• Title/Summary/Keyword: FeS layer

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Properties of an Extracellular Amylase Produced by the Marine Halophilic Bacterium Vibrio alginolyticus (해양 호염성 세균 Vibrio alginolyticus가 생산하는 Extracellular Amylase의 특성)

  • 김영재
    • Microbiology and Biotechnology Letters
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    • v.27 no.3
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    • pp.203-207
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    • 1999
  • V. alginolyticus 138-2, a marine halophilic bacterium, produced an extracellular amylase with a molecular weight of ca. 56,000. The analysis of the digestion products of soluble starch by thin layer chromatography(TLC) revealed that the extracellular amylase of V. alginolyticus 138-2 is a saccharifying-type alpha-amylase. The alpha-amylase activity of the culture supernatant of soluble starch was optimal at pH 6.0 and 45$^{\circ}C$. Ca2+ slightly increased the alpha-amylase activity, whereas Hg2+, An2+, Cu2+, Ni2+, Fe2+, and Mn2+inhibited the enzymatic activity. Alkylating thiol group agent, iodoacetic acid did not affect the alpha-amylase activity, but reduced thiol reagents such as dithiothreitol, cysteine, and beta-mercaptoethanol stimulated theenzymatic activity. On the other hand, even if V. alginolyticus 138-2 is a marine halophilic bacterium, its alpha-amylase activity was significantly inhibited by NaCl.

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Formations and properties of MFIS structure using $LiNbO_3/Si_3N_4$ structure ($LiNbO_3/Si_3N_4$ 구조를 이용한 MFIS 구조의 형성 및 특성)

  • 김용성;정상현;정순원;이남열;김진규;김광호;유병곤;이원재;유인규
    • Proceedings of the IEEK Conference
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    • 2000.11b
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    • pp.221-224
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    • 2000
  • We have successfully demonstrated metal-ferroel-ectric-insulator-semiconductor (MFIS) devices using Al/LiNbO$_{3}$/SiN/Si structure. The SiN thin films were made into metal -insulator- semiconductor (MIS) devices by thermal evaporation of aluminum source in a dot away on the surface. The interface property of MFIS from 1MHz & quasistatic C-V is good and the memory window width is about 1.5V at 0.2V/s signal voltage sweep rate. The gate leakage current density of MFIS capacitors using a aluminum electrode showed the least value of 1x10$^{-8}$ A/$\textrm{cm}^2$ order at the electric field of 300㎸/cm. And the XRD patterns shows the probability of applications of LN for MFIS devices for FeRAMs on amorphous SiN buffer layer.

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Specualr spin valve with nano-oxide layer (나노 oxide 층을 가진 스펙큘라 스핀밸브)

  • Kim, K.Y.;Kim, H.J.;Jang, S.H.;Kang, T.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2002.12a
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    • pp.30-31
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    • 2002
  • 100 Gbit/in$^2$ 이상의 자기기록밀도를 달성하기 위해서는 재생헤드로 사용되고 있는 스핀밸브의 자기저항비가 10% 이상을 가지면서 열적 특성이 우수해야 한다. 현재까지 연구되어진 스핀밸브 구조 중 NiO([,2,3], $\alpha$-Fe$_2$O$_3$[4]등의 산화물 반강자성 층을 사용한 스핀밸브의 경우 기본 스핀밸브 구조를 사용하고도 이미 20% 이상의 자기저항비를 달성하였다. 이러한 높은 자기저항비는 절연층인 산화물 반강자성층과 금속 자성층 계면에서 일어나는 전자의 스펙큘라 반사(specular reflection)로부터 기인한다고 보고하고 있다.[2] (중략)

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Tunneling Magnetoresistance of a Ramp Edge Junction with $SrTiO_3$ Barrier Layer ($SrTiO_3$ 장벽층을 이용한 경사형 모서리 접합의 터널링 자기저항 특성연구)

  • Lee, Sang-Suk;Kim, Young-Il;Hwang, Do-Guwn;Kim, Sun-Wook;Kungwon Rhie;Rhee, Jang-Roh
    • Proceedings of the Korean Magnestics Society Conference
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    • 2002.12a
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    • pp.174-175
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    • 2002
  • A ramp-type tunneling magnetoresistance (TMR) junction having structure NiO(60 nm)/pinned Co(10 nm)MiO(60 nm)/barrier SrTiO$_3$(2-10 nm)/free NiFe(10 nm) with the 15 degree slope was investigated. We obtained nonlinear I(V) characteristics for ramp-type tunneling junctions that have distinctive difference with and without applied magnetic field. In the barrier SrTiO$_3$ thickness of 4 nm, the TMR was about 52% at a bias voltage of 50 mV. (omitted)

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Surface magnetic properties of annealed $Co_{66}Fe_4B_{15}Si_{15}$ amorphous ribbons

  • L. Jin;Y. W. Rheem;Lee, B. S.;Kim, C. G.;Kim, C. O.
    • Proceedings of the Korean Magnestics Society Conference
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    • 2002.12a
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    • pp.208-209
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    • 2002
  • Recently an asymmetric giant magnetoimpedance (GMI) profile has been observed in Co-based amorphous ribbons annealed at the weak field [1-4]. This phenomenon has attracted a large interest due to its practical application to sensitive magnetic sensors. It is known [5.6] that in magnetic materials, the magnetoimpedance is caused by the effect of the magnetic field on the transverse magnetic permeability of a near-surface layer. In consequence of it, the value of the magnetoimpedance depends strongly on near-surface magnetic properties of the sample. (omitted)

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Failure Investigation of Fire-Side Water-Wall Tube Boiler

  • Fatah, M.C.;Agustiadi, D.;Pramono, A.W.
    • Corrosion Science and Technology
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    • v.20 no.5
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    • pp.242-248
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    • 2021
  • Unforeseen failures of boilers in power plants may affect the continuation of electricity generation. Main failures in boilers are influenced by the tube material, tube position, boiler service temperature and pressure, and chemical composition of the feed water and coal. This investigation was intended to find answers on the causes and mechanism of failure of the fire-side boiler water-wall tubes, due to perforation and corrosion. The tube conformed to the material requirements in terms of its chemical composition and hardness. Microscopic examination showed ferrite and pearlite indicating no changes in its microstructure due to the temperature variation. SEM test showed a single layer and homogenous film density particularly on the area far from perforation. However, layers of corrosion product were formed on the nearby perforation area. EDX showed that there were Na, Ca, S, and O elements on the failed surface. XRD indicated the presence of Fe2O3 oxide. The failure mechanism was identified as a result of significant localized wall thinning of the boiler water wall-tube due to oxidation.

Multi-layered Gap Measurement on In-Vessel Cerium Retention Using Ultrasonic Wave Reflective Pattern Analysis and Frequency Diversity Signal Processing (초음파 반사 패턴과 주파수 대역 분할 신호처리를 이용한 다층구조인 노내 간극 측정)

  • Koo, Kil-Mo;Sim, Cheul-Mu;Kim, Jong-Hwan;Kim, Sang-Baik;Kim, Hee-Dong;Park, Chi-Seung
    • Journal of the Korean Society for Nondestructive Testing
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    • v.20 no.4
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    • pp.314-321
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    • 2000
  • A gap between a $Al_2O_3/Fe$ thermite and lower head vessel is formed in the lower-plenum arrested vessel attack(LAVA) experiment which is the 1st phase study of simulation of naturally arrested vessel attack in vessel(SONATA-IV). The gap measurement using a conventional ultrasonic method would be lack of a reliability due to the structure complexity and the metallurgical grain size change of the lower head HAZ occurred by a thermite $Al_2O_3/Fe$ melt or a $Al_2O_3$ melt at $2300^{\circ}C$. The grain echoes having false signals and lower S/N ratio signals are detected due to a multiple scattering, a mode conversion and an attenuation of a ultrasonic resulted from at the interface of increased grain size zone. In this test, the signals pattern was classified to understand the behavior of the ultrasonic in a multi-layer specimen of solid-liquid-solid of assuming that the thermite and the lower head vessel is immersed. The polarity threshold algorithm of frequency diversity gives us the enhancement about 6dB of the ratio S/N.

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Studies on the Strength of Cement Mortars with Surface Crosslinked cPSA Absorbent (표면이 가교된 Crosslinked Poly(sodium acrylate) 흡수제가 첨가된 시멘트 모르타르의 강도 특성 연구)

  • Hwang, Ki-Seob;Jang, Seok-Soo;Jung, Yong-Wook;Lee, Seung-Han;Ha, Ki-Ryong
    • Polymer(Korea)
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    • v.36 no.2
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    • pp.208-215
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    • 2012
  • To study the effect of surface crosslinked layer on the crosslinked poly(sodium acrylate) (cPSA) absorbent, we synthesized several surface crosslinked cPSAs with 5, 10 and 20 g of ethylene glycol dimethacrylate (EGDMA) by an inverse emulsion polymerization method to delay the absorption of excess water in concrete. We measured the compressive and flexural strength of mortars having 0.5, 1.0 and 1.5 wt% cPSA-EGDMA. We observed the increase of compressive and flexural strength of the cPSA-EGDMA added cement mortars except for the 0.5 wt% cPSA-EGDMA (20 g) added cement mortar. 1.0 wt% cPSA-EGDMA (5 g) added cement mortar showed about 16% and 10% increased compressive and flexural strength than those of plain cement mortar. To study the effect of porosity on compressive and flexural strength, we used FE-SEM and porosimeter. FE-SEM analysis showed swollen cPSMAEGDMA (5 g) filled between calcium silicate hydrate (C-S-H) crystals. We observed the decreased porosity of the cPSA-EGDMA added cement mortars than that of plain cement mortar. 1.0 wt% cPSA-EGDMA (5 g) cement mortar showed the lowest porosity of 16.5%.

Hysteretic characteristics of steel plate shear walls: Effects of openings

  • Ali, Mustafa M.;Osman, S.A.;Yatim, M.Y.M.;A.W., Al Zand
    • Structural Engineering and Mechanics
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    • v.76 no.6
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    • pp.687-708
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    • 2020
  • Openings in steel plate shear walls (SPSWs) are usually used for decorative designs, crossing locations of multiple utilities and/or structural objectives. However, earlier studies showed that generating an opening in an SPSW has a negative effect on the cyclic performance of the SPSW. Therefore, this study proposes tripling or doubling the steel-sheet-plate (SSP) layer and stiffening the opening of the SPSW to provide a solution to undesirable opening effects, improve the SPSW performance and provide the infill option of potential strengthening measures after the construction stage. The study aims to investigate the impact of SSP doubling with a stiffened opening on the cyclic behaviour, expand the essential data required by structural designers and quantify the SPSW performance factors. Validated numerical models were adopted to identify the influence of the chosen parameters on the cyclic capacity, energy dissipation, ductility, seismic performance factors (SPF) and stiffness of the suggested method. A finite Element (FE) analysis was performed via Abaqus/CAE software on half-scale single-story models of SPSWs exposed to cyclic loading. The key parameters included the number of SSP layers, the opening size ratios corresponding to the net width of the SSP, and the opening shape. The findings showed that the proposed assembly method found a negligible influence in the shear capacity with opening sizes of 10, 15, 20%. However, a deterioration in the wall strength was observed for openings with sizes of 25% and 30%. The circular opening is preferable compared with the square opening. Moreover, for all the models, the average value of the obtained ductility did not show substantial changes and the ultimate shear resistance was achieved after reaching a drift ratio of 4.36%. Additionally, the equivalent sectional area of the SSP in the twin and triple configuration of the SPSWs demonstrated approximately similar results. Compared with the single SSP layer, the proposed configuration of the twin SSP layer with a stiffened opening suggest to more sufficiency create SSP openings in the SPSW compared to that of other configurations. Finally, a tabular SPF quantification is exhibited for SPSWs with openings.

Effects of TiN/Ti Multilayer Coating on the Ti-30Ta-xZr Alloy Surface (Ti-30Ta-xZr 합금의 표면에 TiN/Ti 다층막코팅효과)

  • Kim, Y.U.;Jeong, Y.H.;Cho, J.Y.;Choe, H.C.;Vang, M.S.
    • Journal of the Korean institute of surface engineering
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    • v.42 no.4
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    • pp.161-168
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    • 2009
  • Effects of TiN/Ti multilayer coating on the Ti-30Ta-xZr alloy surface were studied by using various experiments. The Ti-30Ta containing Zr (5, 10 and 15 wt%) were melted 10 times to improve chemical homogeneity by using a vacuum furnace. And then samples were homogenized for 24 hrs at $1000^{\circ}C$. The specimens were prepared for TiN/Ti coating by cutting and polishing. The prepared specimens were coated with TiN/Ti multilayers by using DC magnetron sputtering method. The analyses of coated surface and coated layer were carried out by field emission scanning electron microscope(FE-SEM), EDX, and X-ray diffractometer(XRD). From the microstructure and XRD analysis of Ti-30Ta-xZr alloys, The equiaxed structure was changed to needle-like structure with increasing Zr content. And $\alpha$-peak and elastic modulus increased as Zr content increased. The $\alpha$ and $\beta$ phase predominantly were found in the specimen containing high Zr content. According to the analysis of TiN/Ti coating layer, the surface defects and structures of Ti-30Ta-xZr were covered with TiN/Ti coating layer and surface roughness decreased.