• 제목/요약/키워드: Electrolytic process

검색결과 321건 처리시간 0.023초

금형의 복합연마 특성에 관한 연구 (A Study on the Intergrated Finishing Characteristics for Dies and Molds)

  • 박준민;정해도
    • 한국정밀공학회지
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    • 제15권2호
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    • pp.14-20
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    • 1998
  • Automatic finishing process requires the development of high efficient and precision abrasive machining method for dies and molds. This study describes the evaluation of the finishing characteristics, such as surfrace roughness, topography and material removal depth of the electrolytic mixed abrasive machining methods. Experimental setup is composed of 3 axis machining center, a newly developed finishing attachment with constant pressure, electrode and electrolytic bath. Finally, we achieved a successful result that surface roughness is $0.01\mu$m Ra and material removal depth is $120\mu$m using electrolytic(0.8A. 30V) mixed abrasive (#400 CBN, #320 SiC) machining method.

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금형의 복합연마 특성에 관한 연구 (A Study on the Intergrated Finishing Characteristics for Dies and Molds)

  • 박준민;정해도
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1997년도 춘계학술대회 논문집
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    • pp.937-941
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    • 1997
  • Utomatic finishing process requires the development of high efficient and precision abrasive machining method for die and molds. This study describes the evaluation of the finishing characteristics, such as sufrace roughness, topography and material removal depth, of the electrolytic chemical mixed abrasive machining method. Experimental setup is composed of 3 axis machining center, a newly developed finishing attachment with constant pressure, electrode and electrolytic bath. Finally, we achieved a successful result that surface roughness is 0.01 .mu. m Ra and material removal depth is 145 .mu. m after 100 times repeat-finishing using electrolytic (0.8A,30V) mixed abrasive (#400 CBN, #320 Sic) machining method.

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MOLTEN SALT VAPORIZATION DURING ELECTROLYTIC REDUCTION

  • Hur, Jin-Mok;Jeong, Sang-Moon;Lee, Han-Soo
    • Nuclear Engineering and Technology
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    • 제42권1호
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    • pp.73-78
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    • 2010
  • The suppression of molten salt vaporization is one of the key technical issues in the electrolytic reduction process developed for recycling spent nuclear fuel from light-water reactors Since the Hertz-Langmuir relation previously applied to molten salt vaporization is valid only for vaporization into a vacuum, a diffusion model was derived to quantitatively assess the vaporization of LiCl, $Li_2O$ and Li from an electrolytic reducer operating under atmospheric pressure. Vaporization rates as a function of operation variables were calculated and shown to be in reasonable agreement with the experimental data obtained from thermogravimetry.

미세 펄스전원을 이용한 스테인레스강의 전기화학연마 (Study on Electrochemical Polishing for Stainless Steel using Micro Pulse Current)

  • 이동활;박정우;문영훈
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2003년도 춘계학술대회논문집
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    • pp.127-130
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    • 2003
  • Electrolytic polishing is the anodic dissolution process in the transpassive state. It removes non-metallic inclusions and improves mechanical and corrosion resistance of stainless steel. Electrolytic polishing is normally used to remove a very thin layer of material from the surface of a metal object. An electrolyte of phosphoric, sulfuric and distilled water has been used in this study. In the low current density region, there can be found plateau region and material removal process and leveling process occur successively. In this study, an electrochemical polishing process using pulse current is adopted as a new electrochemical polishing process. In electrochemical machining processes, it has been found that pulse electrochemical processes provide an attractive alternative to the electrochemical processes using continuous current. Hence, this study will discuss the electrochemical polishing processes in low current density region and pulse electrochemical polishing.

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전기분해와 UV 조사에 의한 수중의 Rhodamine B의 제거(I) (Removal of Rhodamine B in Water by Ultraviolet Radiation Combined with Electrolysis(I))

  • 박영식
    • 한국환경보건학회지
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    • 제34권6호
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    • pp.439-445
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    • 2008
  • The feasibility study for the application of the removal and mineralization of Rhodamine B (RhB) was performed in a batch electrochemical reactor. The electro/UV process was consisted of DSA (dimensionally stable anode) electrode and UV-C or ozone lamp. The experimental results showed that RhB removal by the ozone lamp was higher than that of the UV-C lamp. Optimum current of the electro/UV process was 1 A. The electrochemical, UV and electro/UV process could completely degrade RhB, while a prolonged treatment was necessary to reach a high level RhB mineralization. It was observed that RhB removal in electro/UV process is similar to the sum of the UV and electrolytic decolorization. However, it was found that the COD of RhB could be degraded more efficiently by the electro/UV process (90.2 %) than the sum of the two individual oxidation processes [UV (19.7%) and electrolytic process (50.8%)]. A synergetic effect was demonstrated between the UV and electrolysis.

미세 펄스전원을 이용한 스테인레스강 300 계열의 전기화학연마 (Study on Electrochemical Polishing for Stainless Steel 300 Series using Micro Pulse Current)

  • 이동활;박정우;문영훈
    • 소성∙가공
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    • 제12권4호
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    • pp.388-393
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    • 2003
  • Electrolytic polishing is the anodic dissolution process in the transpassive state. It removes non-metallic inclusions and improves mechanical and corrosion resistance of stainless steel. Electrolytic polishing is normally used to remove a very thin layer of material from the surface of a metal object. An electrolyte of phosphoric acid 50% in vol., sulfuric acid 20% in vol. and distilled water 30% in vol. has been used in this study. In the low current density region, there can be found plateau region and material removal process and leveling process occur successively. In this study, an electrochemical polishing process using pulse current is adopted as a new electrochemical polishing process. In electrochemical machining processes, it has been found that pulse electrochemical processes provide an attractive alternative to the electrochemical processes using continuous current. Hence, this study will discuss the electrochemical polishing processes in low current density region and pulse electrochemical polishing.

전해수를 이용한 견섬유 정련 및 세리신 회수(II)-분리막에 의한 세리신 농축을 중심으로- (The Degumming and Sericin Recovery of the Silk fabric Using the Electrolytic Water(II))

  • 배기서;이태상;노덕길;홍영기
    • 한국염색가공학회지
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    • 제16권4호
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    • pp.10-18
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    • 2004
  • In this work, Aqueous sericin solution was prepared by degumming process with electrolytic reduction water. Then, the microfiltration and ultrafiltration systems were applied to the concentration of aqueous sericin solution. The objective of this study was to select the optimum operating condition among the different pressure. The permeate flux and rejection ratio were observed with time, pressure, flow rate and concentration. and, the wastewater and permeated water quality values such as pH, BOD, COD, and NH levels were measured. In order to see the influence of electrolytic reduction water, the flux of pure water and electrolytic reduction water by PVDF22(MF) and PS100(UF) membrane was measured. In microfiltration system, the relative flux reduction decreased rapidly to 0.02 in the 30min, as the concentration polarization and gel layer formation were increased. and then the sericin concentration rejection ratio was 40%. In ultrafiltration system, the permeate flux decreased with time and concentration, and increased with the operating pressure and flow rate. Optimal condition in PS100 membrane system for sericin concentration was operating pressure 1.464kgf/$cm^24, operating flow rate $7\ell/min at\; 40^{\circ}C$. At that time, sericin concentration rejection ratio was 83% respectably. The sericin solution was concentrated from 0.1wt% solution to 0.2 wt % solution during about 2 hrs by the UF filteration membrane system.

Development of a Mass Transfer Model and Its Application to the Behavior of the Cs, Sr, Ba, and Oxygen ions in an Electrolytic Reduction Process for SF

  • 박병흥;강대승;서중석;박성원
    • 방사성폐기물학회지
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    • 제3권2호
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    • pp.85-93
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    • 2005
  • Isotopes of alkali and alkaline earth metals (AM and AEM) are the main contributors to the heat load and the radiotoxicity of spent fuel (SF) . These components are separated from the SF and dissolved in a molten LiCl in an electrolytic reduction process. A mass transfer model is developed to describe the diffusion behavior of Cs, Sr, and Ba in the SF into the molten salt. The model is an analytical solution of Fick's second law of diffusion for a cylinder which is the shape of a cathode in the electrolytic reduction process. And the model is also applied to depict the concentration profile of the oxygen ion which is produced by the electrolysis of Li$_{2}$O. The regressed diffusion coefficients of the model correlating the experimentally measured data are evaluated to be greater in the order of Ba, Cs, and Sr for the metal ions and the diffusion of the oxygen ion is slower than the metal ions which implies that different mechanisms govern the diffusion of the metal ions and the oxygen ions in a molten LiCl.

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전해드레싱연삭에서 숫돌주속과 표면거칠기의 관계 (Relationships between Wheel Velocity and Surface Roughness in the Electrolytic In-Process Dressing(ELID) Grinding)

  • 차명섭
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2000년도 춘계학술대회논문집 - 한국공작기계학회
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    • pp.459-464
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    • 2000
  • In this paper, it verifies the relationships between wheel velocity and surface roughness with the mirror surface grinding using electrolytic in-process dressing (ELID). In the general, as wheel velocity is high, surface roughness is better on the base of grinding theory. However, the relationships between wheel velocity and surface roughness is undefined due to the effect of electro-chemical dressing and the characteristics of materials. According to above relationships, ELID grinding experiment is carried out by following the change of wheel velocity. As the result of this study, it is found that surface roughness is not better as linearly as the increase of wheel velocity, but the limit of wheel velocity exists according to the characteristics of materials. Also, in contradiction to the present trend of high wheel velocity of manufacturing system for high surface integrity, it is able to expected to the base on the development of new ultra precision grinding method with the practicality of mirror surface grinding using ELID grinding method.

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Characteristics of a Titanium-oxide Layer Prepared by Plasma Electrolytic Oxidation for Hydrogen-ion Sensing

  • Lee, Do Kyung;Hwang, Deok Rok;Sohn, Young-Soo
    • 센서학회지
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    • 제28권2호
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    • pp.76-80
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    • 2019
  • The characteristics of a titanium oxide layer prepared using a plasma electrolytic oxidation (PEO) process were investigated, using an extended gate ion sensitive field effect transistor (EG-ISFET) to confirm the layer's capability to react with hydrogen ions. The surface morphology and element distribution of the PEO-processed titanium oxide were observed and analyzed using field-emission scanning-electron microscopy (FE-SEM) and energy-distribution spectroscopy (EDS). The titanium oxide prepared by the PEO process was utilized as a hydrogen-ion sensing membrane and an extended gate insulator. A commercially available n-channel enhancement MOS-FET (metal-oxide-semiconductor FET) played a role as a transducer. The responses of the PEO-processed titanium oxide to different pH solutions were analyzed. The output drain current was linearly related to the pH solutions in the range of pH 4 to pH 12. It was confirmed that the titanium-oxide layer prepared by the PEO process could feasibly be used as a hydrogen-ion-sensing membrane for EGFET measurements.