• Advances in nano research
• /
• v.1 no.4
• /
• pp.183-192
• /
• 2013

One-dimensional multiferroic nanostructured composites have drawn increasing interest as they show tremendous potential for multifunctional devices and applications. Herein, we report the synthesis, structural and dielectric characterization of barium titanate ($BaTiO_3$)-bismuth ferrite ($BiFeO_3$) composite fibers that were obtained using a novel sol-gel based electrospinning technique. The microstructure of the fibers was investigated using scanning electron microscopy and transmission electron microscopy. The fibers had an average diameter of 120 nm and were composed of nanoparticles. X-ray diffraction (XRD) study of the composite fibers demonstrated that the fibers are composed of perovskite cubic $BaTiO_3$-$BiFeO_3$ crystallites. The magnetic hysteresis loops of the resultant fibers demonstrated that the fibers were ferromagnetic with magnetic coercivity of 1500 Oe and saturation magnetization of 1.55 emu/g at room temperature (300 K). Additionally, the dielectric response of the composite fibers was characterized as a function of frequency. Their dielectric permittivity was found to be 140 and their dielectric loss was low in the frequency range from 1000 Hz to $10^7$ Hz.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.28 no.6
• /
• pp.659-664
• /
• 2004

It is important to measure precisely the size and velocity of micro-bubbles used in various field. The synchrotron X-ray micro-imaging technique was employed to measure the size and velocity of micro-bubbles moving in an opaque tube simultaneously. Phase contrast images were obtained at interfaces of micro-bubbles between water and air due to their different refractive indices. The X-ray micro-imaging technique was found to measure an optical fiber with an accuracy of 0.2%. Micro-bubbles of 20∼60$\mu\textrm{m}$ diameter moving upward in an opaque tube (${\Phi}$＝2.7mm) were tested to measure bubble size and up-rising velocity. For DI water, the measured velocity of micro-bubbles is nearly proportional to the square of bubble size, agreed well with the theoretical result. In addition, the synchrotron X-ray micro-imaging technique can measure accurately the size and velocity of several overlapped micro-bubbles.

• Journal of the Korean Ceramic Society
• /
• v.39 no.10
• /
• pp.977-980
• /
• 2002

Using the micro-pulling down method, $Nd_2O_3$ doped crack-free stoichiometric $LiNbO_3$ single crystals were grown in 1 mm diameter and 30∼35 mm length. The homogeneous distributions of $Nd_2O_3$ concentration were confirmed by the electron probe micro analysis. The absorption and photoluminescence spectra were measured with respect to the $Nd_2O_3$ doping.

• Journal of the Korea Furniture Society
• /
• v.20 no.4
• /
• pp.281-289
• /
• 2009

This research examined the technical feasibility of composite that had two layers of fiberglass reinforcement to enhance the load carrying capacity of lumber. Specimens were prepared from standard lumber made of thinning crop trees such as Larix kaempferi, Pinus koraiensis, and P. rigida. Results indicated that bending properties, hardness, and wood screw withdrawal load of low density lumber from the P. koraiensis increased as the number of layers of fiberglass reinforcement increased. Composite produced by VARTM method showed the MOE increased in all specimens, while the MOR differed on the location, whether the 2-layers of FRP is put on tensile zone or compressive zone. The MOR of high density lumber from Larix kaempferi and P. rigida decreased when they placed into tensile zone, but low density lumber from P. koraiensis increased in same location. The bending toughness only increased high density lumber of Larix kaempferi as the number of layers of fiberglass reinforcement increased. The technique developed by this study may increase an opportunity to use small diameter log with low density for commercial purposes.

• Journal of the Korean Society for Precision Engineering
• /
• v.30 no.5
• /
• pp.520-528
• /
• 2013

A 20 mm diameter of small 5-D.O.F. force sensor has been developed for applications in MR-field Optical intensity modulation was adopted for transducing to miniaturize the sensor structure. For its accurate sensing of 5-D.O.F. force/moment, the elastic detecting module was designed to respond independently to each force or moment component. And for small size, two optical transducing modules of 2-D.O.F. and 3-D.O.F. were designed and integrated with the detecting module where optical fibers were arranged in parallel to make the sensor small. It is confirmed by calibration test that the detecting modules deforms linearly and independently to the input force. The results of evaluating test show that the range and resolution of forces are ${\pm}4$ N and 0.94~7.1 mN and the range and resolution of moments are ${\pm}120N{\cdot}mm$ and $0.023{\sim}0.034N{\cdot}mm$.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2005.06a
• /
• pp.90-95
• /
• 2005

To perform the finish outside-diameter grinding process of ferrules which are widely used as fiber optic connectors, a high-precision centerless grinding machine is necessary. In this study, the thermal characteristics of the high-precision centerless grinding machine such as the temperature distribution, temperature rise and thermal deformation, are estimated based on the virtual prototype of the grinding machine and the heat generation rates of heat sources related to the machine operation conditions. The reliability of the predicted results is demonstrated by the temperature characteristics measured from the physical prototype. Especially, the predicted and measured results show the fact that the high-precision centerless grinding machine consisted of the hydrostatic GW and RW spindle systems, hydrostatic RW feeding mechanism, RW swivel mechanism, on-machine GW and RW dressers, and concrete-filled steel bed, has very stable thermal characteristics.

• Journal of the Korea Concrete Institute
• /
• v.19 no.5
• /
• pp.577-584
• /
• 2007

The effect of steel microfibers (SMF) on alkali-silica reaction (ASR) was investigated using two types of reactive aggregates, crushed opal and a pyrex rod of constant diameter. Cracks are less visible in the SMF mortars compared with the unreinforced mortars. Due to crack growth resistance behavior in SMF mortar specimens, the strength loss is eliminated and the ASR products remained well confined within the ASR site. The expansion and the ASR products were characterized by microprobe analysis and inductively coupled plasma (ICP) spectroscopy. The confinement due to SMF resulted in a higher Na and Si ion concentration of the ASR liquid extracted from the reaction site. The higher concentration reduced the ASR rate and resulted in a lower reactivity of the reactive pyrex rods in SMF mortars.

• Proceedings of the KSME Conference
• /
• 2007.05a
• /
• pp.1312-1316
• /
• 2007

Strip casted and rolled magnesium sheet is become exiting material for car manufacturer, due to its better formability and specific strength compare with conventional extruded sheet. TWB technology was attractive for car body designer, because it saves the weight of the car without strength loss. In this study, the laser welding performance of magnesium sheet was investigated for Mg TWB panel manufacturing. The material was strip casted and rolled magnesium alloy sheet contains 3 wt% Al and 1 wt% Zn (AZ31). Lamp pumped Nd:YAG laser of 2kW was used and its laser light was delivered by optical fiber of 0.6mm core diameter to material surface with focusing optics of 200mm focal length for TWB welding. The microstructure of weld bead was investigated to check internal defects such as inclusion, porosity and cracks. Also mechanical properties and formability were evaluated for press forming of car body. For the results, there was no crack but inclusion or porosity on weld at some conditions.The tensile strength of weld was over 95% of base metal. Inner and outer panel of engine hood were press formed and assembled at elevated temperature.

• Journal of the Korean Wood Science and Technology
• /
• v.48 no.2
• /
• pp.231-244
• /
• 2020

As a way of finding value-added materials from waste medium density fiberboard (MDF), this study characterized cellulose nanocrystals (CNCs) isolated by ammonium persulfate (APS) oxidation using recycled MDF fibers. Chemical composition of the recycled MDF fibers was done to quantify α-cellulose, hemicellulose, lignin, nitrogen, ash and extractives. The APS oxidation was performed at 60 ℃ for 16 h, followed by ultrasonication, which resulted in a CNC yield of 11%. Transmission electron microscope images showed that rod-like CNCs had an average length and diameter of 167±47 nm and 8.24±2.28 nm, respectively, which gave an aspect ratio of about 20. The conductometric titration of aqueous CNCs suspension resulted in a carboxyl content of 0.24 mmol/g and the degree of oxidation was 0.04. Attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy clearly showed the presence of carboxyl group on the CNCs prepared by the APS oxidation. The change of pH of the aqueous CNC suspension from 4 to 7 converted the carboxyl group to sodium carboxylate group. These results showed that the APS oxidation was facile and CNCs had a one-step preparation method, and thus suggested an optimization of the oxidation condition in future.

• Transactions of the Korean Society of Automotive Engineers
• /
• v.4 no.2
• /
• pp.69-79
• /
• 1996

Dynamic stress intensity factors are derives when the crack is propagating with constant velocity under longitudinal shear stress in orthotropic disk plate. General stress fields of crack tip propagating with constant velocity and least square method are used to obtain the dynamic stress intensity factor. The dynamic stress intensity factors of GLV/GTV=1(=isotropic material or transversely isotropic material) which is obtained in out study nearly coincides with Chiang's results when mode Ⅲ stress is applied to boundary of isotropic disk. The D.S.I.F. of mode Ⅲ stress is greater when α(=angle of crack propagation direction with fiber direction) is 90° than that when α is 0°. In case of a/D(a:crack length, D:disk diameter)<0. 58, the faster crack propagation velocity, the less D.S.I.F. but when crack propagation velocity arrive on ghear stress wave velocity, the D.S.I.F. but when crack propagation velocity arrive on shear stress wave velocity, the D.S.I.F. unexpectedly increases and decreases to zero.