• Journal of the Korean Chemical Society
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• v.35 no.5
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• pp.520-526
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• 1991

Retention behavior of lanthanides was studied on the dynamic system using dinonylnaphthalene sulfonic acid cation exchanger and tartaric acid as a complexing agent. The relations between logk' and log$[NH^{4+}]$/log[tartarate], and between logk' and logR showed good linearity in isocratic and gradient elution, respectively. In gradient elution of tartaric acid the slopes were increased as the initial concentrations were decreased. Column efficiencies and resolution of lanthanides on dinonylnaphthalene sulfonic acid equilibrated cation exchanger were found to be better in ${\alpha}$-hydroxyisobutyric acid eluent than in tartaric acid.

• Journal of Radiation Protection and Research
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• v.34 no.2
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• pp.77-81
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• 2009

An Area Radiation Monitoring System (ARMS) ionization chamber, which had an 11.8 L active volume, was fabricated and performance-tested at KAERI. Low leakage currents, linearities at low and high dose rates were achieved from performance tests. The correlation coefficients between the ionization currents and the dose rates are 1 at high dose rate and 0.99 at low dose rate. In this study, an integration-type ARMS ionization chamber was tested over a year for an evaluation of its long-term stability at a radioisotope (RI) repository of the Young-gwang nuclear power plant. The standard deviation of dose rate of 1 day data and over a 100-days mean value were 6.2 $\mu$R/h and 2.9 $\mu$R/h, respectively. The fabricated ARMS ionization chamber showed stable performance from the results of the long-term tests. Design and performance characteristics of the fabricated ionization chamber for the ARMS from performance-tests are also addressed.

• Journal of Radiation Protection and Research
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• v.31 no.3
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• pp.149-153
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• 2006

An ionization chamber is still widely used in many fields by virtue of its' simple operational characteristics and the possibility of its' various shapes. A parallel type of an ionization chamber for a steel sheet thickness measurement was designed and fabricated. High pure xenon gas, which was pressurized up to 6 atm, was chosen as a filling gas to increase the current response and sensitivity for a radiation. A high pressure gas system was also constructed. The active volume and the incident window size of the fabricated ionization chamber were $30\;cm^3\;and\;12\;cm^2$, respectively. Preliminary tests with a 25 mCi $^{241}Am$ gamma-ray source and evaluation tests in a standard X-ray field were performed. The optimal operation voltage was set from the results of the collection efficiency calculation by using an experimental two-voltage method. Linearity for a variation of the steel sheet thickness, which is the most important factor for an application during a steel sheet thickness measurement, was 0.989 in this study.

• Journal of Electrical Engineering and Technology
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• v.8 no.6
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• pp.1320-1327
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• 2013

In this paper, two different electromagnetic energy harvesters using bulk micromachined silicon spiral springs and Polydimethylsiloxane (PDMS) packaging technique have been fabricated, characterized, and compared to generate electrical energy from ultra-low ambient vibrations under 0.3g. The proposed energy harvesters were comprised of a highly miniaturized Neodymium Iron Boron (NdFeB) magnet, silicon spiral spring, multi-turned copper coil, and PDMS housing in order to improve the electrical output powers and reduce their sizes/volumes. When an external vibration moves directly the magnet mounted as a seismic mass at the center of the spiral spring, the mechanical energy of the moving mass is transformed to electrical energy through the 183 turns of solenoid copper coils. The silicon spiral springs were applied to generate high electrical output power by maximizing the deflection of the movable mass at the low level vibrations. The fabricated energy harvesters using these two different spiral springs exhibited the resonant frequencies of 36Hz and 63Hz and the optimal load resistances of $99{\Omega}$ and $55{\Omega}$, respectively. In particular, the energy harvester using the spiral spring with two links exhibited much better linearity characteristics than the one with four links. It generated $29.02{\mu}W$ of output power and 107.3mV of load voltage at the vibration acceleration of 0.3g. It also exhibited power density and normalized power density of $48.37{\mu}W{\cdot}cm-3$ and $537.41{\mu}W{\cdot}cm-3{\cdot}g-2$, respectively. The total volume of the fabricated energy harvesters was $1cm{\times}1cm{\times}0.6cm$ (height).

• Journal of Mechanical Science and Technology
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• v.16 no.11
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• pp.1420-1427
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• 2002

The Monkman-Grant (M-G) and its modified parameters were evaluated for type 316LN and modified 9Cr-Mo stainless steels prepared with minor element variations. Several sets of creep data for the two alloy systems were obtained by constant-load creep tests in 550～650$\^{C}$ temperature range. The M-G parameters, m, m', C, and C' were proposed and discussed for the two alloy systems. The m value of the M-C relation was 0.90 in type 316LN steel and 0.84 in modified 9Cr-Mo steel. The m' value of the modified relation was 0.94 in type 316LN steel and 0.89 in 9Cr-Mo steel. Although creep fracture modes and creep properties between type 316LN and modified 9Cr-Mo steels showed a basic difference, the M-G and its modified relations demonstrated linearity quite well. The m' of modified relation almost overlapped regardless of the creep testing conditions and chemical variations in the two alloy systems, and the parameter m' was closer to unity than that of the M-G relation.

• Journal of Sensor Science and Technology
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• v.29 no.5
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• pp.283-292
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• 2020

Current sensors that use a Hall element and Hall IC to measure the magnetic fields generated in steel silicon core gaps do not distinguish between direct and alternating currents. Thus, they are primarily used to measure direct current (DC) in industrial equipment. Although such sensors can measure the DC when installed in expensive equipment, ascertaining problems becomes difficult if the equipment is set up in an unexposed space. The control box is only opened during scheduled maintenance or when anomalies occur. Therefore, in this paper, a method is proposed for facilitating the safety management and maintenance of equipment when necessary, instead of waiting for anomalies or scheduled maintenance. A Bluetooth 4.0 low-energy current-sensor system based on near-field communication is used, which compensates for the nonlinearity of the current-sensor output signal using a piecewise linear model. The sensor is controlled using its generic attribute profile. Sensor nodes and cell phones used to check the signals obtained from the sensor at 50-A input currents showed an accuracy of ±1%, exhibiting linearity in all communications within the range of 0 to 50 A, with a stable output voltage for each communication segment.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.16 no.1
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• pp.49-55
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• 2020

Creep rupture data for Alloy 690 steam generator tubes in a pressurized water reactor are essentially needed to demonstrate a severe accident scenario on thermally-induced tube failures caused by hot gases in a damaged reactor core. The rupture data were obtained using the tube specimens under different applied-stress levels at 650℃, 700℃, 750℃, 800℃, and 850℃. Important creep constants were proposed using various creep laws in terms of Norton power law, Monkman-Grant (M-G) relation, damage tolerance factor (λ), and Zener-Hollomon parameter (Z). In addition, a creep activation energy (Q) value for Alloy 690 tube was reasonably determined using experimental data. Creep behaviors such as creep strength, creep rates, rupture elongation showed the results of temperature dependence well. Modified M-G plot improved a correlation of the creep rate and rupture life. Damage tolerance factor for Alloy 690 tubes was found to be λ =2.20 in an average value. Creep activation energy for Alloy 690 tube was optimized for Q=350 (kJ/mol). A plot of Z parameter obeyed a good linearity, and the same creep mechanism was inferred to be operative in the present test conditions.

• Bulletin of the Korean Chemical Society
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• v.34 no.3
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• pp.801-809
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• 2013

We investigate sensitivity and limit of detection (LOD) of trace copper (Cu) metal using pristine carbon nanotube (CNT) and acidified CNT (ACNT) electrodes. Squarewave based anodic stripping voltammetry (SWASV) is used to determine the stripped Cu concentration. Prior to performing the SWASV measurements, its optimal conditions are determined and with that, effects of potential scan rate and $Cu^{2+}$ concentration on stripping current are evaluated. The measurements indicate that (1) ACNT electrode shows better results than CNT electrode and (2) stripping is controlled by surface reaction. In the given $Cu^{2+}$ concentration range of 25-150 ppb, peak stripping current has linearity with $Cu^{2+}$ concentration. Quantitatively, sensitivity and LOD of Cu in ACNT electrode are 9.36 ${\mu}A\;{\mu}M^{-1}$ and 3 ppb, while their values are 3.99 ${\mu}A\;{\mu}M^{-1}$ and 3 ppb with CNT electrode. We evaluate the effect of three different water solutions (deionized water, tap water and river water) on stripping current and the confirm types of water don't affect the sensitivity of Cu. It turns out by optical inspection and cyclic voltammetry that superiority of ACNT electrode to CNT electrode is attributed to exfoliation of CNT bundles and improved interfacial adhesion occurring during oxidation of CNTs.

• Journal of Radiation Protection and Research
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• v.37 no.2
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• pp.70-74
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• 2012

Silicon carbide (SiC) is a promising material for neutron detection at harsh environments because of its capability to withstand strong radiation fields and high temperatures. Two PIN-type SiC semiconductor neutron detectors, which can be used for nuclear power plant (NPP) applications, such as in-core reactor neutron flux monitoring and measurement, were designed and fabricated. As a preliminary test, MCNPX simulations were performed to estimate reaction probabilities with respect to neutron energies. In the experiment, I-V curves were measured to confirm the diode characteristic of the detectors, and pulse height spectra were measured for neutron responses by using a $^{252}Cf$ neutron source at KRISS (Korea Research Institute of Standards and Science), and a Tandem accelerator at KIGAM (Korea Institute of Geoscience and Mineral Resources). The neutron counts of the detector were linearly increased as the incident neutron flux got larger.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.66 no.12
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• pp.1804-1809
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• 2017

A data acquisition (DAQ) system based on oscilloscope was developed and evaluated for radiation detector. The dedicated LabVIEW program that perform the oscilloscope control and the data process was developed. Triggered events for each analog channel were acquired and the output signals were subsequently digitized and recorded for offline processing. Radiation pulse generation circuit was developed to evaluate the intrinsic characteristics of DAQ system. Energy linearity and energy resolution performances were assessed by voltage-peak channels and FWHM obtained from Gaussian fit, respectively. Radiation detector consists of LYSO and GAPD array. The 16 output signals were multiplexed by the RCD networks, and they were fed into the custom-made preamplifiers. Voltage-peak channels was linearly changed as a function of input voltage and the estimated coefficient of determination ($R^2$) was 0.999. No considerable changes in voltage resolution were observed. All 16 crystals were clearly identifiable on the resulting flood image and the mean energy resolution was ~15.1%. This study demonstrated that it is feasible to develop the DAQ system based on oscilloscope and LabVIEW program for radiation detector and the proposed approach offers opportunities to build simple DAQ system in various radiation measurement field.