• Journal of the Korean Society of Tobacco Science
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• v.15 no.2
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• pp.174-184
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• 1993

This is to investigate the methodology for the simultaneous determination of Wk, mk and TSNA using gas chromatography(GC) in combination with chemiluminescence detector, thermal energy analyzer(TEA) . The simultaneous analysis has been estimated by evaluating tobacco. The TEA was linked to GC equipped with non -polar SPB -5 fused silica capillary column which was introduced into the ceramic pyrolysis tube by the point of 16cm from the end of TEA. Quantification was carried out by internal standardization with WDPA after calibration of retention times and response factors with authentic nitrosoamines. It was demonstrated that WDPA was most preferable as internal standard for the simultaneous analysis. The recoveries of the internal standard were in the range of 83∼96% . Nitrosoamines in this method were detected with determination limit of 0.1ng and was made by a straight line in calibration curve by TEA response. The suitability of nitrosoamines extraction in tobacco leaf was investigated. It was most suitable to extract nitrosoamines from tobacco leaves with 0.01 M NaOH within a period of 8 hours. Thimerosal as an antibacterial agent was added to NaOH solution to prevent artifactual formation. The fractionation and the purification of nitrosoamines form alkaline extracts were conveniently performed using Extrelut multilayer column and dichloromethane. Reproducible and reliable results were obtained for the determination of nitrosamines in a relatively short time compared to previous known method. TSNA contents in burley were about 4 times higher as those in the fluecured tobacco.

• Journal of Radiation Protection and Research
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• v.15 no.2
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• pp.87-100
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• 1990

For the quantitative evaluation and assessment of radiation exposure from terrestrial component of natural environmental radiation, successive thermoluminescence dosimetry and periodical in-situ gamma ray spectrometry were carried out for a period of 24 months. LiF PTFE dise TLDs and $3&{\phi}{\times}3'$cylindrical NaI(Tl)scintill ation detector in association of portable multichannel analyzer (4096 ch) were used in this study. The doses measured were evaluated and assessed in terms of effective dose equivalent. As a concomitant output, the dose equivalent due to ionizing component of cosmic ray was able to be evaluated. According to the results obtained in terms of variance weighted mean, the annual effective dose equivalents of terrestrial gamma ray and cosmic ray ionizing component in Taejeon area came out to be $564{\pm}4\;{\mu}Sv(64.8{\pm}0.5nSv{\cdot}h^{-1}$ and $300{\pm}2\;{\mu}Sv(34.3{\pm}0.2nSv{\cdot}h^{-1}$, respectively, which are reasonable comparably with that appeared in UNSCEAR Report[28]as per caput annual effective dose equivalent in 'areas of normal background radiation'.

• Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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• 2015.10a
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• pp.1103-1105
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• 2015

Leaked Radioactive source in nuclear power station, radiation related facilities and the aging nuclear power plant for the dismantling must need to detect and remove early to prevent major accidents. In this paper, we implemented a single sensor-based gamma-ray detectors stereo which can provide the distance to the radiation source, a direction and doserate information for fast and efficient decontamination work the radiation source. And we have carried out an algorithm development for high-speed detection of the detection equipment. Two detectors are required for stereo structure for obtaining the distance information of the radioactive source, but we designed the only sensor-based detection device for the weight reduction. We have extracted the region of interest and obtained the distance calculation result and distribution of radiation source in order to minimize a stereo image acquisition time. Detection time of the algorithm showed a shorter time of about 41%.

• Nuclear Engineering and Technology
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• v.5 no.4
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• pp.291-309
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• 1973

Exposure rates due to leakage gamma-rays from operating reactors TRIGA Mark II and III were measured in a horizontal plane by means of scintillation spectrometry using a 3"$\times$3" cylindrical Nal(T1) detector associated with a 400 channel pulse height analyzer under varied conditions of reactor operation. In determining exposure rate due to the leakage gamma-rays at each point of measurement, Moriuchi's spectrum-exposure rate conversion theory was applied instead of using conventional responce matrix method which necessitates very complicated procedures to convert a spectrum into exposure rate. The results show that a basic pattern of "typical" spectrum of the reactor leakage gamma-rays is neither affected by thermal output of the reactor, nor influenced by overall attenuation in radiation intensity. It was indicated that he attenuation of the leakage gamma-rays in air in terms of exposure rate as a whole follows an exponential law, and the total exposure rate due to the leakage gamma-rays at a certain point is nearly proportional to thermal output of the reactor. The complexity in spectrum measured for a movable core reactor, TRIGA Mark III, was analyzed through spectrum resolution, and proper judgement of the leakage gamma-rays in a complex spectrum was discussed.ctrum was discussed.

• Journal of Korean Society for Atmospheric Environment
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• v.27 no.4
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• pp.454-459
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• 2011

In this study, the recovery rate of Tedlar bag (T) sampler was investigated in comparison to polyester aluminum bag (P) sampler. To derive the comparative data sets for the relative performance between different samplers, a series of calibration experiments were performed by using 1 ppb standard of four offensive reduced sulfur compounds (RSC) odorants ($H_2S$, $CH_3SH$, DMS, and DMDS) along with $SO_2$ and $CS_2$. All the analysis was made by gas chromatography/pulsed flame photometric detector (GC/PFPD) combined with air server/thermal desorber (AS/TD). The measurement data were obtained by loading gaseous standards (1 ppb) at 3 injection volumes (250, 500 and 1,000 mL) at three intervals (0, 24 and 72 hrs). The recovery rates (RR) of P sampler were computed against the slope values of T sampler. According to our analysis, P sampler exhibits slightly enhanced loss relative to T, especially with light RSCs ($H_2S$ and $CH_3SH$). At day 0, RR for the two were 88 and 85%, respectively. Such reduction proceeded rather rapidly in the case of $H_2S$ through time. However, P sampler was more stable to store $SO_2$ unlike others. Despite slightly reduced recovery, P sampler appears as a good replacement of T sampler.

• Journal of the Korean Society for Marine Environment & Energy
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• v.5 no.1
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• pp.38-50
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• 2002

To study the distribution of organophosphorus pesticides which are extensively used for agriculture in Korea. Surface sea water samples were taken from 2 coastal areas during July and :;eptember of 1999 and sediment samples were collected from Kyeonggi bay in July of 1999. These samples were analyzed using a Gas Chromatography/Nitrogen Phosphorus Detector(GC/NPD). In coastal waters of the study areas IBP was commonly found the most compound. Traces of Diazinon, DDVP, Ethoprouhos and Chlorpyrifos were also encountered. Concentration of the other major organophosphorus pesticides(Disulfoton, Parathion Methyl, Fenchlorfos, Prothiofos, EDDP) were generally be below the detection limit of the employed analytical method. Tn sediment of the study areas Chlorpyrifos w3s found the most compound. Temporal and geographical distribution of individual organophosphorus pesticides is likely to be affected by types of agricultural practices in the watershed.

• Journal of the Korea Institute of Military Science and Technology
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• v.17 no.1
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• pp.90-95
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• 2014

The system design and the system performance analysis of 3D imaging laser radar system for the mapping purpose is addressed in this article. For the mapping, a push-bloom scanning method is utilized. The pulsed fiber laser with high pulse energy and high pulse repetition rate is used for the light source of laser radar system. The high sensitive linear mode InGaAs avalanche photo-diode is used for the laser receiver module. The time-of-flight of laser pulse from the laser to the receiver is calculated by using high speed FPGA based signal processing board. To reduce the walk error of laser pulse regardless of the intensity differences between pulses, the time of flight is measured from peak to peak of laser pulses. To get 3D image with a single pixel detector, Risley scanner which stirs the laser beam in an ellipsoidal pattern is used. The system laser energy budget characteristics is modeled using LADAR equation, from which the system performances such as the pulse detection probability, false alarm and etc. are analyzed and predicted. The test results of the system performances are acquired and compared with the predicted system performance. According to test results, all the system requirements are satisfied. The 3D image which was acquired by using the laser radar system is also presented in this article.

• Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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• 2017.10a
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• pp.705-707
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• 2017

Stereo-based spatial radiation detection devices can obtain not only spatial distribution information about the radiation source but also distance information from the detection device to the source. And it provides more efficient information on the source than the existing radiation imaging device. In order to provide high-speed information on the spectrum and type of gamma-ray source, a high-sensitivity detection sensor with high sensitivity is required, and a technique capable of solving the saturation phenomenon at a high dose is needed. In this paper, we constructed a high sensitivity sensor for the measurement of multiple gamma - ray spatial distributions using improved function of detection module to solve saturation to high dose and conducted research to increase the scope of a single detector. The result of this paper improves the performance of gamma ray.

• Journal of the Institute of Electronics and Information Engineers
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• v.52 no.4
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• pp.197-203
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• 2015

Nuclear power plant has increased continuously for power production in all over the world and the interest about nuclear accident and the dismantling of aging nuclear power plant has been a growing. The leaked radioactive source that is generated by radiation accidents must detect and remove to minimized the damage as soon as possible. Gamma-ray detection system that have been developed until now cannot provide the precise position of radioactive sources because they detect and imaging the position of radiation sources in just two dimensions. In this paper, stereo gamma ray detection system has developed and the algorithm for calculation of the distance has implemented to be able to measure the distribution of the leakage gamma ray source for the system. Stereo camera calibration for distance detection was conducted with the correction pattern and LED light and we carried out performance test of the system for the LED light source and a gamma ray source. In both experiments the results of the performance test, it was confirmed to have a 5% error. The results of this paper is used as a material for the development of gamma-ray imaging device.

• Journal of the Korean Institute of Gas
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• v.25 no.5
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• pp.57-62
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• 2021

Gas is an energy source widely used in general households and industrial sites, and is also a process material widely used in petrochemical and semiconductor processes. However, while it is easy to use, it can cause large-scale human damage due to leakage, explosion, and human inhalation. Therefore, a gas facility safety management solution that can be safely used at home and industrial sites is essential. In particular, the need to develop advanced gas safety solutions is emerging as gas facilities are aging. In this paper, a technology was developed to measure the presence and concentration of gas leaks from a distance by irradiating photons, the minimum energy unit that can no longer be divided into gas facilities, and analyzing the number of reflected photons. This overcomes technical limitations such as short detection distance and inability to detect fine leaks, which are the limitations of conventional electric/chemical gas sensors or infrared-based gas leak detectors.