• Title/Summary/Keyword: Extraction methods

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Preparation of High Quality Safflower (Carthamus tinctorius L.) Seed Extract by High-Pressure Extraction Process

  • Seo, Il-Ho;Choi, Sang-Won
    • Preventive Nutrition and Food Science
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    • v.14 no.4
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    • pp.373-377
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    • 2009
  • Safflower seed extract was prepared by a high-pressure extraction technology and its quality characteristics were compared to that of other conventional extraction techniques, such ultrasonic and reflux extractions. Safflower seeds were extracted with 80% aqueous ethanol by three above extraction methods, and further fractionated with Diaion HP-20 column chromatography to obtain a partially purified safflower seed extract (PPSSE). Among the three extraction techniques examined, the reflux extraction showed the higher yields of EtOH extract and PPE than the ultrasonic and high-pressure extractions. Levels of most phenolic compounds in the EtOH extract of safflower seed are higher in reflux and ultrasonic extractions than the high pressure extraction, but levels of two serotonin aglycones, N-(p-coumaroyl)serotonin (CS) and N-feruloylserotonin (FS), in PPSSE were higher in the high pressure extraction than the reflux and ultrasonic extractions. In addition, color values (L and a) of the PPSSE were higher in the high-pressure extraction than the reflux and ultrasonic extractions, although there were no significant differences in pH and UV maxima absorption spectra among three extraction techniques. These results indicate that the high-pressure extraction technology is a simple and effective extraction for preparation of a high quality of safflower seed extract containing CS and FS with anti-wrinkle activity.

Physicochemical Characteristics of Coffee Extracts Using Different Extraction Methods (커피의 추출방법에 따른 이화학적 특성)

  • Eun, Jong-Bang;Jo, Mi-Yeon;Im, Ji-Soon
    • Korean Journal of Food Science and Technology
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    • v.46 no.6
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    • pp.723-728
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    • 2014
  • The physicochemical characteristics of coffees extracted using 7 different extraction methods were investigated. The pH values of coffees extracted via different extraction methods ranged from 5.26 to 5.54, and coffee extracted by Ibrik had the highest pH among all samples. The soluble solid content and titratable acidity of coffee extracted using an Espresso machine were significantly higher than those obtained using other extraction methods. Furthermore, the total phenol and caffeine contents of coffee extracted using an Espresso machine were 6.46 and 2.65 mg/mL, respectively. In regard to color, the $L^*$, $a^*$ and $b^*$ values of coffee extracted via different extraction methods were in the ranges of 0.81-38.94, 4.49-37.75, and 0.71-66.42, respectively. In regard to the phenolic compounds, the chlorogenic acid, caffeic acid and ferulic acid contents of coffee extracted using an Espresso machine were higher than those obtained by other extraction methods at 0.15 mg/mL, $0.075{\mu}g/{\mu}L$, and $0.019{\mu}g/{\mu}L$, respectively.

Effects of Extraction Methods on the Antioxidative Activity of Artemisia sp. (추출 방법에 따른 쑥 추출물의 항산화 활성)

  • Kang, Kyoung-Myoung;Lee, Shin-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.42 no.8
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    • pp.1249-1254
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    • 2013
  • The effect of extraction methods, such as reflux extraction (RE), autoclave extraction (AE), low temperature high pressure extraction (LTPE) and ultrasonification extraction (USE) on antioxidant activity of various species of Artemisia (Artemisia capillaris T., Artemisia princeps P., Artemisia annua L.) was investigated. The extraction yield of RE and AE was higher than other methods tested for all Artemisia. The total polyphenol and flavonoid content of Artemisia sp. extracts from RE was highest of the extraction methods tested. The total polyphenol and flavonoid content of A. capillaris T. extracted by RE was 260.82 mg GAE/g and 11.52 mg RHE/g, respectively. The A. capillaris T. extract showed higher DPPH and ABTS radical scavenging activity than that of the other tested Artemisia sp. Nitrite scavenging activity and superoxide dismutase (SOD)-like activity of various extracts from RE was 45.48% and 68.29% (A. capillaris T.), 45.73% and 61.43% (A. princeps P.), and 44.25% and 58.19% (A. annua L.), respectively. The RE method was the most effective method for extracting antioxidant substances from various A. capillaris T. compared with AE, LTPE and USE. These results suggest that extracts of Artemisia sp. from RE can be used as bioactive and functional materials in the food industry.

Health Risk Assessment of Lead Ingestion Exposure by Particle Sizes in Crumb Rubber on Artificial Turf Considering Bioavailability

  • Kim, Sun-Duk;Yang, Ji-Yeon;Kim, Ho-Hyun;Yeo, In-Young;Shin, Dong-Chun;Lim, Young-Wook
    • Environmental Analysis Health and Toxicology
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    • v.27
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    • pp.5.1-5.10
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    • 2012
  • Objectives: The purpose of this study was to assess the risk of ingestion exposure of lead by particle sizes of crumb rubber in artificial turf filling material with consideration of bioavailability. Methods: This study estimated the ingestion exposure by particle sizes (more than 250 um or less than 250 um) focusing on recyclable ethylene propylene diene monomer crumb rubber being used as artificial turf filling. Analysis on crumb rubber was conducted using body ingestion exposure estimate method in which total content test method, acid extraction method and digestion extraction method are reflected. Bioavailability which is a calibrating factor was reflected in ingestion exposure estimate method and applied in exposure assessment and risk assessment. Two methods using acid extraction and digestion extraction concentration were compared and evaluated. Results: As a result of the ingestion exposure of crumb rubber material, the average lead exposure amount to the digestion extraction result among crumb rubber was calculated to be $1.56{\times}10^{-4}$ mg/kg-day for low grade elementary school students and $4.87{\times}10^{-5}$ mg/kg-day for middle and high school students in 250 um or less particle size, and that to the acid extraction result was higher than the digestion extraction result. Results of digestion extraction and acid extraction showed that the hazard quotient was estimated by about over 2 times more in particle size of lower than 250 um than in higher than 250 um. There was a case of an elementary school student in which the hazard quotient exceeded 0.1. Conclusions: Results of this study confirm that the exposure of lead ingestion and risk level increases as the particle size of crumb rubber gets smaller.

Ingredient Contents of Nipa Palm(Nypa fruticans Wurmb.) according to Different Extraction Methods (추출방법에 따른 니파팜의 성분 함량)

  • Kim, Myong-Ki
    • Journal of Convergence for Information Technology
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    • v.11 no.5
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    • pp.104-110
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    • 2021
  • This study was conducted to confirm the change in the contents of the ingredients according to the extraction method of nipa palm. The contents were analyzed by extraction according to the ethanol ratio, extraction time, and extraction temperature. The contents of polyphenols and flavonoids according to the ratio of the extraction solvent were the highest at 36.91 and 27.62 mg/g, respectively, when extracted with 50% ethanol. Polyphenols and flavonoids according to extraction temperature and extraction time showed the highest content of 40.83 and 37.63 mg/g, respectively, when extracted for 6 hours at 60℃. The contents of the major component of nipa palm according to the ethanol ratio were 2.08 mg/g in 70% ethanol for 5-O-caffeoylshikimic acid, 0.10 mg/g for 4-hydroxybenzoic acid in 30% ethanol, and 0.12 mg/g for 3,4- hydroxybenzoic acid in 50% ethanol. It is expected that it can be used as basic research data when developing natural materials such as food and cosmetics through the change in the contents of the ingredients contained in nipa palm according to the extraction methods.

Optimal feature extraction for normally distributed multicall data (가우시안 분포의 다중클래스 데이터에 대한 최적 피춰추출 방법)

  • 최의선;이철희
    • Proceedings of the IEEK Conference
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    • 1998.10a
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    • pp.1263-1266
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    • 1998
  • In this paper, we propose an optimal feature extraction method for normally distributed multiclass data. We search the whole feature space to find a set of features that give the smallest classification error for the Gaussian ML classifier. Initially, we start with an arbitrary feature vector. Assuming that the feature vector is used for classification, we compute the classification error. Then we move the feature vector slightly and compute the classification error with this vector. Finally we update the feature vector such that the classification error decreases most rapidly. This procedure is done by taking gradient. Alternatively, the initial vector can be those found by conventional feature extraction algorithms. We propose two search methods, sequential search and global search. Experiment results show that the proposed method compares favorably with the conventional feature extraction methods.

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Size-Independent Caption Extraction for Korean Captions with Edge Connected Components

  • Jung, Je-Hee;Kim, Jaekwang;Lee, Jee-Hyong
    • International Journal of Fuzzy Logic and Intelligent Systems
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    • v.12 no.4
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    • pp.308-318
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    • 2012
  • Captions include information which relates to the images. In order to obtain the information in the captions, text extraction methods from images have been developed. However, most existing methods can be applied to captions with a fixed height or stroke width using fixed pixel-size or block-size operators which are derived from morphological supposition. We propose an edge connected components based method that can extract Korean captions that are composed of various sizes and fonts. We analyze the properties of edge connected components embedding captions and build a decision tree which discriminates edge connected components which include captions from ones which do not. The images for the experiment are collected from broadcast programs such as documentaries and news programs which include captions with various heights and fonts. We evaluate our proposed method by comparing the performance of the latent caption area extraction. The experiment shows that the proposed method can efficiently extract various sizes of Korean captions.

Comparison of Multi-element Extraction Methods to Determine Available Phosphate and Exchangeable Cations of Korean Soils (토양의 유효태 인산과 치환성 양이온의 다성분동시추출 분석방법 비교)

  • Kim, Myung-Sook;Yang, Jae Eui;Kim, Yoo-hak;Yoon, Jung-Hui;Zhang, Yong-Seon;Kwak, Han-Gang;Ha, Sang-Keon;Hyun, Byung-Keun
    • Korean Journal of Soil Science and Fertilizer
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    • v.42 no.3
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    • pp.192-200
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    • 2009
  • Soil testing is one of the best management practices for sustainable agriculture. Recently, as increasing soil testing needs, simplification of soil analytical procedure has been required. To determine recommendable multi-element extractant, the soil testing results of available phosphate and exchangeable cations between the conventional methods (Lancaster and 1M $NH_4OAc) and multi-element extraction methods such as Mehlich III, Modified Morgan and Kelowna methods were compared. There were highly significant correlation between the conventional methods and multi-element extraction methods (Mehlich III, Modified Morgan and Kelowna) for available phosphate and exchangeable K, Ca, Mg and Na. The coefficients of determination ($R^2) between available phosphate extracted by Lancaster method and multielement extraction methods were in the order of Mehlich III ($0.979^{***}$) > Kelowna ($0.977^{***}$) > Modified(Mod.). Morgan ($0.553^{***}$). For exchangeable cations, there were highly significant correlations between 1M $NH_4OAc method and Mehlich III, Mod. Morgan and Kelowna. However, exchangeable K, Ca and Mg by Mehlich III method were more highly correlated with conventional method than other methods. Therefore, Mehlich III extraction method could be recommended as a single extractant for simultaneous measurement using ICP in the analysis of avaliable phosphate and exchangeable cations.

Complexing Capacity - A Measure of Evaluating Water Quality

  • Akaiwa, Hideo;Itabashi, Hideyuki
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.1089-1094
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    • 1995
  • Methods for the measurement of copper(II) complexing capacity (CuCC) of natural waters by using the back-extraction of bis(benzoyl-trifluoroacetonate)copper(II) and the extraction rate of dithizonato-copper(II) complex were described. Experimental results show that the CuCC of the Kiryu river water samples from urban area were consistently larger than those from up-stream, due to a ligand which originated from human activities.

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The influences of extraction time and pressure on the chemical characteristics of Gyejibokryeong-hwan decoctions

  • Kim, Jung-Hoon;Lee, Nari;Shin, Hyeun-Kyoo;Seo, Chang-Seob
    • The Korea Journal of Herbology
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    • v.29 no.6
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    • pp.1-6
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    • 2014
  • Objectives : This study was aimed to compare Gyejibokryeong-hwan (GBH) decoctions produced using different pressure levels for various extraction times to find the optimal extraction conditions through extraction yield, total soluble solids content (TSSC), hydrogen ion concentration (pH), and the contents of chemical compounds. Methods : Decoctions of GBH were prepared under the pressure levels of 0 or $1kgf/cm^2$ for 30-180 min using water as extraction solvent. The extraction yield, TSSC, and pH were measured, and the amounts of the chemical compounds were determined using high performance liquid chromatography-photodiode array detector. Results : The higher pressure and longer extraction time increased the values of TSSC and extraction yield, while decreased the pH value. The decoctions produced in 180 min by pressurized method and produced in 150 min by non-pressurized method showed maximum values of extraction yield and TSSC with minimum value of pH. The amounts of chemical compounds showed variations in pressurized and non-pressurized decoction during overall extraction times. The influences of pressure and extraction time on extraction yield, TSSC, pH, and the contents of chemical compounds were confirmed by regression analysis, which showed that all extraction values were significantly affected by at least one of two extraction factors, pressure and extraction time. Conclusions : This study suggests that the pressure and extraction time can significantly affect the extraction efficiency of components from GBH decoctions. However, optimal extraction conditions could not be chosen due to the variation of the amounts of chemical compounds.