• Title/Summary/Keyword: Elimination of epoxy

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Study on the Chemically Method of Epoxy Restoration Material in Antic Ceramics and Stabilization of Their Materials (토기.도자기 복원에 사용된 에폭시 복원재료의 화학적 제거방법과 그 안정성에 관한 연구)

  • Han, Won-Sik;Bae, Jin-Soo;Park, Gi-Jung;Hong, Tae-Kee;Wi, Koang-Chul
    • Journal of Conservation Science
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    • v.26 no.1
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    • pp.25-32
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    • 2010
  • The yellowing is always occurred phenomena in epoxy restoration material of antic-ceramics. For re-restoration of remains with epoxy restoration material, the epoxy elimination step is the first one in all course of restoration In this paper, the chemically elimination treatments methods of epoxy in various antic-ceramics were discussed. We fabricated the epoxy elimination material for antic-ceramics restoration which were made up Dichloromethane and Dichlormethane based Dimethylformamide solution. Dichloromethane and Dichloromethane + Dimethylformamide mixture were applied to epoxy in various antic-ceramic sample. Particularly, Dichloromethane + Dimethylformamide solution had the best result in variation of color change, gloss, vending strength, weight, exfoliation time test after deposition in this solution. Dichloromrthane had the volume increase characteristics for epoxy material and Dimethylformamide had the mollification ones. So, Dichloromathane increased exfoliation in approximal surface of the epoxy material and antic ceramic, and Dimethylformamide decreased the surface hardness of epoxy. In this result, epoxy material even inside of ceramic that have very weak inside bonding is adaptable and stable eliminated. And in order to show the perfect elimination of this material, we successfully dissolve the epoxy restoration material in one antic pottery that is in one university museum's possession using this mixture. So, there is guarantee in the eternity and stabilization of restoration for antic-ceramics.

Repair and Strengthening of R/C Structure Using Glass Fiber Reinforced Plastic Thin Panels (유리섬유보강 박판패널에 의한 철근콘크리트 구조물의 보수.보강공법)

  • 천의균;진형장;박석암;김행준
    • Proceedings of the Korea Concrete Institute Conference
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    • 2000.04a
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    • pp.866-873
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    • 2000
  • Reinforced concrete structure can be strengthened by glass fiber reinforced plastic thin panels. The GFRP-Thin Panels are manufactured by pressing form and their application technique are similar to steel plates. The use of FGRP-Thin Panels presents several advantages. The advantages of this structural system are the case of application, the elimination of joint and corrosion at the epoxy-panel interface. This paper introduces the method of manufacturing about GFRP-Thin Panels, mechanical properties and the application of reinforced concrete structures.

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Synthesis and in vitro Cytotoxicity Monoterpenoid as New Antitumor Agents (Monoterpenoid계의 새로운 항암제 합성 및 In vitro 세포독성 평가)

  • 이민정;김대근;백형근;이강노;정규혁
    • Biomolecules & Therapeutics
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    • v.9 no.3
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    • pp.143-155
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    • 2001
  • Many attention has been focused on developing new chemotherapeutic agents for a treatment of cancer from natural products. From Carpesium divaricatum S. et Z. (Compositae), various monoterpenoid compounds were isolated and exhibited mild antitumor activity against human tumor cell lines. These facts prompted us to explore the structure-activity relationship of these compounds. The synthesis of monoterpenoid compound was accomplished by Fries rearrangement, Grignard reaction, elimination, allylic oxidation, esterification and epoxidation as key steps. The results of in vitro cytotoxicity (A549, SK-OV-3, SK-MEL-2, XF498, HCT15) of the synthesised compounds are as follows: First of all, epoxide moiety is prerequisite for cytotoxic activity in diester compound. Any kind of compounds with olefin or diol moiety instead of epoxide ring exhibited poor or mild cytotoxic activity respectively. Of o-acetoxy and isobutoxy epoxy esters, p-sub-stituted phenylacetate compounds exhibited high cytotoxic activities against SK-MEL-2 and HCT15.

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Photoelastic Determination of Stress Intensity Factors by Teflon Molding Method - Evaluation of The Method In Terms of Two Dimensional Mode I and Mode II - (테프론 모울딩법 에 의한 S .I .F.의 광탄성 실험해석 - 이차원 S .I .F. 문제에 대한 실험방법 의 정도평가 -)

  • 최선호;황재석;채영석
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.7 no.1
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    • pp.1-10
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    • 1983
  • The photoelastic determination of S.I.F. in Fracture mechanics has been regarded as one of the most effective and practical experimental methods in which stresses are read directly, except a few shortcomings involved in the process of experiment; the difficulties of making a sharp crack tip similar to the practical one and nearly impossibilities of carving an arbitrarily shaped crack on the test plate, etc. To eliminate flaws mentioned above, recently, Kitagawa and Watanabe of Tokyo Univ.developed a new method named"Teflon Insert Method". which has improved experimental accuracy to a considerable extent byt remaining still room for further improvement, that is, the elimination of bonding boundary scars which render photoelastic fringes obscure. In this paper, a newly exploited"Teflon Molding Method" was attempted for the completion of teflon-epoxy experimental method. The experimental results obtained by this method are compared with existent theoretical and experimental values to evaluate its accuracy. As result, 1-6% of margin of errors were appeared in a series of photoelastic experiments which defied any other conventional method in terms of experimental accuracy.perimental accuracy.

Study on Recycling of Scraps from Process of Silicon-single-crystal for Semiconductor

  • Lee, Sang-Hoon;Lee, Kwan-Hee;Hiroshi Okamoto
    • Proceedings of the IEEK Conference
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    • 2001.10a
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    • pp.705-710
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    • 2001
  • So for the quartz-glassy crucible wastes which was used for pulling up silicon-single-crystal ingot have simply reused for refractory raw-materials, or exhausted. This study is concerned on the advanced recycling-technology that is obtained by the proper micro-particle preparation process in order to fabricate fine amorphous silica filler for EMC (Epoxy Molding Compound). Therefore, this paper will deal with the physical, chemical and thermal pre-treatment process for efficient impurity removal and with the proper micro-particle process for producing the amorphous silicafiller. In view of the results, if the chemical, physical and thermal pre-treatment process for efficient elimination of impurity was passed, the purity of wasted fused glassy crucible is almost equal to the its of first anhydrous quartz glass. Thus, it was understood that this wasted fused glassy crucible was sufficient value of recycling, though it was damaged. When the ingot was fabricated, Phase transformation of crystallization by heat treatment (heat hysteresis phenomenon) was not changed. So, it was understood that as fused silica in the amorphous state, as It is, recycling possibility was very high

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