• Restorative Dentistry and Endodontics
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• v.26 no.5
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• pp.379-386
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• 2001

This study was performed to evaluate the sealing ability of various retrograde filling materials by using bacterial penetration and dye penetration test. One hundred and forty extracted human teeth with single, straight canals and mature apiece were collected and used for this study. All canals were instrumented using an engine driven Ni-Ti file (ProFile). After removing 3mm from the apex of tooth, a standardized 3mm root end cavity was prepared using an ultrasonic instrument. The 70 teeth were randomly divided into 7 groups : 6 groups for retrograde filling using Super-EBA, ZOE, Chelon-Silver, IRM, ZPC and amalgam. The 7th group was used as a negative control. Nail varnish was applied to all external root surfaces to the level of the reseated root ends to prevent lateral microleakages. The specimens were then sterilized in an ethylene oxide sterilizer for 24 hours. 2 mm of the reseated root was immersed in a culture chamber containing a Tripticase Soy Broth with a phenol red indicator. The coronal access of each specimen was inoculated every 72 hours with suspension of Proteus vulgaris. The culture media were observed every 24hours for color change indicating bacterial contamination. The specimens were observed for 4weeks. The remaining 70 teeth were submitted to a dye penetration test. The canals of all teeth were first sealed with AH26 and obturated using an Obtura II system. Root resection, root end preparation and retrograde filling was performed as above. All specimens were suspended in 2% methylene blue dye for 72 hours before being ion gitudinally split. The degree of dye penetration was then measured using a stereomicroscope at 10 magnification and evaluated. The results were as floows : 1. In the bacterial penetration, the degree of leakage was the lowest in the Super-EBA, followed by, in ascending order, ZOE, Chelon-Silver IRM and ZPC. The amalgam showed highest bacterial leakage of all(p<0.01). 2. In the dye penetration, the degree of microleakage was the lowest in the Chelon-Silver and Super-EBA, followed by, in ascending order, IRM, ZPC. The ZOE and amalgam showed the highest microleakage of all (p<0.05). These results suggested that the eugenol based cement, Super-EBA, have excellent sealing ability as a retrograde filling material.

• Journal of Conservation Science
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• v.36 no.6
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• pp.475-482
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• 2020

In this study, we synthesized rosin-based epoxy resin and manufactured two components adhesives and epoxy putty using this epoxy resin. This study manufactured main element of adhesives for enabling it to form epoxide group by letting epichlorohydrin react to maleic anhydride modified rosin, and used room temperature curing type triethylenetetramine for hardener. The ratio between main element and hardener of of manufactured adhesives was 100 : 20, and main element and hardener of filling material were manufactured as clay type by mixing them with filler. Manufactured undiluted adhesives and filling material showed very stable result in the adhesive strength (3.06 MPa) and ultraviolet irradiation, showing outstanding result comparing to existing restoration adhesives. And it is considered a material having reversibility as it was dissolved in organic solvents such as acetone and toluene after being hardened, which showed a result that solved part of possible problems caused by restoration. As a result of use and application of manufactured adhesives and filling material for actual wood crafts, they showed excellent results in workability, stability, removability etc., and this study confirmed that the material can be used for and applied to various fields.

• Maxillofacial Plastic and Reconstructive Surgery
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• v.32 no.3
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• pp.236-241
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• 2010

Purpose: The purpose of this retrospective clinical study was to monitor the outcomes of periapical surgery in periapically infected tooth with or without retrograde filling materials (MTA or IRM). Patients and Methods: A total of 85 teeth in 63 patients were included in the study between November 2004 and August 2008. Randomly, MTA or IRM was used as a retrograde filling material or only apical resection without retrograde filling. Teeth with advanced periodontal bone loss or presence of root fracture were excluded from the study. The patients were subjected to a minimum follow-up period of 12 months, with a mean of 17.1 months. Results: Successful healing was observed in 83.3% of the MTA-treated teeth, 80% of the IRM-treated teeth and 75% of the teeth which was not retrograde filling. Doubtful healing was seen 9.3% (MTA), 13.3% (IRM), 12.5% (no retro-filling). The success rate of upper incisors (92%) was higher than lower lincisor and molars (66.7% and 50%, respectively). Conclusion: In this study, periapical surgery including retrograde filling improves the prognosis. And, no statistically significant differences were found between retrograde filling materials (MTA or IRM).

• Journal of the Korea Academia-Industrial cooperation Society
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• v.21 no.2
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• pp.175-181
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• 2020

This paper suggests a proper hydraulic filling method in downtown areas. Road subsidence on roadways and sidewalks in downtown areas can result in vehicle damage and casualties. The representative cause of road subsidence is the fraudulent construction in nearby construction sites. A deficiency of excavation restoration causes approximately 25~49% of subsidence. This is performed by equipment or manpower. Hydraulic filling is used in backfilling narrow pipe conduits and spaces between structures. On the other hand, standard specifications and quality assurance standards regarding hydraulic filling principles and construction conditions are insufficient. Therefore, in-door model experiments on hydraulic filling principles, backfilling material, and compaction efficiency were performed. This paper suggests guidelines by investigating and analyzing construction status. In conclusion, thrown backfilling material has a particle size distribution and permeability coefficient as major factors, and detailed standards of the factors are suggested. To improve the compaction efficiency, 90% or more, compaction by the floor should be in units of 0.3m while ensuring a lower drainage layer. When an H-shape stabilizing pile is pulled out after filling, additional hydraulic filling should be in the disturbance range.

• Journal of Dental Rehabilitation and Applied Science
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• v.38 no.4
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• pp.213-221
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• 2022

Purpose: The efficacy of the amount of sealer in the root canal and two retreatment NiTi file systems in removing filling materials. Materials and Methods: Extracted premolars with a single root canal were selected for this study. After access opening and root canal preparation up to size #40/.06, the specimens were randomly divided into four groups. Gutta percha (GP) tapers of .06 or .04 were used for each group and filled using a single-cone filling technique with CeraSeal, a calcium silicate-based sealer. Each group was retreated either using the ProTaper Universal Retreatment System (PTUR) or the Hyflex Remover (HR). The time taken to remove the filling material, the amounts of apically extruded debris, and canal cleanliness were measured and compared. Results: The amount of sealer did not affect the efficiency when removing the filling materials. However, the filling material was removed faster in the HR group than in the PTUR group. Two types of NiTi files showed similar retreatment effects in the amounts of apically extruded debris and in the degree of canal cleanliness. Conclusion: The amount of sealer in canal filling had no significant effect on retreatability. Retreatment with HR removed filling materials is faster than PTUR. There was no difference in other removal efficiencies according to the type of retreatment NiTi file.

• Tunnel and Underground Space
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• v.24 no.6
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• pp.449-463
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• 2014

There are many case studies and application cases in abandoned mines for hydraulic filling method filled by slurry or paste form, but research on the pneumatic filling is not applied in Korea. The damage of steel pipe is occurred by wear due to the flow of filling material in the bent area of steel pipe in traditional pneumatic filling method. In this study, the new pneumatic filling method was developed using a newly devised improved nozzle to improve the above problem. The model test for mine filling was performed in the laboratory for the simulated accessible or inaccessible mine cavities, and the filling efficiency by the results obtained from the test was calculated. The filling efficiency was analyzed from the variation of outlet angle, feed rate and grain size of sand in model test of simulated accessible mine cavity. The superiority of improved pneumatic filling method was proved through the analysis of filling efficiency by the results obtained from each model tests of gravitational, traditional, and improved filling method in simulated inaccessible mine cavity.

• Journal of Korean Tunnelling and Underground Space Association
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• v.4 no.3
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• pp.195-205
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• 2002

Most tunnel damage such as cracks or leakage which exist in tunnel liner commonly, is caused by the cavities that exist behind the tunnel liner, through the tunnel safety inspections. These cavities were analysed to check if they affect the stability of tunnels. This study is on the development of the controlled low-strength and flowable filling material which an be applied to the cavity behind the tunnel lining. The backfilling material studied here is crushed sand and stone-dust which is in cake-state and is a by-product obtained in the producing process of aggregate. Varying the compound mixing ratio, laboratory tests of compression test and chemical analyses were carried out. In addition, the material was applied to an old tunnel for the performance assessment.

• Journal of the Architectural Institute of Korea Structure & Construction
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• v.34 no.6
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• pp.19-27
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• 2018

The stone pagoda structure is treated as a discontinuous masonry structure, and the contact surface characteristics between stones is a very important factor in the discontinuum behavior analysis. So, it is necessary to find out material and structural characteristics of stone contact surface to perform the structural analysis for safety evaluation. Accordingly, it is important to analyze the material properties of stone surface and secure the structural characteristics through various contact surface states. Therefore, in this study, various test specimens applying the filler between the surface roughness and the stone in the contact surface treatment technique of the stone pagoda were manufactured, and compression test and shear test were carried out. Also, we analyzed the material and structural characteristics of the stone contact surface through the comparison of experimental results.

• Restorative Dentistry and Endodontics
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• v.12 no.2
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• pp.17-23
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• 1987

The purpose of this study was to evaluate the sealing properties of endodontic cavity filling materials according to the time intervals after filling. Access cavities were prepared in extracted human premolar or molar teeth and filled with caviton, zinc oxide eugenol cement, zinc oxide eugenol cement with a base of gutta percha stopping and gutta percha stopping. After filling at the intervals of immediate, 2 days and 2 weeks the teeth were immersed for 2 weeks in 1% methylene blue solutions. Longitudinal sections were obtained from approximately center of teeth and the depth of dye penetration into the access cavities were observed by 10${\times}$macrolens. The following results were obtained. I. All the materials experimented showed varying depth of dye penetration. 2. Of the material tested, caviton showed the best marginal sealing qualities regardless of the time intervals after filling and the sealing properties of the gutta percha stopping was the worst. 3. Both in zinc oxide eugenol cement and zinc oxide eugenol cement with a base of gutta percha stopping, the fillings allowed to mature for 2 days in normal saline solution showed the best sealing properties and those with no maturing time revealed the worst sealing qualities. 4. The sealing qualities of zinc oxide eugenol cement with a base of gutta percha stopping revealed slightly lower depth of dye penetration than that of zinc oxide eugenol cements.

• Journal of Conservation Science
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• v.27 no.1
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• pp.115-121
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• 2011

A Urethane resin restoration material was made to be used in the restoration of stone cultural assets. The Urethane resin restoration material showed strong adhesive strength and tensile strength similar to epoxy recovery material, which had been mainly used for the recovery of stone cultural assets. The sealing property, anti-shrinking property and paint-ability of Urethane resin restoration material are also similar to existing epoxy system restoration materials. Especially, this Urethane resin restration material is expected to give permanence and continuous stability in the restoration of cultural assets made in stone by resolving the two big issues of existing epoxy recovery material, which are 'yellowing' and 'ir-reversibility'. This Urethane resin restration material had been directly applied as a filling material and adhesive and it was dissolved again. The Urethane resin, which had been used for the recovery, was able to be perfectly removed, which means that this Urethane resin recovery material has perfect reversibility. This Urethane resin restoration material also has enhanced convenience since user can adjust the working-life dependent on work environment. It is believed that this Urethane resin restoration material can also be used as a filling material or adhesive for other cultural assets made of ceramic or metal heritage, in addition to stone, since it has strong adhesive strength and tensile strength.