• Title/Summary/Keyword: Fe-B-P

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The Use of Leucaena leucacephala Leaf Meal as a Protein Supplement for Pigs

  • Zakayo, G.;Krebs, G.L.;Mullan, B.P.
    • Asian-Australasian Journal of Animal Sciences
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    • v.13 no.9
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    • pp.1309-1315
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    • 2000
  • Sixteen Large $White{\times}Landrace$ pigs 12 weeks of age, with an average body weight of $22.9{\pm}2.12kg$ were fed four experimental diets; a commercial grain-based grower diet (control); or a diet containing 20% of either sun-dried leucaena leaf meal (LLM), water soaked LLM or $FeSO_4-treated$ LLM, replacing the basal diet. There was a significant (p<0.05) decrease in live weight gain, feed intake and feed conversion efficiency (FCE) in pigs fed the diet containing sun-dried LLM. Growth rate, feed intake and FCE were not affected by the addition of water-soaked and FeSO4-treated LLM to the basal diet. Triiodothyronine $(T_3)$ and thyroxine $(T_4)$ levels in the blood plasma were not affected by the dietary treatments. Addition of $FeSO_4-treated$ LLM to the basal diet significantly (p<0.05) reduced the back fat thickness of the pigs.

A Study on the Fabrication of Fe-Co Magnetic Fluid from the Waste Pickling Liquor of Steel

  • Kim, Young-Sam;Lee, Jong-Heon
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.149-153
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    • 2001
  • This paper describes on the fabrication of Fe-Co hydrophilic magnetic fluids from the waste pickling liquor of steel. By adding with HNO$_3$in the waste liquor oxidation is proceeded from Fe$^{3+}$ion at 6$0^{\circ}C$ with air blowing. Ultra-fine Co-ferrite particles with the mean particle size of 50 $\AA$ were produced at pH 12 after adjusting the ratio of Fe$^{3+}$Co$^{2+}$=7/3(wt%) and Fe-Co particles with the mean particle size of 94 $\AA$ were produced by reducing the Co-ferrite particle with H$_2$at the temperature of 50$0^{\circ}C$. After triple adsorption of oleic acid dodecyl benzene sulfonate(D.B.S.) and tetra methyl ammonium(T.M.A.) ions on the surface of Fe-Co particles Fe-Co hydrophilic magnetic fluid was produced by dispersing the Fe-Co particles in ethylene glycol solution. The magnetization of the Fe-Co hydrophilic magnetic fluid increased with increasing the Fe-Co concentration. The magnetic fluid containing 70% (g/cc) Fe-Co showed 73 emu/g in magnetization at the magnetic intensity of 10 kOe.kOe.e.

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Magnetic Properties and Cation Distribution of Phosphorous-Doped $Co-{\gamma}-{Fe_2} {O_3}$ Particles

  • Na, J.G.;Han, D.H.
    • Journal of Magnetics
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    • v.1 no.1
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    • pp.51-54
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    • 1996
  • The effects of additional P-doping on the magnetic properties, thermal stability and cation distribution of Co-doped ${\gamma}-{Fe_2} {O_3}$have been investigated by means of magnetic annealing and measurements with vibration sample magnetometer and torque magnetometer. It is found that the P-doping promotes the coercivity and its magnetic-thermal stability, which may be attributed to increase of the cubic magneto-crystalline anisotropy constant, $K_1$ and the activation energy, E, for cation rearrangement, respectively. The cation distribution of P and Co-substituted iron oxide was calculated from the variation of the saturation magnetization with P-doping on the basis of the Neel model. It was found that the most of P ions in the iron oxides occupied the B-site of spinel lattice.

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Studies on Crystallographic and Magnetic Properties of the Sn0.9957Fe0.01O2 (Sn0.9957Fe0.01O2의 결정학적 및 자기적 성질에 관한 연구)

  • Li, Yong-Hui;Kim, Sam-Jin;Kim, Chul-Sung
    • Journal of the Korean Magnetics Society
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    • v.20 no.5
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    • pp.187-190
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    • 2010
  • $Sn_{0.99}{^{57}Fe}_{0.01}O_2$ prepared by a sol-gel method, and studied by x-ray diffractometer, vibrating magnetometer, Superconducting quantum interference devices and M$\ddot{o}$ssbauer spectroscopy. the crystal structure were found to be a rutile tetragonal structure with space group $P4_2$/mnm, and oxygen deficiency are 5.6 % by Rietveld refinement. magnetization value were $M_s=1.95{\times}10^{-2}{\mu}_B/Fe$ at room temperature, and Curri-weiss temperature were and ${\theta}_{cw}$ = 18 k, measurement of VSM and SQUID, respectively. Mssbauer spectra of $Sn_{0.99}{^{57}Fe}_{0.01}O_2$ have been Sextet taken at various temperatures ranging from 4.2 K to RT, and isomer shift value $\delta$ = 0.18~0.36 mm/s of $^{57}Fe$ ion site all of the temperature range the state shows ferric.

The Mineral Contents, Viscosity and Sensory Characteristics of Demi-glace Sauce According to the Varying Quantity of Omija added (오미자 첨가량에 따른 Demi-glace 소스의 무기성분 함량과 점도 및 관능적 특성)

  • Kim, Hyun-Duk
    • Journal of the Korean Society of Food Culture
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    • v.19 no.6
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    • pp.667-677
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    • 2004
  • This study was conducted to examine contents of mineral, viscosity in the Demi-glace with added quantity of Omija extracts. Firstly, The level of mineral content in order was K, Na, P, Ca, Mg, Fe, Zn, Mn, B. The more Omija extracts, Ca, Mg, Fe, Zn, Mn, B was increased, but K, Na, P was decreased. Secondly, Viscosity of control was 538.13cP at rpm 100, and the sauce added with Omija extracts was $464.80{\sim}578.00cP$. Regardless of Omija quantity there was Psedoplastic characteristic which showed apparent viscosity was decreased even though shear rate was increased. Thirdly, Sensory characteristics of Demi-glace sauces based on preference of 5 tastes, It was founded that 2% added Omija was the best, and 1%, 0%, 3%, 5% added Omija was next in order. Finally, Sensory intensities of Demi-glace sauces based on gender and occupation of the 5 tastes : As the sourness, bitterness, hotness, salines taste of all over was Omija added quantity was many more, appeared strong intensity, it was sensory intensities of 5% Omija added sauce was the highest. But sensory intensities of sweetness, Male showed 2% Omija added sauce, Female student and cook showed control was the highest.

Purification and Characterization of Lipase from Acinetobacter sp. B2 Isolated from Oil­contaminated Soil (유류오염지역에서 분리한 Acinetobacter sp. B2로부터의 Lipase 정제 및 특성)

  • Son Seung Hwa;Park Kyeong Ryang
    • Korean Journal of Microbiology
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    • v.40 no.4
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    • pp.320-327
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    • 2004
  • Three hundreds thirty two bacterial colonies which were able to degrade crude oil were isolated from soil sam­ples that were contaminated with oil in Daejeon area. Among them, one bacterial strain was selected for this study based on its higher oil degrading ability, and this selected bacterial strain was identified as Acinetobactor sp. B2 through physiological-biochemical tests and analysis of its 16S rRNA sequence. Acinetobactor sp. B2 was able to utilize various carbohydrates but did not utilize trehalose and mannitol as a sole carbon source. Acinetobactor sp. B2 showed a weak resistance to antibiotics such as kanamycin, streptomycin, tetracycline and spectinomycin, but showed a high resistance up to mg/ml unit to heavy metals such as Ba, Li, Mn, AI, Cr and Pb. The optimal growth temperature of Acinetobactor sp. B2 was $30^{\circ}C.$ The lipase produced by Acinetobactor sp. B2 was purified by ammonium sulfate precipitation, DEAE-Toyopearl 650M ion exchange chromatography and Sephadex gel filtration chromatography. Its molecular mass was about 60 kDa and condition for the optimal activity was observed at $40^{\circ}C$ and pH 10, respectively. The activation energy of lipase for the hydrolysis of p­nitrophenyl palmitate was 2.7 kcal/mol in the temperature range of 4 to $37^{\circ}C,$ and the enzyme was unstable at the temperature higher than $60^{\circ}C.$ The Michaelis constant $(K_m)\;and\;V_{max}$ for p-nitrophenyl palmitate were 21.8 uM and $270.3\;{\mu}M\;min^{-1}mg^{-1},$ respectively. This enzyme was strongly inhibited by 10 mM $Cd^{2+},\;Co^{2+},\;Fe^{2+},\;Hg^{2+},$ EDTA and 2-Mercaptoethalol.

Causes for Abnormal Leaf Chlorosis in Chinese Jujube (Zizyphus jujuba Mill.) (대추나무 잎의 이상황화현상 원인)

  • Lee, Jae-Seog;Lee, Jung-Min;Jung, Jae-sik;Lee, Young-Sun
    • Horticultural Science & Technology
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    • v.18 no.3
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    • pp.399-403
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    • 2000
  • Recently, abnormal leaf chlorosis has been observed in jujube trees of the major production area in Kyongbuk province. To determine possible causes for the observation, physico-chemical properties of the orchard soil and nutrient contents in the jujube trees were investigated. The chlorosis symptoms were categorized into three types based on the site of chlorosis initiation; leaf center, petiole, and intravein. Of the three, leaf center chlorosis was the most common. The symptom occurred more frequently in Ihyeon, Gyuam, and Geugrag soil series with previous history of apple orchard. In general, the soil and the tree showing leaf chlorosis had lesser nutrient contents than normal except P, Fe, and Zn. In particular, Mg contents in leaf, branchlet, and fruit of the tree were as much as 4 times lesser than those in normal tree; the soil also had 7.8 times lesser Mg contents. The results indicate that the abnormal leaf chlorosis in jujube tree may be caused by nutrient deficiency in soil and could be cured by proper fertilization.

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Preconcentration and Determination of Fe(III) from Water and Food Samples by Newly Synthesized Chelating Reagent Impregnated Amberlite XAD-16 Resin

  • Tokahoglu, Serife;Ergun, Hasan;Cukurovah, Alaaddin
    • Bulletin of the Korean Chemical Society
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    • v.31 no.7
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    • pp.1976-1980
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    • 2010
  • A simple and reliable method has been developed to selectively separate and concentrate trace amounts of Fe(III) ions from water and food samples by using flame atomic absorption spectrometry. A new reagent, 5-hydroxy-4-ethyl-5,6-di-pyridin-2-yl-4,5-dihydro-2H-[1,2,4] triazine-3-thione, was synthesized and characterized by using FT-IR spectroscopy and elemental analysis. Effects of pH, concentration and volume of elution solution, sample flow rate, sample volume and interfering ions on the recovery of Fe(III) were investigated. The optimum pH was found to be 5. Eluent for quantitative elution was 10 mL of 2 M HCl. The preconcentration factor of the method, detection limit (3s/b, ${\mu}gL^{-1}$) and relative standard deviation values were found to be 25, 4.59 and 1%, respectively. In order to verify the accuracy of the method, two certified reference materials (TMDA 54.4 lake water and SRM 1568a rice flour) were analyzed. The results obtained were in good agreement with the certified values. The method was successfully applied to the determination of Fe(III) ions in water and food samples.

Olefin Polymerization Activity and Crystal Structure of Alkyliron(Ⅲ) Porphyrin Complexes

  • Oh, Yung-Hee;Swenson, Dale;Goff, Harold M.
    • Bulletin of the Korean Chemical Society
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    • v.24 no.2
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    • pp.167-172
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    • 2003
  • Alkyliron(Ⅲ) porphyrins, n-butyliron(Ⅲ) tetraphenylporphyrin, (TPP)Fe-Bu and n-butyliron(Ⅲ) tetrakis-(pentafluorophenyl)porphyrin, $(F_{20}TPP)Fe-Bu$ have been evaluated as suitable for olefin free-radical polymerization. Butyl radicals dissociated from n-butyliron(Ⅲ) porphyrin initiated the polymerization reaction, but the ratio of the propagation was low. The GCMS analysis of the reaction mixture of nbutyliron(Ⅲ) porphyrin and styrene has revealed several products containing two butyl groups, while traces of b-hydrogen-abstracted products were observed. The crystal structure of (TPP)Fe-Bu has been determined. The structure of the n-butyliron(Ⅲ) porphyrin reveals the compound containing five-coordinated iron with the average Fe-N distance of 1.973(1) Å and Fe-C of 2.030(2) Å. The iron atom is displaced by 0.137Å from a four nitrogen mean plane. Crystal system is triclinic, and space group is P-1.

Synthesis and Structure of trans$[FeH(NCCH_2CH_2CH_2Cl)(dppe)_2]^+[BF_4]^-$ ($[FeH(NCCH_2CH_2CH_2Cl)(dppe)_2]^+[BF_4]^- $착물의 합성 및 구조)

  • 이재경;이순원
    • Korean Journal of Crystallography
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    • v.9 no.2
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    • pp.107-113
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    • 1998
  • Ar하에서 trans-FeHCl(dppe)2, 1을 4-chlorobutyronitrile에 녹이면, 착물 trans-[FeH(NCCH2CH2CH2Cl)(dppe)2]Cl, 2가 생성되고, 2는 NaBF4와 반응하여 착물 trans-[FeH(NCCH2CH2CH2Cl)(dppe)2][BF4], 3로 변환된다. 착물 3의 결정학 자료: 단사정계 공간군 P21/c, a=13.540(2) , b=17.058(3) , c=21.853(4) , β=90.15(1)o, Z=4, R(wR2)=0.0524(0.1239).

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