• Title/Summary/Keyword: Firing strength

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Effect of(Si+C) Content on the Strength of SiC-(Si+C) Sintered Bodies (SiC-(Si+C) 소결체의 강도에 미치는 (Si+C)첨가량의 영향)

  • 김은태;김완덕;최진영;우정인
    • Journal of the Korean Ceramic Society
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    • v.23 no.3
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    • pp.9-14
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    • 1986
  • $\beta$-SiC bonded SiC bodies were prepared from various conditions such as several compositions of(Si+C)/$\alpha$ -SiC ratio and different firing schedules and were respectively investigated compressive strength MOR and mi-crostructure. One firing schedule which produced the specimens that had $\beta$-SiC neck form with the highest strength was selected and experimented by each firing temperature. results obtained are as follows : 1) The amount of (Si+C) for th highest MOR of SiC-(Si+C) sintered body is 20wt% 2) By adding 20wt% content of (Si+C) and heating up to 1, 500 with soaking 3hrs respectively at 1,150$^{\circ}C$ 1,250$^{\circ}C$ 1,350$^{\circ}C$ and 1,400$^{\circ}C$ the highest MOR of fired specimen was resulted and its microstructure of ma-trix was composed of close $\beta$-SiC neck. 3) Microstructure of $\beta$-SiC were different greatly from each other by firing time and/or quantity of adding mix-ture and it was confirmed that they were composed of neck particle-like and heterogeneous texture. 4)$\beta$-SiC synthesis proceed rapidly at the temperature between 1,250$^{\circ}C$ and 1,350$^{\circ}C$ 5) All of the properties of 85 SiC-20(Si+C) specimen improved according to increasing temperature above 1,350$^{\circ}C$.

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Mechanical properties of zirconia after different surface treatments and repeated firings

  • Subasi, Meryem Gulce;Demir, Necla;Kara, Ozlem;Ozturk, A. Nilgun;Ozel, Faruk
    • The Journal of Advanced Prosthodontics
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    • v.6 no.6
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    • pp.462-467
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    • 2014
  • PURPOSE. This study investigated the influence of surface conditioning procedures and repeated firings on monoclinic content and strength of zirconia before cementation. MATERIALS AND METHODS. Sintered bar-shaped zirconia specimens were subjected to no surface treatment (control), air abrasion, or grinding (n=21). Their roughness was evaluated using a profilometer, and microscope analysis was performed on one specimen of each group. Then, 2 or 10 repeated firings (n=10) were executed, the monoclinic content of specimens was analyzed by X-ray diffraction, and a three-point flexural strength test was performed. Surface roughness values were compared using one-way analysis of variance (ANOVA) and Tukey honestly significant difference (HSD) tests, the monoclinic content values were tested using Kruskal-Wallis and Mann-Whitney U tests, and the flexural strength values were tested using two-way ANOVA and Tukey HSD tests (P=.05). Spearman's correlation test was performed to define relationships among measured parameters. RESULTS. Surface-treated specimens were rougher than untreated specimens and had a higher monoclinic content (P<.005), and the relationship between roughness and monoclinic content was significant (P<.000). Neither surface treatment nor firing significantly affected the flexural strength, but Weibull analysis showed that for the air-abraded samples the characteristic strength was significantly lower after the $10^{th}$ firing than after the $2^{nd}$ firing. CONCLUSION. After firing, a negligible amount of monoclinic content remained on the zirconia surfaces, and rougher surfaces had higher monoclinic contents than untreated surfaces. Multiple firings could be performed if necessary, but the fracture probability could increase after multiple firings for rougher surfaces.

Surface Coatings to Enhance Bonding Strength of Dental Titanium-Ceramic Restorative System (치과용 타타늄-세라믹 수복시스템의 결합강도 향상을 위한 표면 코팅)

  • Lee, Hae-Hyoung
    • Journal of the Korean Ceramic Society
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    • v.45 no.10
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    • pp.600-604
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    • 2008
  • Although titanium-ceramic systems have gained substantial interests in dental prosthetic field, bonding problem between porcelain and titanium has not been solved. Main obstacle in titanium-porcelain bonding is excessive oxidation of titanium during porcelain firing. The effects of several coating materials on the bonding strength of titanium-porcelain system were investigated in this study. RF sputtering and electroplating of platinum significantly increased the bonding strength of porcelain-titanium specimen. However, coatings of Ni-Au, Ir, and ceramics(zirconia and hydroxyapatite) did not showed a significant effect on bonding strength. Platinum might be a promising material for the protective layer of excessive oxidation of titanium during porcelain firing, resulting in increase in the bonding strength.

A Study on Sintering Behavior of 16 mol% CaO-84mol% $ZrO_2$ Solid Solution (16mol% CaO-84mol% $ZrO_2$ 고용체의 소결특성에 관한 연구)

  • 박금철;최영섭
    • Journal of the Korean Ceramic Society
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    • v.20 no.4
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    • pp.347-355
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    • 1983
  • A batch mixture was prepared as 16mol% CaO-84mol% $ZrO_2$ of regeant-grade powder. The monoclinic Zirconia powder had an average particle size of $9.24 \mu\textrm{m}$ and calcium carbonate powder had a reported purity of 99.7 weight percent and mean particle size of TEX>$24, 37<\mu\textrm{m}$. The specimens were fired at 1400, 1500, 1650 and $1750^{\circ}C$ for 0. 3, 5 and 7 hours respectively. After fired the specimens were investigated using Scaning electron microscopy. Density Porosity Compressive strength Modulus of rupture and Thermal expansion were measured X-ray diffration analysis was also carried out. The results are as follows ; 1) As the firing temperature or soaking time was increased firing linear shrinkage apparent density compressive strength and modulus of rupture increased but apparent porosity decreased, 2) Cubic and monoclinic Zirconia was found at $1400^{\circ}C$ and cubic Ziconia found above $1500^{\circ}C$ 3) The specimens fired at 140$0^{\circ}C$ without soaking display thermal expansion curves by monoclinic〓tetragonal transformation and no tranformation was found at $1400^{\circ}C$ for 5hrs and above $1500^{\circ}C$. 4) The lattice parameter had constant value of 5.1345 $\AA$ through all the ranges of firing temperature 5) The higher the firing temperature was or the longer the soaking time was the larger the grain size was.

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Effect of firing temperatures on alkali activated Geopolymer mortar doped with MWCNT

  • Khater, H.M.;Gawwad, H.A. Abd El
    • Advances in nano research
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    • v.3 no.4
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    • pp.225-242
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    • 2015
  • The current investigation aims to study performance of geopolymer mortar reinforced with Multiwalled carbon nanotubes upon exposure to $200^{\circ}C$ to $1000^{\circ}C$ for 2 hrs. MWCNTs are doped into slag Geopolymer mortar matrices in the ratio of 0.0 to 0.4, % by weight of binder. Mortar composed of calcium aluminosilicate to sand (1:2), however, binder composed of 50% air cooled slag and 50% water cooled slag. Various water / binder ratios in the range of 0.114-0.129 used depending on the added MWCNT, while 6 wt., % sodium hydroxide used as an alkali activator. Results illustrate reduction in mechanical strength with temperature except specimens containing 0.1 and 0.2% MWCNT at $200^{\circ}C$, while further increase in temperature leads to decrease in strength values of the resulting geopolymer mortar. Also, decrease in firing shrinkage with MWCNT up to 0.1% at all firing temperatures up to $500^{\circ}C$ is observed, however the shrinkage values increase with temperature up to $500^{\circ}C$. Further increase on the firing temperature up to $1000^{\circ}C$ results in an increase in the volume due to expansion.

Development of Ternary Inorganic Binder System for Manufacturing High-Functional Ceramic Molds and Core (고기능성 세라믹 주형 및 중자 제작을 위한 3원계 무기 바인더 시스템 개발)

  • Hye-Yeong Park;Geun-Ho Cho;Hyun-Hee Choi;Bong Gu Kim;Eun-Hee Kim;SeungCheol Yang;Yeon-Gil Jung
    • Korean Journal of Materials Research
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    • v.32 no.12
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    • pp.538-544
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    • 2022
  • In existing ceramic mold manufacturing processes, inorganic binder systems (Si-Na, two-component system) are applied to ensure the effective firing strength of the ceramic mold and core. These inorganic binder systems makes it possible to manufacture a ceramic mold and core with high dimensional stability and effective strength. However, as in general sand casting processes, when molten metal is injected at room temperature, there is a limit to the production of thin or complex castings due to reduced fluidity caused by the rapid cooling of the molten metal. In addition, because sodium silicate generated through the vitrification reaction of the inorganic binder is converted into a liquid phase at a temperature of 1,000 ℃. or higher, it is somewhat difficult to manufacture parts through high-temperature casting. Therefore, in this study, a high-strength ceramic mold and core test piece with effective strength at high temperature was produced by applying a Si-Na-Ti three-component inorganic binder. The starting particles were coated with binary and ternary inorganic binders and mixed with an organic binder to prepare a molded body, and then heat-treated at 1,000/1,350/1,500 ℃ to prepare a fired body. In the sample where the two-component inorganic binder was applied, the glass was liquefied at a temperature of 1,000 ℃ or higher, and the strength decreased. However, the firing strength of the ceramic mold sample containing the three-component inorganic binder was improved, and it was confirmed that it was possible to manufacture a ceramic mold and core via high temperature casting.

Effects of Composition of Porcelain Glages on the Strength of Porcelain (자기유약의 조성이 자기강도에 미치는 영향)

  • 김영상
    • Journal of the Korean Professional Engineers Association
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    • v.23 no.6
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    • pp.117-122
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    • 1990
  • The effect of firing on the development of strength of china with maturing range of a series of glaze that gave no defect on firing was observed in an electrical furnace and oil-fired kiln. The body formular is as follows (equation omitted), and it was applied to a selected china body. Porcelain glaze formular is in the following. (equation omitted) The result obtained is sumarized as follows : (1) It was found that the strength of porcelain increases when the A1$_2$O$_3$ moles of the glaze increses, and the strength of porcelain decreases when the SiO$_2$ moles of glaze decreases at 3.9-5.9 moles, and increases again when the SiO$_2$ moles increases at 5.9-7.9 notes. (2) It was found the most safe glaze is No. 25 glaze.

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Fabrication of Humidity Control Ceramics from Drinking-Water Treatment Sludge and Onggi Soil

  • Lee, Min-Jin;Lee, Hyeon-Jun;Kim, Kyungsun;Hwang, Hae-Jin
    • Journal of the Korean Ceramic Society
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    • v.53 no.3
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    • pp.362-366
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    • 2016
  • In this study, humidity control ceramics with good adsorption/desorption capabilities and high strength were fabricated from drinking-water treatment sludge (DWTS) and Onggi soil. The DWTS powder heat-treated at $800^{\circ}C$ and Onggi soil were mixed at weight ratios of 40:60, 50:50, 60:40, and 70:30 and fired at $800-1000^{\circ}C$. With increasing DWTS content, density and flexural strength increased. For the sample with a DWTS:Onggi soil weight ratio of 70:30, porosity and specific surface area decreased with increasing firing temperature, attributed to densification and grain growth at high firing temperatures. From the results obtained, a firing temperature of $800^{\circ}C$ is the optimum condition for fabricating humidity control ceramics with good adsorption/desorption capabilities and strength. The maximum adsorbed amount for the sample fired at $800^{\circ}C$ was $439g/m^2$.

Synthesis and Characterization of Cordierite Glass-Ceramics for Low Firing Temperature Substrate; (II) Properties of Cordierite Glass-Ceramics Containing CeO2 (저온소결 세라믹기판용 Cordierite계 결정화유리의 합성 및 특성조사에 관한 연구;(II) $CeO_2$를 첨가한 Cordierite계 결정화유리의 특성)

  • 이근헌;김병호;임대순;정재현
    • Journal of the Korean Ceramic Society
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    • v.29 no.10
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    • pp.827-835
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    • 1992
  • The effects of CeO2 on the properties of cordierite-based glass-ceramics and its applicability to low firing temperature substrate were examined. Glass-ceramics were prepared by sintering the glass powder compacts at 900~100$0^{\circ}C$ for 3 h. Density, bending strength, dielectric constant and thermal expansion coefficient of the glass-ceramics were measured as functions of CeO2 contents and sintering temperatures. By adding CeO2, dense glass-ceramics were obtained below 100$0^{\circ}C$. dielectric constant and bending strength were more dependent on the porosity of glass-ceramics containing 5 wt% CeO2, sintered at 100$0^{\circ}C$ for 3 h, were as follows; relative density is 95.3%, bending strength is 178$\pm$11 MPa, dielectric constant is 4.98$\pm$0.20 (at 1 MHz) and thermal expansion coefficient is 33.7$\times$10-7/$^{\circ}C$. Therefore, the glass-ceramics containing 5 wt% CeO2 appeared to be suitable for low firing temperature substrate of electronic devices.

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A study on the brazed bonding of alumina ceramic to aluminum in the air atmosphere (알루미나($Al_2O_3$)세라믹과 알루미늄(A1050)과의 대기중 브레이징 접합에 관한 연구)

  • 최영국;박성현;김윤해;김영식
    • Journal of Advanced Marine Engineering and Technology
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    • v.19 no.3
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    • pp.50-61
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    • 1995
  • In recent years, many ceramic researchers have discoved various methods of joining ceramic to metal. However, most of these joining methods are perfomed under vacuum and pressured circumstances. So, when we join ceramic to metal,the proceedings are very complicated and require a very high cost. The purpose of this study is to develop a new joining method of an alumina ceramic to an aluminum metal in air atmosphere. The joining condition, such as copper metallizing, nickel plating, brazing, etc. was investigated through the shear strength test of the trial joint. The results obtained from the above experimenta are summarized as follows : 1) In the case of the $Al_2O_3$/$Al_2O_3$joint, the shear strength of the joint was affected by the various foctor such as kaolin content, copper metallizing thickness, firing temperature, firing time. 2) The better shear strength of the $Al_2O_3$/Al joint was obtained when Ni plating was conducted under higher current density than existing plating condition. 3) The shear strength of the $Al_2O_3$/Al joint increases with the Ni plating thickness is confined to the range of this paper. 4) The shear strength of the thermal-shocked specimen($Al_2O_3$/Al joint) was far more deteriorated than that of the as-bonded specimen.

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