• Corrosion Science and Technology
• /
• 제12권4호
• /
• pp.163-170
• /
• 2013

In NaCl solutions acidified with $H_2SO_4$, Fe20Cr1.1N alloy showed enhanced pitting corrosion resistance than Fe20Cr alloy. An XPS analysis revealed that the passive film of Fe20Cr1.1N alloy contained higher cationfraction of Cr than that of Fe20Cr alloy, and nitrogen was incorporated into the film. In addition, it was found that the passive film of Fe20Cr1.1N alloy was thinner and had higher oxygen vacancy density than that of Fe20Cr alloy. Based on these observations, it was concluded that the chemical composition was the determining factor for the protectiveness of the passive film of Fe20Cr based alloy in dilute $H_2SO_4$ solution.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 1988년도 추계학술대회 논문집
• /
• pp.5-7
• /
• 1988

Effect of isothermal aging on the crystallization of $Fe_{78}B_{13}Si_{9}$ metallic glass has been investigated by electrical resistivity, X-ray measurements, bending test, thermal analysis and transmission electron microscopy. Amorphous $Fe_{78}B_{13}Si_{9}$ alloy was annealed isothermally for 5 to 1200 mon. between 300 C and 540 C. It has been found that close relation between relative resistivity and X-ray diffraction pattern showed. The crystalline peak of $\alpha$-(Fe, Si) and Fe$_2$B are detected by X-ray experiment. The crystalline phases observed by TEM show $\alpha$-(Fe, Si) and Fe$_3$B with dendritic and cylindrical morphology, respectively. It has been also found that the embrittleness of aged samples rapidly increased with the crystallization and was shown before the crystallization.th the crystallization and was shown before the crystallization.

• 한국분말재료학회지
• /
• 제11권3호
• /
• pp.242-246
• /
• 2004

FePt nanoparticles for high-density magnetic recording media were synthesized by the simultaneous chemical reduction of Fe(acac) $_2$ and Pt(acac) $_2$ with 1,2-hexadecanediol as the reducing reagent. TEM images showed that the shape of as-synthesized FePt nanoparticle was spherical and average particle size was 3 nm. Also, SAD pattern showed that crystal structure was disordered FCC (face centered cubic). These FCC structured nanoparticles were transformed FCT (face centered tetragonal) structure by annealing at 55$0^{\circ}C$ for 30 min in Ar atmosphere. XRD analysis revealed that as-synthesized FePt nanoparticles were transformed from disordered FCC to ordered FCT. Finally, the coercivity of 2 kOe for FePt nanoparticles with FCT structure was obtained by VSM measurement.

• 헤리티지:역사와 과학
• /
• 제40권
• /
• pp.413-430
• /
• 2007

우리나라 저습지에서 출토되는 목제유물은 대부분 흑갈색을 띠고 있다. 이와 같은 현상은 매장 환경의 주체인 토양성분에 기인한다고 할 수 있다. 예를 들면 광주 동림동 저습지 유적과 창녕 송현동 고분군 내의 토양성분을 비교 분석한 결과 두 유적 모두 Si, AI, Fe 등의 함유량이 높게 나타난 바가 있다. 또한 신안선과 광주 동림동 및 창녕 송현동 고분 출토 목재의 무기물 분석에서도 모두 토양의 주성분인 Si보다 Fe의 함유량이 상대적으로 높은 수치를 나타냈으며, 성분과 함유량에 있어서도 유사함을 보였다. 출토지가 다름에도 불구하고 Fe 함량에서 유사한 결과를 나타내는 것은 일반적으로 매장 환경의 영향을 크게 받는다는 근거자료가 될 수 있는 것이다. 그 중 Fe는 목재의 열화로 생성된 타닌과 반응하여 타닌산 제I철이 되고, 산소와 결합하여 타닌산 제II철이 되므로 흑색을 띠게 된다. 이러한 목재흑화의 주원인이라고 할 수 있는 Fe은 EDTA를 사용하여 킬레이트 화합물을 형성함으로써 제거가 가능하다. EDTA를 통해 흑화된 목재에서 Fe을 제거하는 실험을 한 결과 EDTA-2Na가 가장 효율적이었으며, 72시간 동안 반응 후 용액을 제거하고 다시 EDTA와 반응시켜 Fe을 제거하는 방법이 가장 효과적으로 흑화현상을 제거할 수 있었다.

• 소성∙가공
• /
• 제9권3호
• /
• pp.293-303
• /
• 2000

Recent developments of Fe technology make it possible to apply CAD/CAE/CAM techniques successfully to the stamping die design among the automotive parts industries. Those successful applications are greatly attributable to the development of commercial S/W. Up to now most commercial S/W for the analysis of sheet metal forming is based on the dynamic explicit algorithm. The main characteristics of dynamic explicit algorithm is that there is no convergence problem if the time increment is taken less than the stability limit. The stability of the analysis is guaranteed in the commercial code, since the adequate time increment is computed from the so called "Courant Condition". However excess computing time is often pointed out in the dynamic explicit analysis according to the characteristics of process parameters taken. In the study, various parameters that may affect the stability and the method how to improve computational efficiency of analysis have been investigated.estigated.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2000년도 추계학술대회논문집A
• /
• pp.446-451
• /
• 2000

In this paper, a S/W system for a structural analysis of machine tools has been suggested. The system is so designed to reduce manual interfacing effort. An object-oriented language is used for making a graphic user interface. In this system parametric modelling technique is applied to construct a FE model without much user intervention. The FE model is automatically updated when the design parameters are changed by user. Not only single FE analysis but also a trade-off analysis for calculating the sensitivity information of design variables is possible using this system. All data generated by this system are saved in the database. So it possible to retrieve the result later without another analysis. It is found that the design time can be reduced and unnecessary operation avoided using this system.

• 한국정밀공학회지
• /
• 제25권8호
• /
• pp.80-87
• /
• 2008

This paper investigated into the impact characteristics of the stainless sheet with thickness of 0.7 mm on the stretching boundary condition through three-dimensional finite element analysis. High speed tensile tests were carried out to obtain strain-stress relationships with the effects of the strain rate. The FE analysis was performed by the ABAQUS explicit code. In order to improve an accuracy of the FE analysis, the hyper-elastic model and the damping factor were introduced. Through the comparison of the results of the FE analyses and those of the impact tests, a proper FE model was obtained. The results of the FE analyses showed that the absorption rate of energy maintains almost 82.5-83.5% irrespective of the impact energy level and the diameter of the impact head. From the results of FE analyses, variations of stress, strain, dissipation energy, strain energy density, and local deformation characteristics in the stainless sheet during the collision and the rebound of the impact head were quantitatively examined. In addition, it was shown that the fracture of the specimen occurs when the plastic strain is 0.42 and the maximum value of the plastic dissipation energy of the specimen is nearly 1.83 J.

• 콘크리트학회논문집
• /
• 제25권5호
• /
• pp.529-537
• /
• 2013

이 연구의 목적은 하중기반 유한요소 정식화에 의한 FRP 보강된 철근콘크리트 보 또는 기둥 부재의 비선형 층상화의 등매개 골조 유한요소모델을 개발하는데 있다. 단면에서 콘크리트는 3축 응력-변형률 관계로 모델화하고 FRP 피복층은 2차원의 적층복합재료로 모델화하였다. 하중기반 유한요소의 요소강성행렬은 변위형상함수의 가정이 없고 하중보간함수를 갖고 있다. 횡 하중을 받는 GFRP 시트 보강된 철근콘크리트 기둥의 실험에 대해 개발된 하중기반 유한요소모델에 의한 해석을 수행하였다. 기존 강성도법의 유한요소해석과 비교하여 하중기반 유한요소해석은 전체적인 하중-변위 관계 뿐만 아니라 기둥의 소성힌지영역에서의 비선형 변형 및 손상을 보다 정확히 예측해 주었다.

• Structural Engineering and Mechanics
• /
• 제80권6호
• /
• pp.645-655
• /
• 2021

Performance-based reliability analysis is a practical approach to investigate the seismic performance and stochastic nonlinear response of structures considering a random process. This is significant due to the uncertainties involved in every aspect of the analysis. Therefore, the present study aims to evaluate the performance-based reliability within a stochastic finite element (FE) framework for reinforced concrete (RC) shear walls that are considered as one of the most essential elements of structures. To accomplish this purpose, deterministic FE analyses are conducted for both squat and slender shear walls to validate numerical models through experimental results. The presented numerical analysis is performed by using the ABAQUS FE program. Afterwards, a random-effects investigation is carried out to consider the influence of different random variables on the lateral load-top displacement behavior of RC members. Using these results and through utilizing the Monte-Carlo simulation method, stochastic nonlinear analyses are also performed to generate random FE models based on input parameters and their probabilistic distributions. In order to evaluate the reliability of RC walls, failure probabilities and corresponding reliability indices are calculated at life safety and collapse prevention levels of performance as suggested by FEMA 356. Moreover, based on reliability indices, capacity reduction factors are determined subjected to shear for all specimens that are designed according to the ACI 318 Building Code. Obtained results show that the lateral load and the compressive strength of concrete have the highest effects on load-displacement responses compared to those of other random variables. It is also found that the probability of shear failure for the squat wall is slightly lower than that for slender walls. This implies that 𝛽 values are higher in a non-ductile mode of failure. Besides, the reliability of both squat and slender shear walls does not change significantly in the case of varying capacity reduction factors.

• 대한조선학회논문집
• /
• 제45권4호
• /
• pp.411-416
• /
• 2008

A strength problem of propeller blades for large container ships at astern condition has been occasionally reported due to the application of a highly skewed propeller which can reduce the hull surface fluctuation forces. A finite element analysis code for propeller blade was developed and utilized since 1985. Recently, however, further fine mesh modeling for finite element analysis is required to yield higher accuracy in the analysis. The present study shows an application of FE analysis code to the highly skewed propeller for large container ships. Results of FE analysis show that the number of FE mesh affects largely on strength, and also the calculated strength with fine mesh gives good agreements to those of other FEM codes. A method to enlarge strength near the trailing edge was introduced considering the strength criterion on the blade.