• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.10a
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• pp.191-191
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• 2003

It is well-known that the mechanical behavior of fiber-reinforced composites under hydrostatic pressure environment is different from that of atmospheric pressure environment. It is also known that the mechanical behavior of fiber-reinforced composites is affected by strain rate. In this work, we investigated the effect of strain rate on the compressional elastic modulus and fracture stress of fiber-reinforced composites under hydrostatic pressure environment. The material used in the compressional test was unidirectional carbon/epoxy composites and the hydrostatic pressures applied was 250 MPa. Compressional tests were performed applying various strain rates of 0.05 %/sec, 0.25 %/sec, 0.45 %/sec, and 0.75 %/sec. The results showed that the elastic modulus increased with increasing strain rate while the fracture stress was little affected by the strain rate.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.06a
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• pp.593-597
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• 2005

It is generally accepted that fracture toughness of fiber-reinforced polymer composites is affected by loading rate in an atmospheric presure condition. For a present study, the loading rate effect on the fracture toughness of fiber-reinforced laminated composites in the hydrostatic pressure condition was investigated. For this purpose, fracture tests have been conducted using carbon/epoxy composites applying three steps of the strain rate at 270 MPa hydrostatic pressure condition. The loading rates applied were 0.05%/sec, 0.25%/sec, and 0.55%/sec. Fracture toughness was determined from the work factor approach as a function of applied loading rate. The result showed that fracture toughness decreased as the loading rate increased. Specifically, the fracture toughness decreased 12% as the loading rate increased from 0.05%/sec to 0.55%/sec.

• Journal of the Korean Society for Precision Engineering
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• v.21 no.4
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• pp.148-153
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• 2004

It is well-known that the mechanical behavior of fiber-reinforced composites under hydrostatic pressure environment is different from that of atmospheric pressure environment. It is also known that the mechanical behavior of fiber-reinforced composites is affected by a strain rate. In this work, we investigated the effect of strain rate on the compressive elastic modulus, fracture stress, and fracture strain of carbon/epoxy composites under hydrostatic pressure environment. The material used in the compressive test was unidirectional carbon/epoxy composites and the hydrostatic pressures applied was 270㎫. Compressive tests were performed applying three strain rates of 0.05％/sec, 0.25％/sec, and 0.55％/sec. The results showed that the elastic modulus increased with increasing strain rate while the fracture stress was little affected by the strain rate. The results also showed that the fracture strain decreased with increasing strain rate.

• Carbon letters
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• v.16 no.1
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• pp.34-40
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• 2015

In this study, in order to improve the thermal and electrical properties of epoxy/graphene nanoplatelets (GNPs), surface modifications of GNPs are conducted using silane coupling agents. Three silane coupling agents, i.e. 2-(3,4-epoxycyclohexyl)-ethyltrimethoxysilane (ETMOS), 3-glycidoxypropyltriethoxysilane (GPTS), and 3-glycidoxypropyltrimethoxysilane (GPTMS), were used. Among theses, GPTMS exhibits the best modification performance for fabricating GNP-incorporated epoxy composites. The effect of the silanization is evaluated using transmission electron microscopy (TEM), scanning electron microscopy, thermogravimetric analysis, and energy dispersive X-ray spectroscopy. The electrical and thermal conductivities are characterized. The epoxy/silanized GNPs exhibits higher thermal and electrical properties than the epoxy/raw GNPs due to the improved dispersion state of the GNPs in the epoxy matrix. The TEM microphotographs and Turbiscan data demonstrate that the silane molecules grafted onto the GNP surface improve the GNP dispersion in the epoxy.

• Proceedings of the KSR Conference
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• 2008.11b
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• pp.406-415
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• 2008

Recently, the amount of thermosetting plastic wastes have increased with the production of reinforced plastic composites and causes serious environmental problems. The epoxy composites, one of the versatile thermosetting plastics with excellent properties, cannot be melted down and remolded as what is done in the thermoplastic industry. In this research, a series of experiments that recovers carbon fibers from carbon fiber reinforced epoxy composites for train body was performed. We experimentally examined various decomposition processes and compared their decomposition efficiencies and mechanical property of recovered carbon fibers. For the prevention of tangle of recovered carbon fibers, each composites specimen was fixed with a Teflon supporter and no mechanical mixing was applied. Decomposition products were analyzed by scanning electron microscope (SEM), gas chromatography mass spectrometer (GC-MS), and universal testing machine (UTM). Carbon fibers could be completely recovered from decomposition process using nitric acid aqueous solution, liquid-phase thermal cracking and pyrolysis. The tensile strength losses of the recovered carbon fibers were less than 4%.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.11a
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• pp.31-34
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• 2005

For the damage tolerance improvement of conventional laminated composites, stitching process has been utilized for providing through-thickness reinforcements. 2D prefonl1S were stacked with S-2 glass plain weave, and 3D preforms were fabricated using the stitching process. For the matrix system, epoxy and phenol resins were considered. To examine the damage resistance performance the low velocity drop weight impact test has been carried out, and the impact damage was examined by scanning image. CAI (Compressive After Ih1paet) tests were also conducted to evaluate residual compressive strength. Compared with 2D epoxy composites, 2D phenol composites showed drastic reduction in the compressive strength prior to impact because of the higher contents of voids. The damage area of 2D phenol composites were also larger than that of 2D epoxy composites. However, by introducing the stitching, the damage area of 3D phenol composites was reduced by 60%, while the CAI strength improvement was negligible.

• Carbon letters
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• v.14 no.1
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• pp.1-13
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• 2013

Carbon nanotubes (CNTs) are increasingly attracting scientific and industrial interest because of their outstanding characteristics, such as a high Young's modulus and tensile strength, low density, and excellent electrical and thermal properties. The incorporation of CNTs into polymer matrices greatly improves the electrical, thermal, and mechanical properties of the materials. Surface modification of CNTs can improve their processibility and dispersion within the composites. This paper aims to review the surface modification of CNTs, processing technologies, and mechanical and electrical properties of CNT-based epoxy composites.

• Elastomers and Composites
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• v.43 no.2
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• pp.113-123
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• 2008

Epoxy resins are thermoset polymers that exhibit good adhesion, creep resistance, heat resistance, and chemical resistance. These polymers, however, give poor resistance to crack propagation and low impact strength. In this study, epoxy/carboxyl-terminated butadiene acrylonitrile (CTBN) and epoxy/amine-terminated butadiene acrylonitrile (ATBN) composites were prepared with different ratio of CTBN and ATBN to improve low impact strength of epoxy resin. The impact strength of epoxy/elastomeric composites shows high values with increasting nonpolar surface free energy while the tensile strength and the glass transition are decreased. The highest surface free energy, impact strength observed when 15 phr CTBN and 15 phr ATBN added, respectively. It can be concluded that as liquid rubber to improve impact strength of epoxy resin, ATBN is more preferable to CTBN.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.11a
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• pp.49-52
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• 2005

In the development of a propellant tank using liquid oxygen and liquid hydrogen, the improvement of microcrack resistance of carbon/epoxy composites is necessary for the application of a composite material to tank structures. In this research, two types of carbon/epoxy composites with different matrix systems were tested to measure interlaminar shear strength (ILSS), one of the material properties to evaluate fiber-matrix interface adhesion indirectly. Short beam specimens were tested inside an environmental chamber at room temperature(RT) and at cryogenic temperature( - 150 $^{\circ}C$) respectively. Results showed that the matrix system with large amount of bisphenol-A and CTBN modified rubber had good performance at cryogenic temperature.

• Journal of the Korean Society for Railway
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• v.8 no.2
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• pp.195-201
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• 2005

Mode II interlaminar fracture behaviors of carbon fabric/epoxy composites, which are applicable to tilting train carbodies, was investigated by the ENF (End notched flexure) test. The specimens were made of CF3327 plain woven fabric with epoxy and a starter delamination at one end was made by inserting Teflon film with the thickness of 12.5$mu$m or 25.0$mu$m. The equation for mode II interlaminar fracture toughness was suggested based on the effective crack length from the compliance of load-displacement curve. Mode II interlaminar fracture toughness was evaluated for several types of the specimens. Also crack propagating behaviors and fracture surfaces were examined through an optical travelling scope and a scanning electron microscope.