• Title/Summary/Keyword: Floating zone technique

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Single Crystal Growth of $Y_3Fe_5O_{12}$ by the Traveling solvent Floating Zone(TSFZ) Method (Traveling solvent Floating Zone법에 의한 $Y_3Fe_5O_{12}$단결정 육성)

  • 이동주;신건철
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.1 no.1
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    • pp.39-50
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    • 1991
  • Single crystals of yttrium iron garnet $(YIG:Y_3Fe_5O_{12})$have been grown by a modified floating zone crystal growth technique(Traveling Solvent Floating Zone, TSFZ method) using an infrared radiation convergence type heater. A series of evaluations for the resulting YIG single crystals were carried out. The grown crystals are 5~6mm in diameter and 15~35mm in length. The conditions of single crystal growth were as follows; growth rate 1mm/h, rotation rate 30rpm, gas flow rate 0.2 1/min., zone aspect ratio 1, convexity of interface 0.29, respectively.

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Investigation of crystallinity and microstructure of $YMnO_3$ single crystal grown by floating zone method

  • Cho, N.T.;Kwon, D.H.;Shin, J.H.;Ahn, C.I.;Shim, K.B.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.13 no.4
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    • pp.168-171
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    • 2003
  • $YMnO_{3}$ single crystals have been grown by a floating zone technique and the optimal growth conditions were investigated. Their crystallinity and microstructure were characterized by the chemical etch pit patterns, their distribution and the compositional difference depending on the G value. In particular, the microstructural feature was interpreted in terms of compositional deviation along radial direction on (1010) growth plane.

Tunability of Ba(Ti0.92Zr0.08)O3 Polycrystal Grown on Ceramic Seed by Floating Bone Technique (세라믹스 종결정 위에 Floating Zone Technique 법으로 성장한 Ba(Ti0.92Zr0.08)O3 다결정의 Tunability)

  • Hwang, Ho-Byong
    • Journal of the Korean Ceramic Society
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    • v.41 no.10 s.269
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    • pp.771-776
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    • 2004
  • [ $Ba(Zr_{0.08}Ti_{0.92})O_3$ ] polycrystal was grown by floating zone technique with two ellipsoidal mirrors using the $8\%$of Zr-modified BZT ceramics as both a feed rod and a seed crystal. In order to study the annealing effect, a part of the grown crystal was sliced and annealed in the oxygen atmosphere at $1,200^{\circ}C$ for 10 h. The dielectric constant and loss at 10 kHz, 100 kHz, and 1 MHz were measured in the temperature range between $-100^{\circ}C$ and $150^{\circ}C$ to investigate the dielectric properties of the grown polycrystal. The electric-field dependence of the dielectric constant at 10 kHz and 100 kHz was studied by measuring the dielectric constants as a function of the biased-electric fields which ran from -15 kV/cm to 15 kV/cm. Due to the effect of annealing in the oxygen atmosphere, the electric-field tunability of dielectric constants increased from $47.5\%$ to 5 to and the figure of merit for this material from 39.6 to 46.4. Since the figure of merit can be increased to more than 46.4 by increasing the maximum value of the biased-electric fields to more than 15 V/cm, this material nay have a possibility for applications in microwave tuning devices at room temperature.

The Design Development on the Mooring System of a Floating Barge Positioned in the Shallow Water Zone (천해역에 위치한 바지형 부유체의 계류시스템 설계)

  • Kim, Young-Bok
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.27 no.5
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    • pp.364-371
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    • 2015
  • This study is aimed to develop the dynamic analysis technique for a floating aquaculture in a shallow water region under the harsh sea condition. In case of the installation region to transform from a coastal area to the offshore area, the influence of sea bed with sea waves on the mooring lines was announced to be significant by other authors. In this study, the numerical tool was developed to solve dynamic behavior of the floating barge coupled with mooring lines in a shallow zone of the sea considering the influence of sea bed on the floating system.

Annealing Effect and Tunability of BaZr0.08Ti0.92O3 Polycrystal Grown in N2 Gas Atmosphere by Floating Zone Technique (Floating Zone Technique법으로 질소분위기 하에서 성장한 BaZr0.08Ti0.92O3 다결정의 Tunability 및 열처리 효과)

  • Hwang, Ho-Byong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.11
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    • pp.1178-1185
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    • 2004
  • In the atmosphere of $N_2$ gas, BaZ $r_{0.08}$ $Ti_{0.92}$ $O_3$ polycrystal was grown by floating zone technique using BaZ $r_{0.08}$ $Ti_{0.92}$ $O_3$ ceramics as a feed and SrTi $O_3$(1l0) single cystal as a seed. The dielectric constant and loss at 10 kHz, 100 kHz, and 1 MHz for the as-grown sample were measured as a function of temperature in the temperature range between -10$0^{\circ}C$ and 150 $^{\circ}C$ to find a dielectric peak with frequency dispersion at Curie point. The hysteresis loop showed that the grown sample had very small polarization which was 0-0.01 $\mu$C/$\textrm{cm}^2$ for the applied dc-electric fields from -7 kV/cm to +7 kV/cm. However, the normal hysteresis loop was appeared after oxygen annealing. The electric-field dependence of the dielectric constant for both the as-grown and the post-annealed samples was studied by measuring the dielectric constants as a function of the biased-electric fields and their tunability was figured out from it at room temperature(27 $^{\circ}C$) and cryotemperature( -73$^{\circ}C$). Tunability for the as-grown sample was 51 % and the figure of merit 20.4 at 10kHz with the biased electric-field of 12 kV/cm. The tunability for the grown sample may be increased up to 80 % if the electric field of 25 kV/cm is applied. Tunability for the post-annealed sample was 41 % and the figure of merit 10.3 at 10 kHz with the biased electric-field of 12 kV /cm. Post-annealing improved the crystallinity of the as-grown sample but decreased its tunability.ability.

Growth of $MgTiO_3 $ Single Crystals by the Floating Zone Method (F.Z,법에 의한 Mg $TiO_3 $단결정 육성)

  • Jang, Yeong-Nam;Kim, Mun-Yeong;Bae, In-Guk
    • Korean Journal of Crystallography
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    • v.1 no.1
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    • pp.29-34
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    • 1990
  • Single crystals of the peritectic compound MgTiO3 up to 8 m diameter and 100mm long along the [1010] axis. were yon by the travelling solvent floating zone technique using a halogen lamp image furnace. The grown single crystal. which shows a solid solution range at high temperature, exsolves TiO2 component if it is annealed very slowly to room termperature. Grown boules were black but become translucent with pinkish brown color after tempering at 1100 t for 8-10 hours in oxygen atmosphere and showed distint chatoyancy along the (0001) plane. The grown crystal can be used as a new modified cat's eye gemstone. The optimum conditions were as follows ;Sintering temperature of the charge rod, 1300℃ the growth rate, 2-2.5mmh and the composition of the charge rod in molar ratio. MgO : TiO2 : 1:1.05.

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Analysis of Behavior of Train and Track at Transition Zone between Floating Slab Track and Conventional Concrete Slab Track (플로팅 슬래브궤도와 일반 콘크리트궤도 접속부에서의 열차 및 궤도의 거동 분석)

  • Jang, Seung-Yup;Yang, Sin-Chu;Park, Man-Ho;Joh, Su-Ik
    • Proceedings of the KSR Conference
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    • 2009.05b
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    • pp.379-384
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    • 2009
  • It is of great importance to assure the running safety and ride comfort in designing the floating slab track for the mitigation of train-induced vibration. In this paper, for this, analyzed are the system requirements for the running safety and ride comfort, and then, the behavior of train and track at the transition zone between the floating slab track and the conventional concrete slab track according to several main design variables such as spring constant, damping coefficient, spacing and arrangement of isolators and slab length, using the dynamic analysis technique considering the train-track interaction. The results of numerical analysis demonstrate that the discontinuity of the support stiffness at the transition results in a drastic increase of the vertical vibration acceleration of the train body, wheel-rail interaction force, rail bending stress and uplift force. The increase becomes higher with the decrease of the spring constant of isolators and the increase of the isolator spacing, but the damping ratio does not significantly affect the behavior of train and track at the transition. Therefore, to assure the running safety and ride comfort, simultaneously increasing the effectiveness of vibration isolation, it is effective to minimize the relative vertical offset between the floating slab and the conventional track slab by adjusting the spring constant and spacing of isolators at the transition.

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Controlling striated structure in Pt with RF zone refining method (백금 결정 성장시 줄무늬 구조 제어)

  • ;;J. Vuillemin
    • Journal of the Korean Vacuum Society
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    • v.5 no.4
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    • pp.387-390
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    • 1996
  • The study has been performed that the high purity of platinum crystal was grown by rf floating zone refined technique. Direct electric current was also present to examine the controlling striated structure during the sample grown. It has been proved that current and orientation could affect suppression of the striation structure in Pt. Substructure in Pt was thermally unstable and was able to be removed by the annealing technique.

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High-Strain-Rate Deformation of Fe-6.5wt.%Si Alloys using a Split Hopkinson Pressure Bar Technique (홉킨슨 압력봉법을 이용한 Fe-6.5wt.%Si 합금의 고변형률속도 거동)

  • Yoon, Young-Ki;Yoon, Hi-Seak;Umakoshi, Yukichi;Yasuda, Hiroyuki Y.
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.7
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    • pp.1073-1081
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    • 2001
  • Many researches have published numerous papers about the high-strain-rate obtained from Split Hopkinson Pressure Bar(SHPB) tests. And 6.5wt%Si steel is widely known as an excellent magnetic material because its magnetostriction is nearly zero. Single crystals are prepared by the Floating Zone(FZ) method, which melts the alloy by the use of a high temperature electron beam in a pure argon gas condition. In this paper, the fracture behavior of the poly crystals and single crystals (DO$_3$phase) of Fe-6.5wt%Si alloy by SHPB test is observed. The comparison of high-strain-rate results with static results was done. Obtained main results are as follows: (1) Fe-6.5wt%Si alloy has higher strength at high-strain-rate tensile. SHPB results of polycrystal are twice as high as static results. (2) From the fractography, the cleavage steps are remarkably reduced in the SHPB test compared with the static test.