• Title/Summary/Keyword: FE experiment

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Investigation of Synthesis and Antibacterial Properties of a Magnetically Reusable Fe3O4-ACCS-Ag Nanocomposite (재사용이 가능한 나노복합재료 Fe3O4-ACCS-Ag의 제조 및 항균 특성 평가)

  • Shim, Jaehong;Kim, Hea-Won;Kim, Jin-Won;Seo, Young-Seok;Oh, Sae-Gang;Cho, Min;Park, Junghee;Oh, Byung-Taek
    • Journal of Soil and Groundwater Environment
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    • v.20 no.3
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    • pp.25-33
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    • 2015
  • In this study, Fe3O4-ACCS-Ag nanoparticles (NPs) were successfully synthesized using silica extracted from corn cob ash. The synthesized Fe3O4-ACCS-Ag NPs were characterized using X-ray diffraction (XRD), scanning electron microscopyenergy dispersive X-ray spectroscopy (SEM-EDX), transmission electron microscopy (TEM) and fourier transform infrared spectroscopy (FTIR). In addition, the potential application of Fe3O4-ACCS-Ag NPs as an antibacterial material in water disinfection was investigated using Escherichia coli ATCC 8739 as model bacteria. The antibacterial activity of synthesized composite material showed 99.9% antibacterial effect within 20 min for the tested bacteria. From this experiment, the synthesized Fe3O4-ACCS-Ag nanocomposites also hold magnetic properties and could be easily recovered from the water solution for its reuse. The reused nanocomposites presented the decreasing antibacterial efficiencies with the reuse cycle but the composite used three times still killed 90% of bacteria in 20 min.

Root Starch Yield and Physio-Chemical Characteristics of Bracken (Pteridium aquilinum Kuhn) according to Harvesting Time (고사리 뿌리의 채취시기에 따른 전분 추출수율과 이화학적 특성)

  • Jung-Seob Moon;Gue-Saeng, Yeom;Song-Hee Ahn;;Dong-Chun Cheong
    • Proceedings of the Plant Resources Society of Korea Conference
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    • 2020.12a
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    • pp.74-74
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    • 2020
  • 고사리(Pteridium aquilinum Kuhn)는 고사리 속(Pteridium spp.)에 속하는 양치식물의 총칭으로서 우리나라에는 22과 70속 272종이 분포되어 있는 것으로 보고되었다. 고사리의 어린 순에는 가식부 100g 당 칼슘 15.0mg, 칼륨 185.0mg 등이 함유되어 있으며 골다공증, 심혈관 질환 등에 효과가 있고 식이섬유로 인해 변비 예방에도 유용한 것으로 알려져 있다. 우리나라의 고사리 재배면적은 2019년 기준 5,349ha 수준을 보이고 있으며 전체 산채류 재배면적에서 26%의 비중을 차지하고 있으나 재배면적의 증가에 따라 고사리 재배의 부가가치를 높일수 있는 방안이 요구되고 있는 실정으로 그 중 고사리 뿌리에서 추출한 전분은 중국 및 일본 등지에서 면류나 제과용으로 이용되고 있어 고사리 재배의 부가가치를 향상시킬 수 있는 방안으로 기대되고 있다. 본 연구에서는 고사리 뿌리의 채취시기에 따른 뿌리 전분의 생산성과 이화학적 특성을 조사하기 위해 2020년 3월 26일부터 10월 28일 까지 5회에 걸쳐 뿌리를 수확하여 세척한 후 고무망치로 파쇄하고 수침 방법을 이용해 추출한 전분의 추출수율과 이화학적 특성을 조사하였다. 채취시기별 고사리 뿌리의 생산성은 7월 27일 수확에서 3,783.3kg/10a로 유의하게 높은 수량을 보였다. 파쇄한 고사리 뿌리를 24시간 sodium metabisulfite 0.4% V/W 용액에 수침하여 전분을 추출한 후 24시간 간격으로 3회에 걸쳐 진탕, 침전과 세척의 과정을 거친 후 조사한 전분 추출 수율은 3월 26일 수확한 뿌리에서 7.6%로 가장 높았고 7월 27일과 9월 24일 채취한 경우에서는 전분이 검출되지 않았으며 10월 28일에는 4.9%의 유의하게 낮았다. 추출한 전분의 색도분석에서 L값은 채취시기가 늦어질수록 높아지는 경향을 보였고 a, b값은 낮아지는 경향을 보여 전분의 색도가 향상되는 경향을 보였으며, 신속점도측정기로 조사한 전분의 호화특성에서는 채취시기가 늦어질수록 전분의 최고점도는 높아졌으나 최저점도 및 최종점도는 낮아지는 경향을 나타냈다. 전분의 무기물 함량은 3월 26일과 5월 25일 채취하는 경우 Fe > Ca > Mg > K > P의 순으로 함량이 높았으나 10월 28일 채취한 경우에서는 Fe와 Ca이 감소되고 K 함량은 증가하여 Ca > Fe > Mg > K > P의 순으로 무기물 함량이 높게 나타났다.

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Effect of Liquid Fertilizer Contained Medium of Lactobacillus sp. and Saccharomyces sp. on Growth of Creeping Bentgrass (유산균과 효모균 배양액 함유 액비 시용이 크리핑 벤트그래스의 생육에 미치는 영향)

  • Kim, Young-Sun;Ham, Suon-Kyu;Lee, Sang-Jin
    • Asian Journal of Turfgrass Science
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    • v.24 no.2
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    • pp.138-144
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    • 2010
  • This study was conducted to investigate the effect of Lactobacillus sp. and Saccharomyces sp. on turf quality, shoot and root growth of creeping betgrass in golf course by measuring turf color index, chlorophyll content, dry weight of shoot and root, T/R ratio and root length. Fertilizer treatment was designed as follows; nonfertilizer (NF), control (CF; compound fertilizer), microorganism medium(MO; CF+MO)), microorganism medium contained Fe(MO-Fe; CF+MO-Fe) and microorganisum medium contained S (MO-S; CF+MO-S). Soil properties investigated after experiment was scarcely affected by applied fertilizers in root zone of creeping bentgrass. The turf color index and chlorophyll index of MO, MO-Fe, MO-S treatment were higher than those of NF, and similar to those of CF. The turfgrass root in MO and MO-Fe treatment was longer than others. The dry weight of shoot in MO and MO-S was higher than CF and that of root in MO and MO-Fe, and dry weight of MO was increased than that of NF and CF, by 26% and 6%, respectively. AS compared with NF, T/R ratio of CF, MO, MO-Fe and MO-S was increased, and MO and MO-Fe was similar to CF, MO-S higher. Nutrient content in CF, MO, MO-Fe and MO-S was contained more than in NF, and it was higher in shoot. These was suggested that application of MO induced the development of quality and growth of creeping bentgrass by assisting root growth and nutrients uptake.

Electrochemical Properties of Diiron Complexes wish Conjugated Chains (공액 사슬을 갖는 철 화합물의 전기화학적 특성)

  • ;Micheal b. Sponsler
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.6
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    • pp.511-517
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    • 2002
  • The complex 1 $([Cp*Fe(CO)_2]_2-(\mu-CH=CH-CH=CH))$ which have butadiene as a bridge were synthesized from $Cp*(CO)_2FeK$ and cis-3,4-dichlorocyclobutene. The derivatives of complex 1 where one or two carbonyl groups are replaced by phosphine ligands have been prepared by photochemical substitution. The new derivatives $([Cp*Fe(L)_2]_2-(\mu-CH=CH-CH=CH))$ where L = $(Ph_2PCH_2CH_2PPh_2)$ and $([Cp*Fe(CO)(L)]_2-(\mu-CH=CH-CH=CH))$ where L : $PPh_3$ have been characterized from $^^1H-$, $^^13C-$,$^^31P-NMR$ and elemental analysis. Obtained complexes have been studied in electrochemical experiment and UV/VIS-near-IR. The mixed-valence radical cation forms of complex 2, 3 species were found to be delocalized as the Class III. Based on the separation of the waves ($\triangle E$ : 0.470 ~ 0.605 V), the efficiency of electronic communication between two metal centers of cation species leading to stabilization relative to neutral species. The phosphine-substitute complexes (2, 3) displays two reversible oxidation waves and oxidation state of metal centers-dependent color change, electrochromism, was observed from yellow to orange and deep blue in methylene chloride.

The first of its kind metallicity map of the Large Magellanic Cloud

  • Choudhury, Samyaday;Subramaniam, Annapurni;Cole, Andrew A.
    • The Bulletin of The Korean Astronomical Society
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    • v.41 no.2
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    • pp.30.1-30.1
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    • 2016
  • We have estimated a metallicity map of the Large Magellanic Cloud (LMC) using the Magellanic Cloud Photometric Survey (MCPS) and Optical Gravitational Lensing Experiment (OGLE III) photometric data. This is a first of its kind, high-spatial resolution map of metallicity up to a radius of $4^{\circ}-5^{\circ}$, derived using large area photometric data and calibrated using spectroscopic data of Red Giant Branch (RGB) stars. The RGB is identified in the V, (V - I) colour- magnitude diagrams of small subregions of varying sizes in both data sets. The slope of the RGB is used as an indicator of the mean metallicity of a subregion, and it is calibrated to metallicity using spectroscopic data for field and cluster red giants in selected subregions. The mean metallicity of the LMC is found to be [Fe/H] = -0.37 dex (${\sigma}[Fe/H]=0.12$) from MCPS data, and [Fe/H] = -0.39 dex (${\sigma}[Fe/H]=0.10$) from OGLE III data. The bar is found to have an uniform and higher metallicity compared to the disk, and is indicative of an active bar in the past. Both the data sets suggest a shallow radial metallicity gradient up to a radius of 4 kpc ($-0.049{\pm}0.002$ dex kpc-1 to $-0.066{\pm}0.006$ dex kpc-1). This metallicity gradient of the LMC disk, though shallow, resembles the gradient seen in spiral galaxies, and similar to that found in our Galaxy.

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Finite element analysis of shear-deficient RC beams strengthened with CFRP strips/sheets

  • Lee, H.K.;Ha, S.K.;Afzal, M.
    • Structural Engineering and Mechanics
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    • v.30 no.2
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    • pp.247-261
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    • 2008
  • Performance of shear-deficient reinforced concrete (RC) beams strengthened with carbon fiber-reinforced polymer (CFRP) strips/sheets is analyzed through numerical simulations on four-point bending tests. The numerical simulations are carried out using the finite element (FE) program ABAQUS. A micromechanics-based constitutive model (Liang et al. 2006) is implemented into the FE program ABAQUS to model CFRP strips/sheets. The predicted results are compared with experiment data (Khalifa and Nanni 2002) to assess the accuracy of the proposed FE analysis approach. A series of numerical tests are conducted to investigate the influence of stirrup lay-ups on the shear strengthening performance of the CFRP strips/sheets, to illustrate the influence of the damage parameters on the microcrack density evolution in concrete, and to investigate the shear and flexural strengthening performance of CFRP strips/ sheets. It has been shown that the proposed FE analysis approach is suitable for the performance prediction of RC beams strengthened with CFRP strips/sheets.

Preparation and Electromagnetic Properties of an Electromagnetic Wave Absorber

  • Sun, Chang;Sun, Kangning;Pang, Laixue;Liu, Jian
    • Journal of Magnetics
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    • v.21 no.1
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    • pp.61-64
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    • 2016
  • In this study, we report the as-prepared MgO-doped $BaFe_{12}O_{19}$, which was prepared by calcination technique and high-energy ball milling process, as an electromagnetic wave absorber. The phase analysis of $BaFe_{12}O_{19}$ and the as-prepared MgO-doped $BaFe_{12}O_{19}$ was detected utilizing X-ray Diffractometer (XRD). The microstructure was characterized using Scanning Electron Microscope (SEM). By means of the transmission/reflection coaxial line method, the electromagnetic properties and microwave absorbing properties of the as-prepared electromagnetic wave absorber were studied. It is found that the electromagnetic wave absorber has a minimum reflection loss value of -41 dB at 4.27 GHz with a matching thickness of 2.6 mm. The experiment results revealed that the as-prepared electromagnetic wave absorber could find potential applications in many military as well as commercial industries.

Periodicity Dependence of Magnetic Anisotropy and Magnetization of FeCo Heterostructure

  • Kim, Miyoung
    • Journal of Magnetics
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    • v.21 no.1
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    • pp.6-11
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    • 2016
  • The magnetic anisotropy energy (MAE) and the saturation magnetization $B_s$ of (110) $Fe_nCo_n$ heterostructures with n = 1, 2, and 3 are investigated in first-principles within the density functional theory by using the precise full-potential linearized augmented plane wave (FLAPW) method. We compare the results employing two different exchange correlation potentials, that is, the local density approximation (LDA) and the generalized gradient approximation (GGA), and include the spin-orbit coupling interaction of the valence states in the second variational way. The MAE is found to be enhanced significantly compared to those of bulk Fe and Co and the magnetic easy axis is in-plane in agreement with experiment. Also the MAE exhibits the in-plane angle dependence with a two-fold anisotropy showing that the $[1{\overline{I}}0]$ direction is the most favored spin direction. We found that as the periodicity increases, (i) the saturation magnetization $B_s$ decreases due to the reduced magnetic moment of Fe far from the interface, (ii) the strength of in-plane preference of spin direction increases yielding enhancement of MAE, and (iii) the volume anisotropy coefficient decreases because the volume increase outdo the MAE enhancement.

A Study on the Forming of Automotive Front Side Member Part with Ultra High Strength Steel of DP980 (980MPa급 초고장력 강판의 자동차 프런트 사이드 멤버 부품 성형에 관한 연구)

  • Cha, C.H.;Lee, S.K.;Ko, D.C.;Kim, B.M.
    • Transactions of Materials Processing
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    • v.18 no.1
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    • pp.39-44
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    • 2009
  • This paper is concerned with forming technology of an automotive front side member part with ultra high strength steel sheet of DP980. The forming technology considered in this paper is the draw & form type, which installs the upper pad and lower pad to produce the complicated shape of ultra high strength steel sheet. In order to produce sound product, comparison between form type and draw & form type and between draw type and draw & form type are investigated by FE-analysis. FE-analysis is carried out with commercial sheet metal forming analysis S/W, DYNAFORM. It was shown from FE-analysis that the draw & form type satisfied the required specifications such as the dimensional accuracy and soundness of automotive front side member part. The effectiveness of the analytical result was verified by the experiment. From this investigation, the draw & form type is proved to be able to supply useful forming technology in forming ultra high strength steel.

Fabrication of Nanostructured Fe-Co powders by Mechanical Alloying and Their Magnetic Properties (기계적 합금화에 의한 나노구조 Fe-Co 합금분말의 제조 및 자성특성)

  • 정진영
    • Journal of Powder Materials
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    • v.6 no.1
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    • pp.27-35
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    • 1999
  • A study was made on the fabrication of nanostructured Fe-Co powders by mechanical alloying and their magnetic properties. Microstrural development during the process of MA was inverstigated by means of X-ray diffraction, differential thermal analyzer, scanning electron microscopy and transmission electron microscopy. The magnetic properties of NS Fe-Co powders were evaluated through the measurements of the saturation magnetization $(M_s)$ as well as the coercivity $(H_c)$. The average grain size calculated from line braodening in XRD peak was about 10nm or less and confirmed by TEM. In this experiment, two different milling methods (cycle opertion and conventional milling) were used. Cycle operation had an advantage over the conventional milling method in that more refined powders can be obtained. Solid state alloying of the components was confirmed from both the change of the saturation magnetization and the change of lattice parameter with Co contentration. Maxium $M_s$ was obtained at the composition of 30at.%Co. Relatively high coercivities of 10~150e were obtained for the compositions investigated, and this seems to be due to the high amount of internal strain introduced during milling.