• Advances in nano research
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• v.10 no.1
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• pp.59-69
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• 2021

Electrospinning is a cost-effective and versatile method for producing submicron fibers. Although this method is relatively simple, at the theoretical level the interactions between process parameters and their influence on the fiber morphology are not yet fully understood. In this paper, the aim was finding optimal electrospinning parameters in order to obtain the smallest fiber diameter by using Taguchi's methodology. The nanofibers produced by electrospinning a solution of Thermoplastic Polyurethane (TPU) in Dimethylformamide (DMF). Polymer concentration and process parameters were considered as the effective factors. Taguchi's L9 orthogonal design (4 parameters, 3 levels) was applied to the experiential design. Optimal electrospinning conditions were determined using the signal-to-noise (S/N) ratio with Minitab 17 software. The morphology of the nanofibers was studied by a Scanning Electron Microscope (SEM). Thereafter, a tensile tester machine was used to assess mechanical properties of nanofibrous scaffolds. The analysis of DoE experiments showed that TPU concentration was the most significant parameter. An optimum combination to reach smallest diameters was yielded at 12 wt% polymer concentration, 16 kV of the supply voltage, 0.1 ml/h feed rate and 15 cm tip-to-distance. An empirical model was extracted and verified using confirmation test. The average diameter of nanofibers at the optimum conditions was in the range of 242.10 to 257.92 nm at a confidence level 95% which was in close agreement with the predicted value by the Taguchi technique. Also, the mechanical properties increased with decreasing fibers diameter. This study demonstrated Taguchi method was successfully applied to the optimization of electrospinning conditions for TPU nanofibers and the presented scaffold can mimic the structure of Extracellular Matrix (ECM).

• Transactions of the Korean Society of Mechanical Engineers A
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• v.23 no.6 s.165
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• pp.1026-1038
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• 1999

Interlaminar fracture toughness of carbon/epoxy composite materials has been studied under tensile and flexural loading by the use of width tapered double cantilever beam(WTDCB) and end notched flexure(ENF) specimens. This study has significantly examined the effect of various interfacial ply orientation, ${\alpha}(0^{\circ},\;45^{\circ}\;and\;90^{\circ})$ and crack propagation direction, ${\theta}(0^{\circ},\;15^{\circ},\;30^{\circ}\;and\;45^{\circ})$ in terms of critical strain energy release rate through experiments. Twelve differently layered laminates were investigated. The data reduction for evaluating the fracture energy is based on compliance method and beam theory. Beam theory is used to analyze the effect of crack propagation direction. The geometry and lay-up sequence of specimens are considered various conditions such as skewness parameter, beam volume, and so on. The results show that the fiber bridging occurred due to the non-midplane crack propagation and causes the difference of fracture energy evaluated by both methods. For safer and more reliable composite structures, we obtain the optimal stacking sequence from initial fracture energy in each mode.

• Korean Journal of Materials Research
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• v.14 no.9
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• pp.649-654
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• 2004

In this paper, the fracture toughness and mechanisms of failure in a random SiC-whisker/$Al_{2}O_3$ ceramic composite were investigated using in situ observations during mode I(opening) loading. $SiC_{w}/Al_{2}O_3$ composite was obtained by hot press sintering of $Al_{2}O_3$ powder and SiC whisker as the matrix and reinforcement, respectively. The whisker and powder were mixed using a turbo mill. The composite was produced at SiC whisker volume fraction of $0.3\%$. Compared with monolithic $Al_{2}O_3$, fracture toughness enhancement was observed in $SiC_{w}/Al_{2}O_3$ composite. This improved fracture toughness was attributed to SiC whisker bridging and crack deflection. $SiC_{w}/Al_{2}O_3$ composite exhibited typically brittle fracture behavior, but a fracture process zone was observed in this composite. This means that the load versus load-line displacement curve of $SiC_{w}/Al_{2}O_3$ composite from a fracture test may involve a small non-linear region near the peak load.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.30 no.4
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• pp.28-34
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• 1998

Polyvinyl acetate emulsion has been widely used as adhesives for wood and paper, paint additives and binders for fiber, leather, and other materials because it is an excellent adhesive with many advantages including low in toxicity risks and manufacturing cost. It is expected the consumption of polyvinyl acetate emulsion as adhesives will increase in cigarette industry as well as in paperboard coating industry. Recently the operation speed of the cigarette tip wrapper increased so substantially that improvement of the emulsion properties is required including good wet tack development, narrow and controlled particle size distribution, low viscosity, etc. In this study the effects of such polymerization conditions as the type and amount of emulsifier, internal or external plasticizing, and emulsification methods on the viscosity and particle size of polyvinyl acetate emulsions were examined. Results showed that polyvinyl alcohol with a high degree of hydrolysis and low molecular weight and nonionic surfactants are superior to anionic surfactant in improving adhesion and emulsion stability. They also tend to produce emulsions with smaller particle size. External plasticization with dipropylene glycol dibenzoate was more effective in improving flexibility than internal plasticization with butyl acrylate. Monomer emulsification under high shear was more effective in decreasing the particle size.

• Journal of Power System Engineering
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• v.4 no.3
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• pp.25-33
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• 2000

This study represents three-dimensional turbulent flow characteristics around an axial fan measured at the operating point ${\varphi}=0.32$, which is equivalent to the maximum flowrate region, by using three-dimensional fiber-optic type LDA system. This LDA system is composed of a 5 W Argon-ion laser, two optics in back-scatter mode, three BSA's, a PC, and a three-dimensional automatic traversing system. A kind of paraffin fog is used for laser particles in this study. Mean velocity profiles around an axial fan along the downstream radial distance show that the streamwise and the tangential components exist as a predominant velocity and have the maximum value at the radial distance ratio 0.8, while the radial component has a small scale distribution and its flow direction is inward except a part of blade tip. The turbulent intensity profiles show that the radial component exists the most greatly. And also the turbulent kinetic energy shows about 60% as a maximum value at the radial distance ratio 0.9. Moreover, the Reynolds shear stresses do not exist at upstream flow, but the streamwise and the radial components of them show about 20% as a maximum value at the radial distance ratio 0.9 at downstream flow.

• Transactions of the Korean Society of Automotive Engineers
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• v.4 no.2
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• pp.69-79
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• 1996

Dynamic stress intensity factors are derives when the crack is propagating with constant velocity under longitudinal shear stress in orthotropic disk plate. General stress fields of crack tip propagating with constant velocity and least square method are used to obtain the dynamic stress intensity factor. The dynamic stress intensity factors of GLV/GTV=1(=isotropic material or transversely isotropic material) which is obtained in out study nearly coincides with Chiang's results when mode Ⅲ stress is applied to boundary of isotropic disk. The D.S.I.F. of mode Ⅲ stress is greater when α(=angle of crack propagation direction with fiber direction) is 90° than that when α is 0°. In case of a/D(a:crack length, D:disk diameter)<0. 58, the faster crack propagation velocity, the less D.S.I.F. but when crack propagation velocity arrive on ghear stress wave velocity, the D.S.I.F. but when crack propagation velocity arrive on shear stress wave velocity, the D.S.I.F. unexpectedly increases and decreases to zero.

• Smart Structures and Systems
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• v.6 no.2
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• pp.91-100
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• 2010

An experimental study was carried out to investigate the shape control of plates via embedded shape memory alloy (SMA) wires. An extensive body of literature proposes the use of SMA wires to actively modify the shape or stiffness of a structure; in most cases, however, the study focuses on modeling and little experimental data is available. In this work, a simple proof of concept specimen was built by attaching four prestrained SMA wires to one side of a carbon fiber laminate plate strip. The specimen was clamped at one end and tested in an environmental chamber, measuring the tip displacement and the SMA temperature. At heating, actuation of the SMA wires bends the plate; at cooling deformation is partially recovered. The specimen was actuated a few times between two fixed temperatures $T_c$ and $T_h$, whereas in the last actuation a temperature $T_f$ > $T_h$ was reached. Contrary to most model predictions, in the first actuation the transformation temperatures are significantly higher than in the following cycles, which are stable. Moreover, if the temperature $T_h$ is exceeded, two separate actuations occur during heating: the first follows the path of the stable cycles; the second, starting at $T_h$, is similar to the first cycle. An interpretation of the phenomenon is given using some differential scanning calorimeter (DSC) measurements. The observed behavior emphasizes the need to build a more comprehensive constitutive model able to include these effects.

• 한국연소학회:학술대회논문집
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• 2005.10a
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• pp.120-131
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• 2005

The evaporation characteristics of single and multicomponent droplets hanging at the tip of a quartz fiber are studied experimentally at the different environmental conditions under normal gravity. Heptane and Hexadecane are selected as two fuels with different evaporation rates and boiling temperatures. At the first step, the evaporation of single component droplet of both fuels has been examined separately. At the next step the evaporation of several blends of these two fuels, as a binary component droplet, has been studied. The temperature and pressure range is selected between 400 and 700 $^{\circ}C$, and 0.1 and 2.5 MPa, respectively. High temperature environment has been provided by a falling electrical furnace. The initial diameter of droplet was in range of 1.1 and 1.3 mm. The evaporation process was recorded by a high speed CCD camera. The results of binary droplet evaporation show the three staged evaporation. In the the first stage the more volatile component evaporates. The droplet temperature rises after an almost non evaporating period and in the third stage a quasi linear evaporation takes place. The evaporation of the binary droplet at low pressure is accompanied with bubble formation and droplet fragmentation and leads to incomplete microexplosion. The component concentration affects the evaporation behavior of the first two stages. The bubble formation and droplet distortion does not appear at high environment pressure. Nomenclature

• Composites Research
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• v.13 no.4
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• pp.67-74
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• 2000

The general solution of the anti-plane shear problem for the curved interfacial crack between viscoelastic foam and composites was investigated with the complex variable displacement function. Kelvin-Maxwell three parameter model is used to present viscoelasticity and the Laplace transform was applied to treat the viscoelastic characteristics of foam in the analysis. The stress intensity factor near the interfacial crack tip was predicted by considering both anisotropic and viscoelastic properties of two different materials. The results showed that the stress intensity factor increased with increasing the curvature of the curved interfacial crack and it also increased and eventually converged to a specific value with increasing time. The stress intensity factor increased with increasing the ratio of stiffness coefficients between foam and composites and the effect of fiber orientation on the stress intensity factor decreased with increasing the ratio of stiffness coefficients between foam and composites.

• Structural Engineering and Mechanics
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• v.42 no.3
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• pp.409-424
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• 2012

Since relatively low elasticity modulus of the FRP materials results in lower natural frequencies, it is necessary to study the free vibration of FRP transmission poles. In this paper, the free vibration of tapered FRP transmission poles with thin-walled circular cross-section is investigated by a tapered beam element. To model the flexible joints of the modular poles, a rotational spring model is used. Modal analysis is performed for typical FRP poles with/without joint and they are also modeled by ANSYS commercial finite element software. There is a good correlation between the results of the tapered beam finite element model and those obtained from ANSYS as well as the existing experimental results. The effects of different geometries, material lay-ups, concentrated masses at the pole tip, and joint flexibilities are evaluated. Moreover, it is concluded that using tougher fibres at the inner and outer layers of the cross-section, results in higher natural frequencies, significantly.