• Title/Summary/Keyword: FeS layer

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Effect of 2nd Anodization on the Pore Formation for Alumina Nano Templates (알루미나 나노템플레이트의 기공형성에 미치는 2차 양극산화의 영향)

  • Cho, S.H.;Oh, H.J.;Joo, E.K.;Yoo, C.W.;Chi, C.S.
    • Korean Journal of Materials Research
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    • v.12 no.7
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    • pp.533-539
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    • 2002
  • Porous anodic aluminum oxide layer for nano templates was prepared in acidic solutions. In order to investigate effects of 2nd anodization on ordered formation behaviors of the porous oxide layers, electrochemical and microstructural studies were performed, primarily using TEM, FE- SEM, AFM, and Ultramicrotomy. The pore diameter of the anodic oxide layer increased approximately linearly with increasing voltages, and to the contrary, the pore density decreased. It was shown that 2nd anodizing on the cell base after dissolving 1st anodic oxide layer was remarkably effective for forming ordered array of the pores, comparing with the case for 1st anodization only. And for controlling the diameter of pores, widening method by chemical dissolution seemed more practical than by electrochemical methods.

Lacquer Manufacturing Method for the Wooden Coffins of King Muryeong's Tomb based on the Scientific Analysis (과학적 분석방법을 이용한 무령왕릉 목관재의 옻칠 기법 연구)

  • Kim, Soo-Chul;Lee, Gwang-Hee;Kang, Hyung-Tae;Shin, Seong-Phil;Han, Min-Soo
    • Journal of Conservation Science
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    • v.26 no.3
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    • pp.247-258
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    • 2010
  • We conducted optical microscopy, infra-red spectroscopy and SEM-EDS analysis of the lacquer layers on the wooden coffins excavated from King Muryeong's Tomb. We found four varnishing methods according to the sub-materials of lacquer layers: The lacquer of wooden coffins with black paint layer on the surface were classified with two groups; single layer and three layers. The lacquer of wooden coffins without black paint layer on the surface were classified with two groups; single layer and two layers. IR spectra of the laquer were same as those of the oriental laquer. The SEM-EDS analysis showed that the lacquer layers were mixed with iron, copper and calcium.

Fully Integrated Electromagnetic Noise Suppressors Incorporated with a Magnetic Thin Film on an Oxidized Si Substrate

  • Sohn, Jae-Cheon;Han, S.H.;Yamaguchi, Masahiro;Lim, S.H.
    • Journal of Magnetics
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    • v.12 no.1
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    • pp.21-26
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    • 2007
  • Si-based electromagnetic noise suppressors on coplanar waveguide transmission lines incorporated with a $SiO_2$ dielectric layer and a nanogranular Co-Fe-Al-O magnetic thin film are reported. Unlike glass-based devices, large signal attenuation is observed even in the bare structure without coating the magnetic thin film. Much larger signal attenuation is achieved in fully integrated devices. The transmission scattering parameter ($S_{21}$) is as small as -90 dB at 20 GHz at the following device dimensions; the thicknesses of the $SiO_2$ and Co-Fe-Al-O thin films are 0.1 $\mu$m and 1 $\mu$m, respectively, the length of the transmission line is 15 mm, and the width of the magnetic thin film is 2000 $\mu$m. In all cases, the reflection scattering parameter ($S_{11}$) is below -10 dB over the whole frequency band. Additional distributed capacitance formed by the Cu transmission line/$SiO_2$/Si substrate is responsible for these characteristics. It is considered that the present noise suppressors based on the Si substrate are a first important step to the realization of MMIC noise suppressors.

A Study on Properties of $CuInS_2$ thin films by composition ratio (조성비에 따른 $CuInS_2$ 박막의 특성변화에 관한 연구)

  • Yang, Hyeon-Hun;Kim, Young-Jun;Jeong, Woon-Jo;So, Soon-Youl;Lee, Jin;Chung, Hae-Deok;Park, Gye-Choon;Choi, Yong-Sung;Lee, Gyung-Sup
    • Proceedings of the KIEE Conference
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    • 2008.07a
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    • pp.1268-1269
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    • 2008
  • $CuInS_2$ thin films were fabricated by sulpurization of Cu/In Stacked elemental layer deposited onto glass substrates by vacuum annealing at various temperatures. And structural and electrical properties were measured in order to certify optimum conditions for growth of the ternary compound semiconductor $CuInS_2$ thin films by composition ratio. Physical properties of the thin film were investigated at various fabrication conditions; substrate temperature, annealing temperature and annealing time by XRD, FE-SEM and hall measurement system. $CuInS_2$ thin film was well made at the heat treatment 200[$^{\circ}C$] of SLG/Cu/In/S stacked elemental layer.

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A Study on the Manufacturing Technique of Horse Strap Pendants excavated from Seobongchong, Sikrichong and Geumryeongchog (서봉총(瑞鳳塚)·식리총(飾履塚)·금령총(金鈴塚) 출토 행엽(杏葉)의 제작기법 연구)

  • Son, Eun-a;Kwon, Heehong;Park, Haksoo
    • Conservation Science in Museum
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    • v.12
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    • pp.35-45
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    • 2011
  • To keep relics excavated in the era of the Japanese Colonist's rule in the Korean Peninsula in order, the National Museum of Korea selected some of horse strap pendants (Haengyeob) that were excavated from Seobongchong, Sikrichong and Geumryeongchong, and it investigated conservation and production technique. The horse strap pendants selected were classified into three, that is to say, Oval and fish-tail shape, heart shape and atypical: At the results of microscopic observation, XRF and SEM-EDS analysis, base plate was made of iron, and top plate as well as pattern plate was made of iron, copper and silver. Both Oval and fish-tail shape and heart shape horse strap pendants had horse strap pendants having same production technique and sizes at all of three ancient tombs were made of iron and copper. The gold layer of horse strap pendants except the atypical one having no gold layer were made by amalgam gilding.

Characterization of the Microstructure and the Wear Resistance of the Flame-Quenched Cu-8.8Al-4.5Ni-4.5Fe Alloy (화염급냉 표면처리된 Cu-8.8Al-4.5Ni-4.5Fe 합금의 미세구조 분석 및 내마모성에 관한 연구)

  • Lee, M.K.;Hong, S.M.;Kim, G.H.;Kim, K.H.;Kim, W.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.6
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    • pp.346-355
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    • 2004
  • The flame quenching process has been employed to modify the surfaces of commercial marine propeller material, aluminum bronze alloy (Cu-8.8Al-5Ni-5Fe), and the microstructure, hardness and wear properties of the flame-quenched layers have been studied. The thermal history was accurately monitored during the process with respect to both the designed maximum surface temperature and holding time. The XRD and EDX analyses have shown that at temperatures above $T_{\beta}$, the microstructure consisting of ${\alpha}+{\kappa}$ phases changed into the ${\alpha}+{\beta}^{\prime}$ martensite due to an eutectoid reaction of ${\alpha}+{\kappa}{\rightarrow}{\beta}$ and a martensitic transformation of ${\beta}{\rightarrow}{\beta}^{\prime}$. The ${\beta}^{\prime}$ martensite phase formed showed a face-centered cubic (FCC) crystal structure with the typical twinned structure. The hardness of the flame-quenched layer having the ${\alpha}+{\beta}^{\prime}$ structure was similar to that of the ${\alpha}+{\kappa}$ structure and depended sensitively on the size and distribution of hard ${\kappa}$ and ${\beta}^{\prime}$ phases with depth from the surface. As a result of the sliding wear test, the wear resistance of the flame-quenched layer was markedly enhanced with the formation of the ${\beta}^{\prime}$ martensite.

Magnetic Bio-Sensor Using Planar Hall Effect (평면홀 효과를 이용한 자기 바이오센서)

  • Oh, Sun-Jong;Hung, Tran Quang;Kumar., S. Ananda;Kim, Cheol-Gi;Kim, Dong-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.28 no.5
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    • pp.421-426
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    • 2008
  • The magnetic bio-sensor used the PHR (planar hall resistance) effect generated by the free layer in spin-valve giant magnetoresistance structure of Ta/NiFe/CoFe/Cu/NiFe/IrMn/Ta. The PHR element with micrometer size was fabricated through the photolithograph and dry etching process. The PHR signal with magnetic field was measured under the conditions of with and without single magnetic bead. A single magnetic bead of diameter $2.8\;{\mu}m$ was successfully detected using the PHR sensor. Therefore, the high resolution PHR sensor can be applied to bio-sensor application utilizing the output voltage variation of the PHR signals in the presence and absence of a single magnetic bead.

Magnetoimpedance(MI) Effect due to the Removal of Skin Layer in Amorphous Metal $\textrm{Co}_{66}\textrm{Fe}_{4}\textrm{NiB}_{14}\textrm{Si}_{15}$ (표면층 제거에 대한 비정질 금속 $\textrm{Co}_{66}\textrm{Fe}_{4}\textrm{NiB}_{14}\textrm{Si}_{15}$의 자기임피턴스 효과)

  • Jo, Wan-Sik;Kim, Jong-O;Lee, Hui-Bok
    • Korean Journal of Materials Research
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    • v.7 no.9
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    • pp.728-732
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    • 1997
  • 비정질 금속 $Co_{66}$F $e_{4}$Ni $B_{14}$S $i_{15}$ 의 표면층 제거에 대한 자기임피턴스 효과는 시료의 길이방향에 평행한 일축자기장에 대하여 측정하였다. MIR(Magnetoimpedance Ratios)은 비정질 금속의 두께가 얇아짐에 따라 감소하고, 전류에 비례하여 증가하는 경향을 나타내었다. 인가전류 주파수에 대한 MIR과 자기장의 감도는 모든 시료에서 주파수에 비례하여 증가하며 수 MHz 부근에서 최대값을 가지고 점차 감소하는 경향을 나타내었다. 시료의 표면층제거에 기인한 이방성자기장의 변화는 MI $R_{Max}$을 나타내는 외부 자기장을 감소시키지만, MIR은 표면층 제거에 따른 부피효과에 기인하여 감소하였다....

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Magnetic Properties of Electrodeposited Iron and Cobalt on Porous Aluminum Oxide Layer (다공성 알루미늄 양극산화 피막에 도금된 철 및 코박트의 자기적 성질)

  • Kim, K. H.;Kang, T.;Sohn, H. J.
    • Journal of the Korean institute of surface engineering
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    • v.23 no.3
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    • pp.150-159
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    • 1990
  • The magnetic properties of electrodeposited iron and cobalt films on porous aluminum oxide film were examined. There exists perpendicular magnetic anisotropy due to the shape anisotropy. The coercivity and squareness ratio of films were strongly dependent on deposited particle diameter. The effect of packing fraction on squareness ratio was also apprecible. Unlike the iron-deposited films, the magnetic properties of cobalt films were changed by preferred orientation because of it's large crystal ansotropy constant.(about 10 times of Fe) The Fe deposited films were found to be more suitable for perpendicular magenetic recording media bacause perpendicular coercivity, squareness ratio and the ratio of perpendicular coercivity to horizontal ones of iron films are greater than those of cobalt films.

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