• Title/Summary/Keyword: Fiber blending ratio

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Tensile Behavior of Hybrid Fiber Reinforced Cement Composite According to the Hooked Steel Fiber and Polyvinyl Alcohol Fiber Blending Ratio and Strain Rate (후크형 강섬유와 폴리비닐알코올 섬유의 혼합 비율과 변형속도에 따른 하이브리드 섬유보강 시멘트복합체의 인장거동)

  • Son, Min-Jae;Kim, Gyu-Yong;Lee, Sang-Kyu;Kim, Hong-Seop;Nam, Jeong-Soo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.6
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    • pp.98-105
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    • 2017
  • In this study, the fiber blending ratio and strain rate effect on the tensile behavior of hybrid fiber reinforced cement composite was evaluated. Hooked steel fiber and polyvinyl alcohol fiber were used for reinforcing fiber. The fiber blending ratio of HSF+PVA were 1.5+0.5, 1.0+1.0 and 0.5+1.5vol.%. As a results, the tensile strength, strain capacity and fracture toughness of the hooked steel fiber reinforced cement composites were improved by the increase of the bond strength of the fiber and the matrix according to increase of strain rate. However, the tensile stress sharply decreased after the peak stress because of the decrease in the number of straightened pull-out fibers by micro cracks in the matrix around hooked steel fiber. On the other hand, PVA fiber showed cut-off fracture at strain rate $10^{-6}/s$ with multiple cracks. However, at the strain rate $10^1/s$, the multiple cracks and strain capacity were decreased because of the pull-out fracture of PVA fiber. The HSF1.5PVA0.5 shown the highest tensile strength because the PVA fiber suppressed the micro cracks in the matrix around the hooked steel fiber and improved the pull-out resistance of hooked steel fiber. Thus, DIF of strain capacity and fracture toughness of HSF1.5PVA were greatly improved. In addition, the synergistic response of fracture toughness was positive because the tensile stress was slowly decreased after the peak stress by improvement of the pull-out resistance of hooked steel fiber at strain rate $10^1/s$.

In-line Monitoring of Fluid-Bed Blending Process for Pharmaceutical Powders using Fiber Optics Probe and NIR Spectroscopy (광섬유-탐침과 근적외선(NIR) 분광기를 이용한 약제분말 유동층 혼합공정의 인라인 모니터링 연구)

  • Park, Cho-Rong;Kim, Ah-Young;Lee, Min-Jeong;Lee, Hea-Eun;Seo, Da-Young;Shin, Sang-Mun;Choi, Yong-Sun;Kwon, Byung-Soo;Bang, Kyu-Ho;Kang, Ho-Kyung;Kim, Chong-Kook;Lee, Sang-Kil;Choi, Guang-Jin
    • Journal of Pharmaceutical Investigation
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    • v.39 no.1
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    • pp.29-36
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    • 2009
  • Since the quality of final products is significantly affected by the homogeneity of powder mixture, the powder blending process has been regarded as one of the critical pharmaceutical unit processes, especially for solid dosage forms. Accordingly, the monitoring to determine a blending process' end-point based on a faster and more accurate in-line/on-line analysis has attracted enormous attentions recently. Among various analytical tools, NIR (near-infrared) spectroscopy has been extensively studied for PAT (process analytical technology) system due to its many advantages. In this study, NIR spectroscopy was employed with an optical fiber probe for the in-line monitoring of fluid-bed blending process. The position of the probe, the ratio of binary powder mixture, the powder size differential and the back-flush period of the shaking bag were examined as principal process parameters. During the blending process of lactose and mannitol powders, NIR spectra were collected, corrected, calibrated and analyzed using MSC and PLS method, respectively. The probe position was optimized. A reasonable end-point was predicted as 1,500 seconds based on 5% RSD value. As a consequence, it was demonstrated that the blending process using a fluid-bed processor has several advantages over other methods, and the application of NIRS with an optical fiber probe as PAT system for a fluid-bed blending process could be high feasible.

Polymer Electrolytes Based on Poly(vinylidenefluoride-hexafluoropropylene) and Cyanoresin

  • Lee, Won-Jun;Kim, Seong-Hun
    • Macromolecular Research
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    • v.16 no.3
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    • pp.247-252
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    • 2008
  • Lithium gel electrolytes based on a mixed polymer matrix consisting of poly(vinylidenefluoride-hexafluoropropylene) (PVDF-HFP) and cyanoresin type M (CRM) were prepared using an in situ blending process. The CRM used in this study was a copolymer of cyanoethyl pullulan and cyanoethyl poly(vinyl alcohol) (PVA) with a mole ratio of 1:1. The mixed plasticizer was ethylene carbonate (EC) and propylene carbonate (PC) with a volume ratio of 1:1. In this study, the presence of PVDF in the electrolytes helps to form a dimensionally stable film over a broad composition range, and decreases the viscosity. In addition, it provides better rheological properties that are suitable for the extrusion of thin films. However, the presence of HFP has a positive effect on generating an amorphous domain in a crystalline PVDF structure. The ionic conductivity of the polymer electrolytes was investigated in the range 298-333 K. The introduction of CRM into the PVDF-HFP/$LiPF_6$, complex produced a PVDF-HFP/CRM/$LiPF_6$ complex with a higher ionic conductivity and improved thermal stability and dynamic mechanical properties than a simple PVDF-HFP/$LiPF_6$, complex.

Evaluation of Recyclability at Varied Blending Ratios of Gable Top and Aseptic Brick Carton (상온보존팩과 냉장보존팩의 배합비율에 따른 재활용 특성 평가)

  • Seo, Jin Ho;Lee, Tai Ju;Lee, Dong Jin;Lee, Myoung Ku;Ryu, Jeong Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.47 no.6
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    • pp.123-129
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    • 2015
  • There are two kinds of cartons for beverage packaging, one is aseptic brick (AB) type and the other is gable top (GT). In this study, AB and GT were used as a raw material of recycled paper to investigate the recyclability at their varied blending ratios. Fiber consistency at pulping decreased as the blending ratio of AB increased. As a result, a lot of fines were generated from AB and flakes from GT increased because shear force in pulper decreased. Bulk of handsheets was more than $2.0cm^3/g$, and ISO brightness decreased as the blending ratio of AB increased. The best condition to recycle beverage cartons is to discriminate each cartons separately because of differences in the composition. However, there are problems such as the limit of the collection system and social costs. Therefore, it is assumed that the blending ratios of AB should be adjusted at less than 20% for effective recycling of beverage cartons.

Imparting Disperse and Cationic Dyeability to Polypropylene through Melt Blending

  • Teli M. D.;Adivarekar R. V.;Ramani V.Y.;Sabale A.G.
    • Fibers and Polymers
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    • v.5 no.4
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    • pp.264-269
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    • 2004
  • The present paper deals with improvement in disperse dyeablility as well as imparting of cationic dyeablility to difficultly dyeable polypropylene by a melt blending technique. Isotactic polypropylene (PP) was blended with fibre grade polybutylene terephthalate (PBT), cationic dyeable polyethylene terephthalate (CDPET) and polystyrene (PS), individually. The resulting binary blends were spun and drawn into fibres at draw ratio 2, 2.5, and 3. The compatibility of blends, structural changes of fibres in terms of X-ray crystallinity, relative crystallinity, sonic modulus, birefringence and thermal stability were examined. The blended fibres were found to be disperse dyeable by the conventional method of high temperature and high pressure dyeing. And this dye ability increased with increase in the level of substitution. PP/CDPET blend also exhibited dyeablility with cationic dyes in addition to that with disperse dyes. The optimum level of blending was predicted keeping in view of tenacity and thermal stability of melt blend fibres. The wash fastness properties of the dyed fibres were found to be of high rate.

Improvement of Heat Resistant of Adhesion between m-Aramid Sheet and Metal Materials using Epoxy/Phenolic Resin (Epoxy/Phenolic resin을 활용한 메타-아라미드 시트지와 금속 소재의 내열접착성 향상)

  • Kang, Chan Gyu;Chae, Ju Won;Choi, Seung Jin;Lee, Ji Su;Kim, Sam Soo;Lee, Sang Oh;Lee, Jaewoong
    • Textile Coloration and Finishing
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    • v.34 no.3
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    • pp.157-164
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    • 2022
  • This study tried to analyze the heat resistance properties by blending epoxy and phenolic resin in a certain ratio, and to analyze the adhesive properties at the time of metal-polymer hetero-adhesion by applying Epoxy-phenolic resin between a silicon steel sheet and m-aramid sheet, the viscosity, adhesive peel strength, and adhesive cross section were measured using a rotational rheometer, a tensile tester(UTM), and a field emission scanning electron microscopy(FE-SEM). The thermal stability and heat resistance were confirmed by measuring the mass loss according to the temperature increase using Thermogravimetric analysis(TGA). After blending with epoxy and Phenolic resin(1:0.25 ratio) curing at 110℃ for 10 min, high adhesive strength was improved more than 40% compared to the adhesive strength using epoxy alone. When the space between the silicon steel sheet and m-aramid sheet, which is created during curing of the E-P blend, is cured with a slight weight, it is possible to control the empty space and improve adhesion.

Development of Isolation Process of Barley Starch Using $\beta$-glucanase ($\beta$-Glucanase를 이용한 보리전분 분리공정의 개발)

  • 서호찬
    • Korean journal of food and cookery science
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    • v.15 no.3
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    • pp.238-243
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    • 1999
  • For the development of technique for isolation of naked barley starch from Youngsan variety, optimum conditions of the isolation process were investigated. The effect of blending was examined and the results showed that 29.7% starch yield was obtained by 6 times of blending. After the blending, the barley starch contained 3.2% protein, 0.7% fat, 0.4% fiber, 0.4% ash and 2.8% ${eta}$-glucan. The opitmum conditions of ${eta}$-glucanase treatment were studied and the results showed that the amount of ${eta}$-glucanase and barley flour-water ratio were 60,000 unit and 1/2, the optimum steeping temperature, pH were $45^{\circ}C$ and 6.5, respectively. The effect of alkali treatment which would be supposed to increase the yield and purity of the barley starch was also examined. 76.7% starch content was obtained by 2 hr of alkali treatment. After all the treatment of isolation process, the barley starch finally contained 0.2% protein and 0.1% ${eta}$-glucan.

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Strain Rate Effect on tensile properties of Hooked Steel Fiber and PVA Fiber hybrid reinforced cementitious composites (후크형 강섬유와 PVA섬유를 하이브리드 보강한 시멘트복합체의 인장특성에 미치는 변형속도의 영향)

  • Son, Min-Jae;Kim, Gyu-Yong;Lee, Sang-Kyu;Kim, Gyeong-Tae;Baek, Jae-Uk;Nam, Jeong-Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2018.05a
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    • pp.208-209
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    • 2018
  • In this study, the tensile properties of hybrid fiber reinforced cementitious composites under the high strain rate was evaluated. Experimental results, the HSF1.5PVA0.5 shown the highest tensile strength because the PVA fiber suppressed the micro cracks in the matrix around the hooked steel fiber and improved the pull-out resistance of hooked steel fiber. Thus, DIF of strain capacity and fracture toughness of HSF1.5PVA were greatly improved. Also, the fracture toughness was greatly improved because the tensile stress was slowly decreased after the peak stress by improvement of the pull-out resistance performance of hooked steel fiber at strain rate 101/s.

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Tensile Strength Characteristics of Steel Cord and PVA Hybrid Fiber Reinforced Cement-Based Composites (Steel Cord와 PVA 혼합섬유 보강 고인성 시멘트 복합체의 인장강도 특성)

  • Yun Hyun Do;Yang Il Seung;Han Byung Chan;Hiroshi Fukuyama;Cheon Esther;Moon Youn Joon
    • Proceedings of the Korea Concrete Institute Conference
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    • 2004.05a
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    • pp.18-21
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    • 2004
  • This paper discusses how steel cord and PVA hybrid fibers enhance the performance of high performance fiber reinforced cementitious composites (HPRFCC) in terms of elastic limit, strain hardening response and post peak of the composites. The effect of microfiber(PVA) blending ratio is presented. For this purpose flexure, direct tension and split tension tests were conducted. It was found that HFRCC specimen shows multiple cracking in the area subjected to the greatest bending tensile stress. Uniaxial tensile test confirms the range of tensile strain capacity from 0.5 to $1.5\%$ when hybrid fiber is used. The cyclic loading test results identified a unique unloading and reloading response for this ductile composite. Cyclic loading in tension appears not to affect the tensile response of the material if the uniaxial compressive strength during loading is not exceeded.

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An Experimental Study on Spalling Reduction Methode of Polymer Modified Cement Mortar Using Fiber Cocktail (섬유혼입 공법을 이용한 폴리머 시멘트 모르타르의 폭렬저감방안에 관한 실험적 연구)

  • Kim, Ji-Hoon;Ryu, Dong-Woo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.06a
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    • pp.96-97
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    • 2020
  • Polymer modified cement mortar (PCM) is commonly used as a repair material. However, in high-temperature environments such as fire, it is more likely to explode than cement mortar. The polymer is thermally decomposed at a high temperature to form a gas, and the gas remaining inside the structure increases the internal pressure to generate a burst. When an spalling occurs, the coating is peeled off and dropped, and high temperature is transmitted to the inside of the structure. In severe cases, even the reinforcing bar is exposed, which can lead to the collapse of the structural member due to severe loss of strength. In this study, in order to reduce spalling of PCM, a fiber mixing method was selected from the refractory method to find an appropriate blending ratio of fibers and polymers.

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