단 강도 (ILSS)와 파괴 인성 ( $K_{IC}$ )의 측정 결과로부터 사이징제의 처리에 따라 계면 결합력이 증진되며 결과적으로 복합재료의 기계적 강도가 증가함을 알 수 있었다. 이것은 복합재료에서 유리섬유의 표면 자유에너지 증가에 기인한다고 사료된다.

• Journal of Welding and Joining
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• 제31권6호
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• pp.50-57
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• 2013

Characterization of microstructures and cryogenic mechanical properties of electro beam (EB) welds between cast and forged Inconel 718 superalloys has been investigated. Optimal EBW condition was found in the beam current range of 36~39 mA with the constant travel speed of 12 mm/s and arc voltage of 120 kV for 10 mm-thick specimens. Electron beam current lower than 25 mA caused to occur the liquation microfissuring in cast-side heat affected zone (HAZ) of EB welds. The HAZ liquation microfissure was found on the liquated grain boundaries with resolidified ${\gamma}/Laves$ and ${\gamma}/NbC$ eutectic constituents. EBW produced welds showing a fine dendritic structure with relatively discrete Laves phase due to fast cooling rate. After post weld aging treatment, blocky Laves phase and formation of ${\gamma}^{\prime}+{\gamma}^{{\prime}{\prime}}$ strengtheners were observed. Presence of primary strengthener and coarse Laves particles in PWHT weld may cause to reduce micro-plastic zone ahead of a crack, leading to a significant decrease in Charpy impact toughness at $-196^{\circ}C$. Fracture initiation and propagation induced by Charpy impact testing were discussed in terms of the dislocation structures ahead of crack arisen from the fractured Laves phase.

• 대한금속재료학회지
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• 제47권12호
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• pp.797-810
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• 2009

A study was made of the effects of a Sn addition on the microstructure and microfracture mechanism of squeeze cast AZ51-xSn magnesium alloys. Microstructural observation, in situ fracture testing, and fractographic observations were conducted on these alloys to clarify the microfracture process. The microstructural analyses indicated that $Mg_2Sn$ particles as well as $Mg_{17}Al_{12}$ particles precipitated mainly along the solidification cell boundaries; the volume fraction of these hard particles increased as the amount of added Sn increased, with increased the strength. From in situ fracture observations of the AZ51-7Sn alloy, coarse precipitates located on the cell boundaries worked as easy crack propagation sites and caused abrupt intercellular fracturing. On the other hand, the overall fracture properties of the AZ51-3Sn alloy improved because crack propagation proceeded into the Mg matrix rather than into the cell boundaries as twins developed actively, as confirmed by an R-curve analysis. These findings suggest that the addition of 3~5 wt.% Sn is effective in improving both the tensile and fracture properties on the basis of well-developed twins, the blocking of crack propagation, and crack blunting.

• Journal of Welding and Joining
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• 제5권1호
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• pp.73-80
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• 1987

During PWHT, it is well known that residual stress in weld HAZ is one of the reasons for PWHT embitterment. In case of static loading, it was experimentally found that fracture toughness of weld HAZ was dependant upon PWHT conditions. However, the effects of PWHT on fatigue behavior are not clearly verified. Therefore, in this paper, the effects of heating rate PWHT conditions and residual stress simulated in weld HAZ of Cr-Mo steel on fatigue crack propagation behavior were evaluated by fatigue Testing and SEM observation. The obtained results are summarized as follows; 1. Applied stress($10 Kgf/mm^2$) in weld HAZ during PWHT tneded to decrease fatigue strength and to increase fatigue crack growth rate. 2. Applied stress and slow heating rate of 60.deg. C/hr during PWHT contributed to precipitin of impurity elements as well as carbide, which promoted the fatigue crack growth. 3. Fatigue crack growth rate decreased at the heating rate of 220.deg. C/hr in contrast with 600.deg. C/hr and 60.deg. C/hr.

• Carbon letters
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• 제11권2호
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• pp.102-106
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• 2010

In this work, the effect of aminized multi-walled carbon nanotubes (NH-MWNTs) on the mechanical interfacial properties of epoxy nanocomposites was investigated by means of fracture toughness, critical stress intensity factor ($K_{IC}$), and impact strength testing, and their morphology was examined by scanning electron microscope (SEM). It was found that the incorporation of amine groups onto MWNTs was confirmed by the FT-IR and Raman spectra. The mechanical interfacial properties of the epoxy nanocomposites were remarkably improved with increasing the NH-MWNT content. It was probably attributed to the strong physical interaction between amine groups of NH-MWNTs and epoxide groups of epoxy resins. The SEM micrographs showed that NH-MWNTs were uniformly embed and bonded with epoxy resins, resulted in the prevention of the deformation and crack propagation in the NH-MWNTs/epoxy nanocomposites.

• Journal of Welding and Joining
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• 제33권1호
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• pp.72-79
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• 2015

Evaluation of fracture toughness of welded structures has a significant influence on the structural design. However the residual stresses is redistributed while the welded structures is cut for preparing specimens. This study investigated an effect of the welding residual stress redistribution on the impact absorption energy of Charpy specimen. SA516Gr70 steel plate by at the flux cored arc welding (FCAW) and gas tungsten arc welding(GTAW) was cutting. Specimens for Charpy impact testing were taken from the welded plate. Two material removal mechanisms (wire cutting and water jet) were used to make the specimens. Welding residual stress and redistribution residual stress were measured using the XRD (X-Ray Diffraction) method. The amount of redistribution of residual stress depends on the different material removal mechanism. Redistribution of residual stress of reduced the impact absorption energy by 15%.