• Nuclear Engineering and Technology
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• v.25 no.4
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• pp.548-551
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• 1993

A simple and new uranium analysis technique for raffinate solution of nuclear fuel conversion process was developed using a time-resolved laser-induced fluorimetry. The addition of 4 M-phosphoric acid more than 10 times in volume to the raffinate sample was found to be efficient for obtaining stable uranium fluorescence signal which was not influenced by many fluorescence quenchers. A calibration curve of a good linearity for the fluorescence intensity vs. the uranium concentration was obtained at the range of 3.0$\times$10$^{-6}$－6.0$\times$10$^{-5}$ M U $O_2$$^{2＋}$ in the raffinate samples.

• Coupled systems mechanics
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• v.8 no.1
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• pp.1-17
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• 2019

The present paper deals with delamination fracture analyses of the multilayered functionally graded non-linear elastic Symmetric Split Beam (SSB) configurations. The material is functionally graded in both width and height directions in each layer. It is assumed that the material properties are distributed non-symmetrically with respect to the centroidal axes of the beam cross-section. Sine laws are used to describe the continuous variation of the material properties in the cross-sections of the layers. The delamination fracture is analyzed in terms of the strain energy release rate by considering the balance of the energy. A comparison with the J-integral is performed for verification. The solution derived is used for parametric analyses of the delamination fracture behavior of the multilayered functionally graded SSB in order to evaluate the effects of the sine gradients of the three material properties in the width and height directions of the layers and the location of the crack along the beam width on the strain energy release rate. The solution obtained is valid for two-dimensional functionally graded non-linear elastic SSB configurations which are made of an arbitrary number of lengthwise vertical layers. A delamination crack is located arbitrary between layers. Thus, the two crack arms have different widths. Besides, the layers have individual widths and material properties.

• Journal of Sensor Science and Technology
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• v.32 no.6
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• pp.470-474
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• 2023

In this study, a diaphragm-type pressure sensor was developed using multi-layer(four-layer) graphene produced at 1 nm thickness by thermally transferring single-layer graphene produced by chemical vapor deposition (CVD) to a 6" silicon wafer. By measuring the gauge factor, we investigated whether it was possible to produce a pressure sensor of consistent quality. As a result of the measurement, the pressure sensor using multilayer graphene showed linearity and had a gauge factor of about 17.5. The gauge factor of the multilayer graphene-based pressure sensor produced through this study is lower than that of doped silicon, but is more sensitive than a general metal sensor, showing that it can be sufficiently used as a commercialized sensor.

• Atmosphere
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• v.20 no.4
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• pp.399-414
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• 2010

Sand and dust storm in East Asia, so called Asian dust, is a seasonal meteorological phenomenon. Mostly in spring, dust particles blown into atmosphere in the arid area over northern China desert and Manchuria are transported to East Asia by prevailing flows. An Asian dust event occurred on 6-8 May 2007 is chosen to investigate how sensitive the Asian dust transport forecast to the initial condition uncertainties and to interpret the characteristics of sensitivity structures from the viewpoint of dynamics and predictability. To investigate the forecast sensitivities to the initial condition, adjoint sensitivities that calculate gradient of the forecast aspect (i.e., response function) with respect to the initial condition are used. The forecast aspects relevant to Asian dust transports are dry energy forecast error and lower tropospheric pressure forecast error. The results show that the sensitive regions for the dry energy forecast error and the lower tropospheric pressure forecast error are initially located in the vicinity of the trough and then propagate eastward as the surface low system moves eastward. The vertical structures of the adjoint sensitivities for the dry energy forecast error are upshear tilted structures, which are typical adjoint sensitivity structures for extratropical cyclones. Energy distribution of singular vectors also show very similar structures with the adjoint sensitivities for the dry energy forecast error. The adjoint sensitivities of the lower tropospheric pressure forecast error with respect to the relative vorticity show that the accurate forecast of the trough (or relative vorticity) location and intensity is essential to have better forecasts of the Asian dust event. Forecast error for the atmospheric circulation during the dust event is reduced 62.8% by extracting properly weighted adjoint sensitivity perturbations from the initial state. Linearity assumption holds generally well for this case. Dynamics of the Asian dust transport is closely associated with predictability of it, and the improvement in the overall forecast by the adjoint sensitivity perturbations implies that adjoint sensitivities would be beneficial in improving the forecast of Asian dust events.

• Journal of the Korean Society of Radiology
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• v.16 no.6
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• pp.771-778
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• 2022

The purpose of this study is to present a method of measuring noise by the percentage of effective line attenuation coefficient of water that can be used for quality control of CT image noise using AAPM CT performance phantom in clinical practice. In the CT images obtained by scanning the AAPM CT performance phantom with a 120 kVp CT X-ray beam, the mean CT number was measured for each pin and water in the CT number linearity insert part. The effective energy was determined as the photon energy with the largest correlation coefficient from the correlation coefficients of the linear regression analysis of the measured mean CT number for each pin and water and the linear attenuation coefficient for each photon energy. And for water and acrylic, the contrast scale was calculated as 0.000188 cm^-1 · HU^-1 from the measured mean CT number and effective line attenuation coefficient. Using the calculated contrast scale, the effective line attenuation coefficient of water, and the standard deviation measured in the water of the alignment pin part of the AAPM CT performance phantom, The noise measurement value by the percentage of effective line attenuation coefficient of water obtained 0.31 ~ 0.52% in the range of 100 ~ 300 mAs.

• Analytical Science and Technology
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• v.12 no.2
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• pp.99-104
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• 1999

A stepwise gradient elution with two wavelengths detection was performed for the separation and determination of some anions in saline water. The eight anions such as iodate, bromate, nitrite, bromide, nitrate, chromate, iodide and thiocyanate were successfully separated using AS-7 column and sodium chloride/sodium phosphate buffer solution as an eluant within 40 min. The separation behaviors of anions were studied at various sodium chloride concentrations. The peak shapes of anions of bromate, nitrite, bromide and nitrate gradually broadened as the concentration of sodium chloride increased until 1.0 M in the sample solutions. However, no effect was observed in the peak shapes of chromate, iodide and thiocynate. A good linearity was obtained at the range of ppm(mg/L). The detection limit was proved to be $10-720{\mu}g/L$ for the eight anions with $50{\mu}L$ injection volume. This method was applied to the determination of $Br^-$, ${NO_3}^-$ and $I^-$ in sea water.

• Transactions of the Korean hydrogen and new energy society
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• v.16 no.2
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• pp.136-141
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• 2005

Li-doped NiO was synthesized by molten salt method. $LiNO_3$-LiOH flux was used as a source for Li doping. $NiCl_2$ was added to the molten Li flux and then processed to make the Li-doped NiO material. Li:Ni ratios were maintained from 5:1 to 30:1 during the synthetic procedure and the Li doping amount of synthesized materials were found between 0.086-0.190 as a Li ion to Ni ion ratio. Li doping did not change the basic cubic structural characteristics of NiO as evidenced by XRD studies, however the lattice parameter decreased from 0.41769nm in pure NiO to 0.41271nm as Li doping amount increased. Hydrogen gas sensors were fabricated using these materials as thick films on alumina substrates. The half surface of each sensor was coated with the Pt catalyst. The sensor when exposed to the hydrogen gas blended in air, heated up the catalytic surface leaving rest half surface (without catalyst) cold. The thermoelectric voltage thus built up along the hot and cold surface of the Li-doped NiO made the basis for detecting hydrogen gas. The linearity of the voltage signal vs $H_2$ concentration was checked up to 4% of $H_2$ in air (as higher concentrations above 4.65% are explosive in air) using Li doped NiO of Li ion/Ni ion=0.111 as the sensor material. The response time T90 and the recovery time RT90 were less than 25 sec. There was minimum interference of other gases and hence $H_2$ gas can easily be detected.

• Journal of Radiation Protection and Research
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• v.27 no.1
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• pp.51-57
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• 2002

An electronic personal dosimeter(EPD) with hybrid type preamplifier adopting a semiconductor detector as a radiation detector has been developed, manufactured and test-evaluated. The radiation detection characteristics of this EPD has been performance-tested by using a reference photon radiation field. After several test-irradiations to a $^{137}Cs$ gamma radiation source the radiation detection sensitivity of this EPD appeared to be $3.8\;cps/Gy{\cdot}h^{-1}$. The linearity of radiation response was kept within 8% of the dose equivalent ranges of $10{\mu}Sv{\sim}4Sv$ and the angular dependence was under less than 4% in angles of ${\pm}60^{\circ}$. It was confirmed that the energy response range was in $60{\sim}1,250keV$ given in the ISO standard. This EPD satisfied the international criteria for the EPD in the mechanical and the environmental performance test for 9 test categories according to IEC 61526.

• Korean Journal of Pharmacognosy
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• v.47 no.1
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• pp.79-83
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• 2016

This study developed an HPLC analysis method for the determination of isoegomaketone (IK) and perillaketone (PK) in Perilla frutescens (L.) Britton leaves. P. frutescens ethanol extract was optimized through an HPLC analysis using a C18 column ($250{\times}4.6mml$, D, $S-5{\mu}m$, 12 nm) with gradient elution of water and acetonitrile as the mobile phase at a flow rate of 1 mL/min and a UV detection wavelength of 254 nm. The results of this method showed linearity in the calibration curve at a coefficient of correlation ($R^2$) of IK 0.9995, PK 0.9998. The limits of detection (LOD) for IK and PK were $0.234{\mu}g/mL$ and $0.952{\mu}g/mL$. The limits of quantification (LOQ) for IK and PK were $0.017{\mu}g/mL$ and $0.043{\mu}g/mL$. The inter-day precision RSDs of IK and PK in the P. frutescens were 1.25 to 2.69% and 0.36 to 1.10%, respectively, and the intra-day precision RSDs of IK and PK were 0.96 to 2.51% and 0.90 to 1.93%, respectively. The accuracies of IK and PK were 96.31 to 97.92% and 101.26 to 105.14%. In conclusion, this method was applied successfully to the detection of IK and PK in P. frutescens.

• Analytical Science and Technology
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• v.23 no.6
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• pp.518-523
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• 2010

In this paper, the study of analysis of uranium isotopes in environmental samples with a kinetic phosphorescence analyzer (KPA) was described. After leaching uranium fraction from soil and glass material with microwave acid digestion technology, uranium isotopes were purified with UTEVA column, and then measured using KPA. Linearity and repeatability tests for measurement of uranium isotopes were carried out in the uranium standard solution with KPA. The reliability for analytical method of uranium with KPA was validated by its application to uranium standard solution, ground water, IAEA and NIST reference samples.