• Title/Summary/Keyword: Electron detector

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Determination of 3-Monochloro-1, 2-propanediol in Acid Hydrolyzed Soysauce(Ganjang) by Gas-Chromatography with Electron Capture Detector (Gas Chromatography-Electron Capture Detector를 이용한 산분해간장중의 3-Monochloro-1, 2-propanediol 분석법에 관한 연구)

  • 최종동;문귀임;오현숙;김동술
    • Journal of Food Hygiene and Safety
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    • v.16 no.1
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    • pp.61-65
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    • 2001
  • To investigate the optimum condition of 3-monochloro-1, 2-propanediol(MCPD) analysis, gas chromatography with electron capture detector was used. Determination of MCPD derivatized with phenylboric acid was more effective than that of underivatized MCPD. In derivatization of MCPD with phenyl boric acid, there were no significantly different between boiling for 2min at 9$0^{\circ}C$ and vortexing for 5min at room temperature. Extrelut column was suitable for extraction of MCPD diluted in 20% NaCl solution and recovery rates were higher than direct extraction of MCPD with ethyl acetate. But, the method of direct extraction of MCPD with ethyl acetate was useful for rapid ants qualitative analysis. The sample extracted in soysauce(ganjang) was derivatized with phenylboric acid and analyzed by gas chromatography-mass selective detector. That was confirmed as MCPD-phenylboronate.

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Research of Efficiency for Gas Electron Multiplier Detector to Monitor Low Energy Gamma-Ray and Beta-Ray (낮은 에너지 감마선과 베타선 모니터링을 위한 Gas Electron Multiplier 검출기의 효율성에 대한 연구)

  • Lee, Soonhyouk;Jung, Jae Hoon;Lee, Rena
    • Progress in Medical Physics
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    • v.25 no.2
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    • pp.95-99
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    • 2014
  • Radiation monitoring is one of the most important process in all places where radioactive material is used including hospital. In this preliminary study, we made GAS electron multiplier (GEM) detector and acquired relative efficiencies in order to see if GEM detector can be useful in radiation monitoring system. The relative efficiency was acquired by using the ratio of GEM detector efficiency to CdTe detector efficiency. The relative efficiency of 72% and 4% was acquired for beta-ray and gamma-ray respectively.

Development of Scientific Payloads for Korea Sounding Rocket-III (3단형 과학로켓용 과학탑재체 개발)

  • Hwang, Seung Hyeon;Kim, Jun;Lee, Su Jin;Jeon, Yeong Du;Park, Jeong Ju
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.31 no.2
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    • pp.80-88
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    • 2003
  • This paper describes the development of an ozone detector and an electron probe as parts of scientific payloads for sounding rockets such as the KSR-III. Each detector consists of sensor parts and electronic parts. We successfully carried out the calibration tests with developed ozone detector and the space plasma simulation chamber tests with electron detector. These payloads could be onboard the KSR-III and with measured data, it is expected and temperature profile over the Korean Peninsular.

Development of Electron Beam Monte Carlo Simulation and Analysis of SEM Imaging Characteristics (전자빔 몬테 카를로 시물레이션 프로그램 개발 및 전자현미경 이미징 특성 분석)

  • Kim, Heung-Bae
    • Journal of the Korean Society for Precision Engineering
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    • v.29 no.5
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    • pp.554-562
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    • 2012
  • Processing of Scanning electron microscope imaging has been analyzed in both secondary electron (SE) imaging and backscattered electron (BSE) image. Because of unique characteristics of both secondary electron and backscattered electron image, mechanism of imaging process and image quality are quite different each other. For the sake of characterize imaging process, Monte Carlo simulation code have been developed. It simulates electron penetration and depth profile in certain material. In addition, secondary electron and backscattered electron generation process as well as their spatial distribution and energy characteristics can be simulated. Geometries that has fundamental feature have been imaged using the developed Monte Carlo code. Two, SE and BSE images generation process will be discussed. BSE imaging process can be readily used to discriminate in both material and geometry by simply changing position and direction of BSE detector. The developed MC code could be useful to design BSE detector and their position. Furthermore, surface reconstruction technique is possibly developed at the further research efforts. Basics of Monte Carlo simulation method will be discussed as well as characteristics of SE and BSE images.

Multi-Pesticide Residue Method for Organopesticide Analysis (유기농약 분석을 위한 Multi-Pesticide Residue Method)

  • 김우성;이봉헌
    • Journal of Environmental Science International
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    • v.6 no.4
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    • pp.385-389
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    • 1997
  • Pesticide residues were extracted with 70% acetone and transferred to dichloromethane. Extracts were applied to open-column chromatography with florisil and alumina-N. The final extract was analyzed by gas chromatography with electron-capture detector(GC /ECD) and nitrogen-phosphorus detector(GC/NPD). Recoveries of the 17 organochlorine pegticides were ranged from 60.8 to 84.9% and those of 15 organophosphate pesticides, from 70.5% to 100.0%(except phosmet and azlnphos-methyls. The minimum detectable levels of this analytical method were low(0.021-0.058mg/kg).

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A Study on Dose Distribution of Electron Beams by Semiconductor Detector (반도체 검출기에 의한 전자선 선량분포에 관한 연구)

  • Kang, Wee-Saing;Ha, Sung-Whan;Park, Charn-Il
    • Journal of Radiation Protection and Research
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    • v.9 no.1
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    • pp.19-25
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    • 1984
  • There is not yet an universal method of electron dosimetry. The Authors measured dose distributions of the electron beams from Clinac-18 by means of silicon detector connected to X-Y recorder, and compared them in water phantom with dose distributions measured by film and ion chamber, both inserted in polystyrene phantom. The results are as followings, 1. Dose in build-up region increased with the field size for all energy, and depth dose profiles of $6{\sim}12MeV$ beam under the depth of maximum dose were independent of field size, but those of 15 and 18 MeV beam were dependent on the field size. 2. The widths of penumbra by semiconductor detector were narrower than those by film for same energy beam. 3. Depth dose profiles by three different dosimeter did not coincide each other. In the build-up region, dose by semiconductor detector was lower than that by any other dosimeter.

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Simulation of amorphous selenium considering diffraction and interference models (간섭과 회절 모델을 고려한 비정질 셀레늄(a-Se) 시뮬레이션)

  • Kim, Si-hyung;Song, Kwang-soup
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2012.10a
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    • pp.997-999
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    • 2012
  • Digital X-ray image detector is widely used for radiodiagnosis. Amorphous selenium has been received attention as one of the major material that confirmed photoconductor of direct methode detector. We analysis the photocurrent using 2-dimensional device simulator when blue-ray (${\lambda}=486nm$) is irradiated and high voltage is biased. We evaluate electron-hole generation rate, electron-hole recombination rate, and electron/hole distribution in the amorphous selenium. This simulation methode is helpful to the analysis of digital X-ray image detector. We expect that many applications will be developed in digital X-ray image detector using 2-dimensional device simulator.

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