• 제목/요약/키워드: Fractions as ratios

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홍삼유출액으로부터 Diaion HP-20 수지 흡착법에 의한 조사포닌의 분리 (An Isolation of Crude Saponin from Red-Ginseng Efflux by Diaion HP-20 Resin Adsorption Method)

  • 곽이성;경종수;김시관;위재준
    • 한국식품영양과학회지
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    • 제30권1호
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    • pp.1-5
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    • 2001
  • This study was carried out to isolate saponin compounds from red-ginseng efflux, which was produced during the industrial processing of red-ginseng from fresh ginseng. We isolated crude saponin from the efflux extract (moisture content 35.0%) by using Diaion HP-20 adsorption method. Non-saponin fraction, which was adsorbed on Diaion HP-20 resin, was removed by eluating with $H_{2}O$ and 25% spirit. Then crude saponin was eluated with 95% spirit, continuously. Saponin in the eluated fractions was confirmed by TLC analysis. Crude saponin isolated from red ginseng efflux extract contained 12.10% of saponin. whereas those of white ginseng and red-ginseng were 3.30 and 3.39%, respectively. Ginsenoside contents showed the highest contents kin crude saponin from red ginseng efflux extract. Expacilly, the ginsenoside-$Rb_{1}$ and Re showed the highest contents in red-ginseng efflux extract when compared with those of white ginseng and red ginseng crude saponins. And the other ginsenosides except ginsenoside-$Rb_{1}$ and -Re also showed the highest contents in red ginseng efflux extract. However, the ratio of PD saponin (Panaxadiol saponin: $Rb_{1}+Rb_{2}$+Rc+Rd) to PT saponin (panaxatriol: $Re+Rg_{1}$) showed almost the same level when compared with those of ginseng saponin fractions. Ratio of PD/PT from red ginseng efflux extract was 1.99. Ratios of PD/PT from white ginseng and red ginseng were 1.85 and 1.84, respectively. Saponin purity, which was calculated by ratio percent of total ginsenoside to curde saponin content, was 45.90%. In case of white ginseng and red ginseng, the purities were 35.50 and 36.00%, respectively. However, by PHLC analysis, we confirmed that crude saponin isolated from red ginsengs. It suggested that crude saponin isolated from red ginseng ellux also would be useful component as ginseng saponins.

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폴리프로필렌 섬유보강 콘크리트의 파괴특성 연구 (Fracture Characteristics of Polypropylene Fiber Reinforced Concrete)

  • Shin-Won Paik
    • 한국안전학회지
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    • 제12권4호
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    • pp.230-240
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    • 1997
  • 본 연구에서는 폴리프로필렌 섬유보강 콘크리트의 파괴특성을 알아보기 위해 Monofilament 섬유와 Fibrillated 섬유의 두 종류 폴리프로필렌 섬유를 선택하여 10$\times$10$\times$50 cm 보 시편을 만들었는데, 이때 사용된 두 종류의 섬유 길이는 19 mm이고, 섬유 혼입량은 0%, 1%, 2%, 3%로 하였으며, 초기균열 깊이의 영향을 알아보기 위해 초기 균열길이를 각 섬유 혼입량에 따라 1.5cm, 3.0cm, 4.5cm로 하여 실험을 수행하였다. 또한, 본 연구에서는 폴리프로필렌 섬유보강 콘크리트의 파괴특성을 규명하기 위해 보 시편에 대한 4 점 하중 휨시험을 통해 하중-하중점 변위 곡선을 각 시편에 대해 측정하였고, 이때 COD 게이지를 이용하여 하중-CMOD 곡선도 측정할 수 있었다. 이러한 실험결과를 통해, 섬유혼입량과 초기 균열 깊이에 따른 압축강도, 휨강도 및 휨인성, 응력확대계수, 파괴에너지 등이 규명되었다. 이러한 결과에 대한 분석으로부터 Fibrillated 폴리프로필렌 섬유가 Monofilament 섬유보다 연성 효과가 큰 것을 알 수 있었으며, 특히 하중-CMOD 곡선으로부터 계산되는 파괴에너지인 Jc가 믿을만한 파괴특성 인자임을 알 수 있었다.

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Mechanical buckling of FG-CNTs reinforced composite plate with parabolic distribution using Hamilton's energy principle

  • Tayeb, Tayeb Si;Zidour, Mohamed;Bensattalah, Tayeb;Heireche, Houari;Benahmed, Abdelillah;Bedia, E.A. Adda
    • Advances in nano research
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    • 제8권2호
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    • pp.135-148
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    • 2020
  • The incorporation of carbon nanotubes in a polymer matrix makes it possible to obtain nanocomposite materials with exceptional properties. It's in this scientific background that this work was based. There are several theories that deal with the behavior of plates, in this research based on the Mindlin-Reissner theory that takes into account the transversal shear effect, for analysis of the critical buckling load of a reinforced polymer plate with parabolic distribution of carbon nanotubes. The equations of the model are derived and the critical loads of linear and parabolic distribution of carbon nanotubes are obtained. With different disposition of nanotubes of carbon in the polymer matrix, the effects of different parameters such as the volume fractions, the plate geometric ratios and the number of modes on the critical load buckling are analysed and discussed. The results show that the critical buckling load of parabolic distribution is larger than the linear distribution. This variation is attributed to the concentration of reinforcement (CNTs) at the top and bottom faces for the X-CNT type which make the plate more rigid against buckling.

강섬유 보강 콘크리트의 조기 재령에서의 휨 인성 발현에 관한 연구 (Investigation of Flexural Toughness Development of Steel Fiber Reinforced Concrete at Early Ages)

  • 이창준;신성우
    • 한국안전학회지
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    • 제24권6호
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    • pp.103-110
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    • 2009
  • Since the mechanical properties of cement-based materials are time-dependent due to the prolonged cement hydration process, those of fiber reinforced concrete(FRC) may also be time-dependent. Toughness is one of important properties of FRC. Therefore, it should be investigated toughness development of FRCs with curing ages to fully understand the time-dependent characteristics of FRCs. To this end, the effect of curing ages on flexural toughness development of steel fiber reinforced concrete is studied. Three point bending test with notched beam specimen was adapted for this study. Hooked-end steel fiber(DRAMIX 40/30) was used as a fiber ingredient to investigate w/c ratio and fiber volume fraction effect on toughness development during curing. Three different water-cement ratios(0.44, 0.5 and 0.6) and fiber volume fractions(0%, 0.5% and 1%) were used as influence factors. Each mixture specimens were tested at five different ages, 0.5, 1, 3, 7 and 28 days. The study shows that flexure toughness development with age is quite different than other concrete material properties such as compressive strength. The study also shows that the toughness development trend correlates more closely to water/cement ratio than to fiber volume fraction.

Increase of Conjugated Linoleic Acid Level in Milk Eat by Bovine Feeding Regimen and Urea Fractionation

  • KIM, YOUNG JUN;KI WON LEE;HYONG JOO LEE
    • Journal of Microbiology and Biotechnology
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    • 제13권1호
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    • pp.22-28
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    • 2003
  • Increasing conjugated linoleic acid (CLA) content in dairy products has been a research Interest due to the potential health benefits resulted from consuming CLA. Attempts were made to obtain high level natural CLA containing fatty acid fractions from milk fat through bovine feeding of sunflower oil (SO) and urea fractionation. SO feeding changed the fatty acid profile of milk fat. increasing the CLA content five-fold at eight weeks of trial. Milk fat obtained from S0-fed cows was hydrolyzed to free fatty acids, which were then fractionated with urea at various ratios. The profiles of fatty acids were also greatly influenced by urea fractionation. Long-chain unsaturated fatty acids, Including CLA, were concentrated in milk fat after the fractionation, whereas saturated long-chain counterparts were eliminated. The highest level of CLA was achieved by the fractionation at 2:1 urea/fatty acid ratio (UFR2). CLA level was elevated 2.5-fold, and the Cl8:1/C18:0 fatty acid ratio was increased 120 times after the fractionation. The level of CLA in high CLA-milk fat (24mg/g fat) obtained from the feeding study was further increased through urea fractionation up to 52mg/g fat, 10 folds as high as CLA in the control milk fat (5mg/g fat).

A new higher-order shear and normal deformation theory for functionally graded sandwich beams

  • Bennai, Riadh;Atmane, Hassen Ait;Tounsi, Abdelouahed
    • Steel and Composite Structures
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    • 제19권3호
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    • pp.521-546
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    • 2015
  • A new refined hyperbolic shear and normal deformation beam theory is developed to study the free vibration and buckling of functionally graded (FG) sandwich beams under various boundary conditions. The effects of transverse shear strains as well as the transverse normal strain are taken into account. Material properties of the sandwich beam faces are assumed to be graded in the thickness direction according to a simple power-law distribution in terms of the volume fractions of the constituents. The core layer is still homogeneous and made of an isotropic material. Equations of motion are derived from Hamilton's principle. Analytical solutions for the bending, free vibration and buckling analyses are obtained for simply supported sandwich beams. Illustrative examples are given to show the effects of varying gradients, thickness stretching, boundary conditions, and thickness to length ratios on the bending, free vibration and buckling of functionally graded sandwich beams.

Free vibration of an annular sandwich plate with CNTRC facesheets and FG porous cores using Ritz method

  • Emdadi, Mohsen;Mohammadimehr, Mehdi;Navi, Borhan Rousta
    • Advances in nano research
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    • 제7권2호
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    • pp.109-123
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    • 2019
  • In this article, the free vibration analysis of annular sandwich plates with various functionally graded (FG) porous cores and carbon nanotubes reinforced composite (CNTRC) facesheets is investigated based on modified couple stress theory (MCST) and first order shear deformation theories (FSDT). The annular sandwich plate is composed of two face layers and a functionally graded porous core layer which contains different porosity distributions. Various approaches such as extended mixture rule (EMR), Eshelby-Mori-Tanaka (E-M-T), and Halpin-Tsai (H-T) are used to determine the effective material properties of microcomposite circular sandwich plate. The governing equations of motion are extracted by using Hamilton's principle and FSDT. A Ritz method has been utilized to calculate the natural frequency of an annular sandwich plate. The effects of material length scale parameters, boundary conditions, aspect and inner-outer radius ratios, FG porous distributions, pore compressibility and volume fractions of CNTs are considered. The results are obtained by Ritz solutions that can be served as benchmark data to validate their numerical and analytical methods in the future work and also in solid-state physics, materials science, and micro-electro-mechanical devices.

강섬유의 형상비와 혼입률에 따른 강섬유 보강 콘크리트 보의 역학적 특성 추정 모형 개발 (Development of Estimation of Model for Mechanical Properties of Steel Fiber Reinforced Concrete according to Aspect Ratio and Volume Fraction of Steel Fiber)

  • 곽계환;황해성;성배경;장화섭
    • 한국농공학회논문집
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    • 제48권3호
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    • pp.85-94
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    • 2006
  • Practially useful method of steel fiber for construction work is presented in this study. The most important purpose of this study is to develop a model which can predict mechanical behavior of the structure according to aspect ratio and volume fraction of steel fiber. Experiments on compressive strength, elastic modulus, and splitting strength were performed with self-made cylindrical specimens of variable aspect ratios and volume fractions. The experiment showed that compressive strength was not in direct proportion to volume fraction which doesn't seem to have great influence over compressive strength. However, splitting strength showed almost direct proportion to aspect ratio and volume fraction. Improvement of optimal efficiency was confirmed when the aspect ratio was 70. Experiments on flexural strength, fracture energy, and characteristic length were carried out with self-manufactured beams with notch. As a result, increases of flexural strength, fracture energy, and characteristic length according to increase of volume fraction tend to be prominent when aspect ratio is 70. The steel fiber improves concrete to be more ductile and tough. Moreover, regression analysis was the performed and predictable model was developed after determining variables. With comparison and analysis of suggested estimated values and measured data, reliance of the model was verified.

마이크로 역학기반 GFRP 원통형 적층 쉘 구조의 변위 해석 (Deflection Analysis of Laminated Composite Cylindrical Shell Structures Based on Micro-Mechanics)

  • 김규동;이상열
    • 복합신소재구조학회 논문집
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    • 제4권4호
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    • pp.15-21
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    • 2013
  • This study carried out finite element deflection analysis of cylindrical shell structures made of composite materials, which is based on the micro-mechanical approach for different fiber-volume fractions. The finite element (FE) models for composite structures using multi-scale approaches described in this paper is attractive not only because it shows excellent accuracy in analysis but also it shows the effect of the material combination. New results reported in this paper are focused on the significant effects of the fiber-volume fraction for various parameters, such as fiber angles, layup sequences, and length-thickness ratios. It may be concluded from this study that the combination effect of fiber and matrix, largely governing the dynamic characteristics of composite shell structures, should not be neglected and thus the optimal combination could be used to design such civil structures for better dynamic performance.

Investigation of thermal buckling properties of ceramic-metal FGM sandwich plates using 2D integral plate model

  • Salah, Fethi;Boucham, Belhadj;Bourada, Fouad;Benzair, Abdelnour;Bousahla, Abdelmoumen Anis;Tounsi, Abdeldjebbar
    • Steel and Composite Structures
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    • 제33권6호
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    • pp.805-822
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    • 2019
  • In this work, a simple four-variable integral plate theory is employed for examining the thermal buckling properties of functionally graded material (FGM) sandwich plates. The proposed kinematics considers integral terms which include the effect of transverse shear deformations. Material characteristics and thermal expansion coefficient of the ceramic-metal FGM sandwich plate faces are supposed to be graded in the thickness direction according to a "simple power-law" variation in terms of the "volume fractions" of the constituents. The central layer is always homogeneous and consists of an isotropic material. The thermal loads are supposed as uniform, linear, and nonlinear temperature rises within the thickness direction. The influences of geometric ratios, gradient index, loading type, and type sandwich plate on the buckling properties are examined and discussed in detail.