• Archives of Pharmacal Research
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• v.6 no.2
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• pp.103-108
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• 1983

Such sulfur-containing drugs as chlorpromazine, sulfonamides and thiazides were determined by gas chromatography with flame photometric detector (FPD) and flame ionization detector (FID). 0.6% QF-1 or 3% SE-30 on Chromosorb WAWDMCS were found suitable for drugs listed above. In the experimental conditions given maximum response the FPD response and the response ratio of FPD increased with the number of sulfur atom per molecule. It was possible to obtain a linear calibration curve from $10^{-9}$ / mole to $2{\times}10^{-8}$ / mole and to analyze variety of sulfur drugs by the calibration curve of one sulfur standard.

• YAKHAK HOEJI
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• v.22 no.3
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• pp.157-162
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• 1978

Total organic carbon(TOC) can be determined by means of combustion and flame ionization detector. The principle of string method is that a sample acidified to pH2 and transferred into combustion tube by string is oxidized with air. Another combustion tube method is that organic compounds are oxidized in the combustion tube charged with CuO and cobalt asbestos after the acidified sample is injected directly by microsyringe. Carbon dioxide evolved was reduced under specially treated nickel catalyst and hydrogen, the methane produced was detected by flame ionization detector. Linear relationship was found between concentration and the peak height by the string method. The peak area in the case of combustion tube method is in the range of 1-200ppm. The coefficient of variation by string method was 2.3% and that by combustion tube method was 1.8%. The lower detectable limit was about 10mol. Advantages of the latter are simplicity, sensitivity and reproducibility. TOC in contineous stream can also be determined automatically by means of the string method.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.28 no.1
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• pp.88-95
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• 2014

The infrared, flame detector uses to detect fire situation from the characteristics of fire sources radiant energy. But it is able to malfunction on account of susceptible to interference of various surrounding waves. This paper is designed 6 independent PCB-boards to minimize the closed loops of siginal circuit. Also considering the interaction of electric and magnetic fields, this paper is designed protecting circuit of current and voltage output to reduced electromagnetic interference. And this paper is improving electromagnetic susceptibility by ferrite bid, capacitor filter and grounding circuits.

• Journal of Mechanical Science and Technology
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• v.19 no.12
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• pp.2197-2204
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• 2005

The combination of Gas chromatography (GC) for separation and Flame Ionization Detection (FID) for detection and identification of the components of a mixture of compounds is a fast and strongly proved method of analytic chemistry. The objective of this research was to design a combined High-speed miniature screening Gas chromatograph along with a Flame Ionization Detector for quick, quantitative and qualitative analysis of gas components. This combined GC-FID system is suitable to detect the volatile and semi-volatile hydrocarbons present in a gas mixture. The construction made it less expensive, easy to use and movable. The complete gas path was developed. On/off valves, temperature and flow sensors and their interface electronics were used for controlling purpose. A Microcontroller was programmed to measure the temperature and gas flow using the sensors and to control and regulate them using the electronics and valves. A pocket PC with its touch screen served as a user interface for the system. Software was developed for the pocket PC, which makes the communication possible with the Microcontroller. The system parameters can be indicated in the Pocket PC as simple text and also the analysis result can be displayed.

• Korean Journal of Food Science and Technology
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• v.37 no.5
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• pp.695-701
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• 2005

Efficient method was established for analysis of sulfur-containing compounds, including dimethyl disulfide, dimethyl trisulfide, 3-methyl thiophene, allyl mercaptan, 2-methyl-3-furanthiol, and methional. Sulfur-containing compounds were extracted through solid phase microextraction (SPME) or static headspace extraction (SH), and quantified using gas chromatograph equipped with pulsed flame photometric detector. All sulfur compounds, except ally mercaptan, showed higher detection response when dissolved in hexane than in dichloromethane. Linear range was $10^2-10^4$. Dimethyl trisulfide showed lowest limit of detection (LOD) value of 15.2 ppt, and methional highest of 70.5 ppb. Highest extraction efficiency for sulfur-containing compounds, particularly polar and small molecular weight compounds, was observed in 75mm carboxen/polydimethylsiloxane fiber, followed by 65mm polydimethylsiloxane/divinylbenzene and 100mm polydimethylsiloxane. Compared to SPME, less sulfur-containing compounds could be analyzed by SH, mainly due to its low extraction efficiency, although lower amount of artifacts were formed during sample preparation.

• Journal of the Korean Society of Safety
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• v.32 no.2
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• pp.38-45
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• 2017

This paper is an experimental study to find an optimal detection method for detecting fire early in a rack-type warehouse stored with goods. In this study, we constructed rack-type structure with the fourth floor of 13.5 m high and conducted fire experiments which were to measure flow of heat/smoke in rack-type structure and response time of fire detectors. The detectors used at experiments were fixed temperature type detectors, rate of rise detectors, photoelectric smoke detectors, air sampling smoke detectors and flame detectors. The used ignition sources are n-heptane fire for response of heat detection and cotton fire for response of smoke detection. The fixed temperature type detectors, rate of rise detectors and photoelectric detectors were installed to every rack level respectively. The results show that the rate of rise detector should be installed every 2 levels and photoelectric smoke detector should be installed every 4 levels for the early stage fire detection. Air sampling smoke detectors can detect fire early in response to control of sensitivity, but there is a problem in false alarm. The fixed temperature detector is not suitable for early stage fire detection in warehouse and flame detector not worked if flame is not visible, so it need to install combination with other detector.

• Fire Protection Technology
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• s.13
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• pp.18-26
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• 1992

This report is explained about operating principles, characteristices of flame detectors. Flame detector is designed to detect the UV (Ultraviolet) and IR (Infrared) rediation produced by flaming involving carbonaceous materials.

• YAKHAK HOEJI
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• v.28 no.1
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• pp.25-27
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• 1984

Some $\betha$-lactam antibiotics-penicillins and cephalosporins-were determined by gas chromatography (GC) with flame photometric detector (FPD) which was selective and sensitive to sulfur-containing compounds. Methyl ester derivatives of carboxyl group in $\betha$-lactam antibiotics were prepared using 0.5Mmethyl iodide in methylene chloride and were taken for gas chromatography with 0.9% or 0.6% QF-1 on Chromosorb WAW-DMCS. We have found that it is possible to determine methyl esters of $\betha$-lactam antibiotics by GC/FPD.

• Journal of Microbiology and Biotechnology
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• v.25 no.5
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• pp.704-708
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• 2015

For the analysis of multiple-reaction intermediates for long-chain dicarboxylic acid biotransformation, simple and reproducible methods of extraction and derivatization were developed on the basis of gas chromatography with flame ionization detector (GC-FID) instead of mass spectrometry. In the derivatization step, change of the ratio of pyridine to MSTFA from 1:3 to 9:1 resulted in higher peak intensity (p = 0.021) and reproducibility (0.6%CV) when analyzing 32 g/l ricinoleic acid (RA). Extraction of RA and ω-hydroxyundec-9-enoic acid with water containing 100 mM Tween 80 showed 90.4-99.9% relative extraction efficiency and 2-7%CV compared with those with hydrophobic ethyl acetate. In conclusion, reduction of the pyridine content and change of the extraction solvent to water with Tween 80 provided compatible derivatization and extraction methods to GC-FID-based analysis of longchain carboxylic acids.

• Fire Science and Engineering
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• v.23 no.3
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• pp.67-72
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• 2009

This paper is for response feature of fire detectors not only to analysis response feature of fire detector, but also to observe flame spread of inside-building and fire enlargement by using the row house which is supposed to be broken up. Many kinds of popular detectors such as heat type detector(differential type, fixed temperature type, Analogue type)and smoke type(light scattered type, Analogue type, single alarm type) were installed in the house in order to check for the change of temperature by installing of thermocouples. As a result, smoke detectors are better than heat detectors when it comes to making effective fire-detect system in the row house.