• Title/Summary/Keyword: Flux materials

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Flux pinning properties of rf-sputtered YBCO films with $BaZrO_3$ doping (스퍼터링법에 의한 $BaZrO_3$도핑 YBCO 박막의 자속고정 특성 연구)

  • Chung, K.C.;Kim, Y.K.;Wang, X.L.;Dou, S.X.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.374-374
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    • 2009
  • We have fabricated pure YBCO films and $BaZrO_3$ doped ones on $CeO_2$ buffered YSZ single crystal substrates using rf-sputtering method. In this work, pure YBCO and 2 vol% BZO doped YBCO target were used to investigate the flux pinning properties of BZO doped YBCO films compared to undoped ones. BZO nanodots within the superconducting materials was known to comprise the self-assembled columnar defects along the c-axis from the bottom of YBCO films up to the top surface, thus can be a very strong pinning sites in the applied magnetic field parallel to them. We will discuss the possibility of growing self-assembled columnar defects in the rf-sputtering method. It is speculated that BZO and YBCO phases can separate and BZO form nanodots surrounded by YBCO epitaxial layers and continuous phase separation and ordering between these two materials, which was well studied in Pulsed Laser Deposition method. For this purpose, some severe experimental conditions such as on-axis sputtering, shorter target-substrate distance, high rf-power, etc was adopted and their results will be presented.

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Cu Corrosion Test Method for Lead-Free Solders (무연솔더 동판부식 시험법 연구)

  • Kim, Mi-Song;Hong, Won Sik;Oh, Chul Min;Kim, Keun-Soo
    • Journal of Welding and Joining
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    • v.35 no.3
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    • pp.21-27
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    • 2017
  • A soldering temperature of ($235{\pm}3$) $^{\circ}C$ is described in ISO 9455-15 for the copper corrosion test. However, this temperature is not suitable for performing lead-free solder pastes. We evaluated the compatibility of a lead-free solder paste in the experimental conditions of (Liquidus temperature + ($35{\pm}3$)) $^{\circ}C$. Based on the results after a Cu corrosion test, a proper temperature for Pb-free soldering was (melting point+($35{\pm}3$)) $^{\circ}C$. Criteria used to evaluate corrosion due to discoloration of flux residue is described in ISO 9455-15, but a more quantitative evaluation standard is needed. In this study, experimental error level was estimated by analyzing flux residue after a corrosion test for 72, 500 hours of specimens using EDS analysis with acceleration voltage. It was determined that the copper area at the flux residue boundary is suitable for the EDS analysis area.

Evaluation of Morphology and Water Flux for Polysulfone Flat Sheet Membrane with Conditions of Coagulation Bath and Dope Solution (응고조와 도프조성에 따른 폴리술폰 평막의 모폴로지 및 수투과도 평가)

  • Woo, Seung Moon;Chung, Youn Suk;Nam, Sang Yong
    • Membrane Journal
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    • v.22 no.4
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    • pp.258-264
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    • 2012
  • In this study, to research effect of coagulation bath and composition of dope solution, polysulfone flat sheet membrane was fabricated by phase inversion method. PEG and PVP were used as additive. Concentration of polymer and additive, composition of coagulation bath was controlled to prepare flat sheet membrane. And then the morphology and water flux of prepared membrane were measured by FE-SEM and water flux testing apparatus. The highest value of water flux was measured at the membrane prepared under a 15 wt% PSF, 25 wt% PEG conditions, and water as coagulation bath. The pure water flux of the membrane composed of PSf/PEG was drastically decreased with increasing amount of DMAc. We confirmed that change of amount in additive and composition in coagulation bath influence the morphology and water flux performance of the membrane.

Green-Emitting Silicate Phosphor Under Long Wavelength Ultraviolet Prepared by High Temperature Flame Spray Pyrolysis (고온 화염분무열분해법에 의해 합성된 장파장 자외선 하에서의 녹색 발광 실리케이트 형광체)

  • Cho, Jung-Sang;Koo, Hye-Young;Lee, Sang-Ho;Kang, Yun-Chan
    • Korean Journal of Materials Research
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    • v.18 no.2
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    • pp.77-83
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    • 2008
  • Green-emitting $Ba_{1.468}Sr_{0.5}SiO_4\;:\;Eu_{0.012},\;Y_{0.02}$ phosphor powders under long-wavelength ultraviolet light were prepared via high-temperature flame spray pyrolysis from spray solutions with and without $NH_4Cl$ flux. The effects of the temperature of the diffusion flame and the $NH_4Cl$ flux on the morphologies, crystal structures and photoluminescence intensities of the $Ba_{1.468}Sr_{0.5}SiO_4\;:\;Eu_{0.012},\;Y_{0.02}$ phosphor powders were investigated. The phosphor powders obtained from the spray solution with the $NH_4Cl$ flux had higher photoluminescence intensities compared to phosphor powders obtained from the spray solution without the flux. The photoluminescence intensity of the phosphor powders obtained from the spray solution without the flux decreased as the flow rate of the fuel gas increased. On the other hand, the photoluminescence intensity of the phosphor powders obtained from the spray solution with the flux increased as the flow rate of the fuel gas increased. The difference of in the phase purity and morphology of the powders affected the photoluminescence intensities of the phosphor powders.

Burning Tests for Interior Flooring Materials (건축용 바닥재의 연소성능 시험)

  • Lee, Bong-Woo;Lee, Jang-Won;SaKong, Seong-Ho;Kim, Hee-Soo;Lee, Byoung-Ho;Kim, Hyun-Joong
    • Fire Science and Engineering
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    • v.22 no.2
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    • pp.30-37
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    • 2008
  • We have performed the inflammability test for various flooring materials through a radiant heat panel tester by using the specification KSISO 9239-1 (an examination method of flooring materials) that has been set as an international standard for the fire prevention means of interior flooring materials. We have measured the flame spread distance, critical heat flux and smoke density generated by the fire of various flooring materials while using the radiant heat panel tester. The measurement result has shown the burning characteristics different from each other by the respective flooring materials and we could see that the surface materials and construction elements influence greatly on the heat release and smoke generation. We could see that the evaluation method above is an important test method in evaluating the critical heat flux, smoke generation and flame spread distance that are Important factors in studying for fire risks and it is judged that setting and applying a fire evaluation method of flooring materials suitable for the domestic construction use would be relevant.

New Magnetic Porcelain Mmaterials using Isotropic Sr-ferrite Granules (등방성 Sr-페라이트 과립을 이용한 새로운 자성도자기 소지)

  • 조태식;정지욱
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.8
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    • pp.882-887
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    • 2004
  • The new magnetic porcelain materials have been studied by mixing magnetic St-ferrite powders with traditional porcelain materials before forming process. For the maintenance of magnetic characteristics after glaze firing process, the Sr-ferrite grains with the size of 1∼2 ${\mu}{\textrm}{m}$ were agglomerated as the isotropic granules with the size of 0.5∼2 mm. The high characteristics of magnetic porcelain materials were achieved at the following conditions; isotropic Sr-ferrite granules of 30 wt%, granule size of 1.4∼2 mm, and glaze firing temperature of $1250^{\circ}C$ in air The magnetic porcelain materials indicated the high magnetic properties, such as the remanent flux density of 240 G, the intrinsic coercivity of 3910 Oe, and the surface flux density of 178 G. The extraction properties of the magnetic tea cups were high compared to that of the traditional tea cups.

Recyling of Waste Materials for Iron Ore Sintering (제철소내 폐기물의 소결공정에서의 이용기술)

  • 문석민;이대열;정원섭;신형기
    • Resources Recycling
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    • v.3 no.3
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    • pp.12-20
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    • 1994
  • Difficulties lies on using the dust from iron making process as a raw material for sintering process mainly because of high amount of Zn or alkali content and its ultra fine characteristics. To eliminate these toxic influence, new fluxing materials were tested and could get a very successful results. This fluxing materials, Calcium-ferrite of magnesio-ferrite were made from various waste materials such as lime stone sludge, bag filter dust, waste EP dust and dolomite sludge by simple way of pre-sintering. Sintering behavior as a fluxing materials was revealed to be good in any aspects and new concept of total recycling system could be established.

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Hydrophilization of hydrophobic membrane surfaces for the enhancement of water flux via adsorption of water-soluble polymers

  • Kim, Ka Young;Rhim, Ji Won
    • Membrane and Water Treatment
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    • v.7 no.2
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    • pp.101-113
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    • 2016
  • In this study, to improve the water flux of porous hydrophobic membranes, various water-soluble polymers including neutral, cationic and anionic polymers were adsorbed using 'salting-out' method. The adsorbed hydrophobic membrane surfaces were characterized mainly via the measurements of contact angles and scanning electron microscopy (SEM) images. To enhance the durability of the modified membranes, the water-soluble polymers such poly(vinyl alcohol) (PVA) were crosslinked with glutaraldehyde (GA) and found to be resistant for more than 2 months in vigorously stirred water. The water flux was much more increased when the ionic polymers used as the coating materials rather than the neutral polymer and in this case, about 70% of $0.31L/m^2{\cdot}h$ (LMH) to 0.50 LMH was increased when 300 mg/L of polyacrylamide (PAAm) was used as the coating agents. Among the cationic coating polymers such as poly(styrene sulfonic acid-co-maleic acid) (PSSA_MA), poly(acrylic acid-comaleic acid) (PAM) and poly(acrylic acid) (PAA), PSSA_MA was found to be the best in terms of contact angle and water flux. In the case of PSSA_MA, the water flux was enhanced about 80%. The low concentration of the coating solution was better to hydrophilize while the high concentration inclined to block the pores on the membrane surfaces. The best coating condition was found: (1) coating concentration 150 to 300 mg/L, (2) ionic strength 0.15, (3) coating time 20 min.

Proposal of Potted Inductor with Enhanced Thermal Transfer for High Power Boost Converter in HEVs

  • You, Bong-Gi;Ko, Jeong-Min;Kim, Jun-Hyung;Lee, Byoung-Kuk
    • Journal of Electrical Engineering and Technology
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    • v.10 no.3
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    • pp.1075-1080
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    • 2015
  • A hybrid electric vehicle (HEV) powertrain has more than one energy source including a high-voltage electric battery. However, for a high voltage electric battery, the average current is relatively low for a given power level. Introduced to increase the voltage of a HEV battery, a compact, high-efficiency boost converter, sometimes called a step-up converter, is a dc-dc converter with an output voltage greater than its input voltage. The inductor occupies more than 30% of the total converter volume making it difficult to get high power density. The inductor should have the characteristics of good thermal stability, low weight, low losses and low EMI. In this paper, Mega Flux® was selected as the core material among potential core candidates. Different structured inductors with Mega Flux® were fabricated to compare the performance between the conventional air cooled and proposed potting structure. The proposed inductor has reduced the weight by 75% from 8.8kg to 2.18kg and the power density was increased from 15.6W/cc to 56.4W/cc compared with conventional inductor. To optimize the performance of proposed inductor, the potting materials with various thermal conductivities were investigated. Silicone with alumina was chosen as potting materials due to the high thermo-stable properties. The proposed inductors used potting material with thermal conductivities of 0.7W/m·K, 1.0W/m·K and 1.6W/m·K to analyze the thermal performance. Simulations of the proposed inductor were fulfilled in terms of magnetic flux saturation, leakage flux and temperature rise. The temperature rise and power efficiency were measured with the 40kW boost converter. Experimental results show that the proposed inductor reached the temperature saturation of 107℃ in 20 minutes. On the other hand, the temperature of conventional inductor rose by 138℃ without saturation. And the effect of thermal conductivity was verified as the highest thermal conductivity of potting materials leads to the lowest temperature saturations.

Fabrication of YAG : Er3+ powders for the single crystal growth according to the synthetic temperature and flux concentration (다양한 온도조건과 flux 첨가량에 따른 단결정 성장용 YAG : Er3+ 분말 제조)

  • Park, Cheol Woo;Kang, Suk Hyun;Park, Jae Hwa;Kim, Hyun Mi;Choi, Jae Sang;Kang, Hyo Sang;Shim, Kwang Bo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.25 no.4
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    • pp.166-171
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    • 2015
  • In this study, using solid-state and flux, $Y_3Al_5O_{12}:Er^{3+}\;(YAG:Er^{3+})$ powders were successfully synthesized at low temperatures. To analyze the crystallinity of powders according to the synthesis or non-synthesis of powders and powder calcination temperatures, X-ray diffraction (XRD) was measured. In the case of pure YAG, when YAG was analyzed using the general solid-phase method, it was calcined for 12 hours at $1400^{\circ}C$ and pure YAG phase could be obtained. But when $BaF_2$ was added to YAG, YAG was synthesized at lower temperature (1000^{\circ}C$). It was thus found that the synthesis temperature could be lowered by about $400^{\circ}C$. Also, when BaF2 with an optimal concentration was added to $YAG:Er^{3+}$, the particle shape and size according to synthesis temperatures were surveyed, and corresponding luminous intensity was discussed.