• Transactions of Materials Processing
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• v.11 no.1
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• pp.45-53
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• 2002

The forming process of metal matrix composites by die casting and squeeze casting process are limited in size and dimension In term of final parts. The melt strirring method have the problems that the homogeneous distribution of the reinforcements is difficult due to the low weldability and the density difference between the molten metal and the reinforcement. The thixoforming process for metal matrix composites has numerous advantages compacted to die casting, squeeze casting and compocasting. However, for the thixofoming process, the billet with the desired volume fraction must be heated to obtain a uniform temperature distribution over the entire cross-sectional areas. To obtain the reheating conditions of composites, the particulate reinforced metal matrix composites for thixoforming were fabricated by combined stirring process which is simultaneously performed with electro-magnetic stirring and mechanical stirring process. The matrix alloy and reinforcement are used to aluminum alloy(A357) and SiCp with diameter 14, $25{\mu}m$, respectively. The microstructure characteristics were investigated by changing the volume fraction and reinforcement size. The heating conditions to obtain the uniform temperature distribution in cross section area of fabricated metal matrix composites billet are proposed with heating time, the heating temperature and the holding time.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1997.10a
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• pp.808-811
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• 1997

MMC has excellent mechanical properties in many ways in automotive industrial, and get into the spotlight as a light materials substituted for iron and steel. But the know-how about MMC research lack, MMC is expensive and difficult to apply the sound parts. Especially it is difficult to produce the hollow type parts composed with MMC. Therefore, hollow type parts of metal composites by using thixoforming process which as co-existing solidus-liquidus phase, it is very important to obtain forming condition. In this study, MMC billet producted by electro-magnetic stirring and mechanical stirring process is formed to hollow type parts of thixoforming process and inspected of suitability for application. It is optimized production condition, and applied to experiment. After variable materials were produced for thixoforming process, it were inspected of suitability for application by comparsion with mechanical properties. In this study, used materials were A357, A380 10%vol, and 20%vol SiCp, and the size of particultes were 14$\mu\textrm{m}$ and 5.5$\mu\textrm{m}$.

• Composites Research
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• v.14 no.5
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• pp.1-11
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• 2001

The particulates reinforced metal matrix composites(PMMC) have a number of interesting mechanical properties. including high strength and good resistance to wear at high temperature and low thermal expansion. The equipment structure to obtain the homogeneous distribution in composites are proposed for the continuous pouring of reinforcement at the desired temperature. The particulates reinforced metal matrix composites(A357/SiCp) were fabricated by the process of the combined stirring method with the various fabrication process. The combined stirring method to niform distribution of particle is consisted of two stirring force both electro-magnetic stirring generated from induction heating and mechanical stirring with graphite stirrer. PMMC billets were fabricated with the volume fractions ranged from 0% to 20% and particle sizes ranged from 14${\mu}{\textrm}{m}$ to 25${\mu}{\textrm}{m}$. It is important to cont the size of primary $\alpha$-Al solid particles because it could become the cause of the particle pushing or capture phenomena from the fact that secondary dendrite arm spacing size depends on the cooling rate during the solidification in hypoeutectic Al-Si alloy. Therefore, the effect of primary $\alpha$-Al on the reinforcement distribution in matrix alloys has been investigated. The microstructure of PMMC fabracated with various volume fractions(0%, 10%, and 20%) and particle size were observed.

• Transactions of Materials Processing
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• v.7 no.3
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• pp.215-224
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• 1998

A semi-solid forming has a lot of advantages compared to the die casting. squeeze casting and conventional forging. therefore, semi-solid forming process is now becoming industrial interest for the production of metal components and metal matrix composites. However the material behaviour in the semi-solid temperature range is not sufficiently known although it controls the whole process through forces and geometry evolutions because the behaviour of metal slurries is complex. The semi-solid materials(SSMs) fabricated under electric-magnetic stirring condition is necessary to be applicated in forming process. A reheating conditions were studied with the reheating time holding time and reheating temperatures. The microstructure of SSM(specimen size : d39${\times}$h85) at the condition of heating time 10min and heating temperature 590${\circ}C$ is the most globular and finest one. The microstructure of SSM(specimen size : d76${\times}$h60) reheated under the three step reheating conditions is most globular and finest.

• Journal of Korea Foundry Society
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• v.40 no.3
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• pp.61-65
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• 2020

Rheo-diecasting with stirring has been used in many material industries. As the 4th Industrial Revolution approaches the world, eco-friendly high-strength and light-weight materials become more important. Casting methods have been studied and used for aluminum-alloy automobile parts. This study carried out the effect analysis of the micro-structure and mechanical properties, such as yield/ultimate tensile strength, elongation, and hardness, of A356 using the 6-pole EMS (electro-magnetic stirring) casting process with a high electromagnetic force. As a result, the hardness and elongation of the A356 after T6 heat-treatment show a significant improvement, respectively, by 20% and 50%.

• 한국전산유체공학회:학술대회논문집
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• 2005.04a
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• pp.1-13
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• 2005

Fluid flows within microchannels are characterized by low Reynolds numbers. Therefore the effect of mixing is a crucial factor in design of the channels. Since the action of the electro-osmotic or magnetic forces used in the mixing enhancement is usually periodic in the three-dimensional channel configuration, use of the various concepts of chaotic advection is reasonable in the quantification of the stirring effect. In this paper, the details of the method of material-stretching mapping is explained. The actual application of the method to the screw extruder is also presented.

• 한국신재생에너지학회:학술대회논문집
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• 2010.06a
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• pp.146.2-146.2
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• 2010

PEMFC를 구성하는 여러 부품 중 핵심부품은 MEA(Membrane Electrode Assembly)으로서 실제 연료전지 반응이 일어나며 연료전지의 성능을 결정하는 부품이다. 그러나 PEMFC의 특성 상 촉매로 귀금속인 Pt가 사용됨에 따라 경제성이 확보된 MEA의 성능을 얻기 위해선 현재 Pt 담지량을 0.3mg/$cm^2$ 이하로 크게 감소시키면서 Pt촉매의 고분산화와 미반응 사이트의 감소가 필요하다. 본 연구에서는 Pt 촉매의 미반응 사이트를 줄이고자 전기영동법에 의해 카본전극(carbon black + GDL) 상에 Pt 나노입자를 직접 석출시켜 Pt/C 촉매 전극을 제조 하였다. 본 실험에서는 가장 좋은 Pt 나노입자의 석출거동을 나타낸 30mA/$cm^2$, pH 2, duty cycle 25% 조건을 기준으로 하여 electro-deposition time을 통한 석출량 제어와 carbon paper의 wet proofing 정도에 따른 Pt의 석출거동을 조사하였으며, 종래의 방법으로 제조한 Pt/C 촉매전극의 전기화학적 특성과 비교 분석하였다. 전기영동 석출법에 사용된 Pt나노입자는 $H_2PtCl_6{\cdot}6H_2O$로부터 화학적 환원법으로 합성한 2~3nm 입경을 갖는 Pt콜로이드를 사용하였으며, magnetic stirring과 항온 ($20^{\circ}C$)을 유지하여 실험하였다. 전기영동 석출량 제어는 electro-deposition time을 5~25분까지 5분 간격으로 나누어 실험하였고 카본전극을 구성하는 carbon paper의 wet proofing 정도가 Pt 나노입자 석출거동에 미치는 영향을 조사하기 위하여 20, 40, 60%의 서로 다른 wet proofing 값을 갖는 carbon paper를 사용하여 Pt/C 촉매 전극을 제조하였다. 전기영동법으로 석출된 카본블랙 전극 상 Pt나노입자의 분산도와 담지량는 각각 FE-SEM과 TGA 장비를 사용하여 측정하였고, 제조된 Pt/C 촉매 전극의 전기화학적 촉매 특성은 cyclic voltammetry(CV)법으로 측정하였다.

• Journal of Korea Foundry Society
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• v.20 no.4
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• pp.269-276
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• 2000

So far, the study on semi-solid process has been carried out to develop and research new advanced materials without some casting defects. In this study, A356 billets consisted of various dendritic shapes were prepared using electro-magnetic stirring process continuously. As-cast respectively has liquidus temperature of $625.6^{\circ}C$ and solidus temperature of $573.55^{\circ}C$ A356 slugs were reheated homogeneously at different temperatures of 580, 590 and $605^{\circ}C$, followed by squeezing in a mold insulated with applied pressures(0, 25, 50 and 70 MPa). In order to investigate on aging responce for casts, 50 MPa squeezed specimen among all specimens was prepared in aging treatments, which conditions are aging temperature of $160^{\circ}C$ and holding times of 0, 45, 90, 270, 360, 720, 1440 and 2880 min after solution treatment ($540^{\circ}C$ for 10 hr). SSM ingot with the output velocity of 150mm/min appeared more spheroidal shape and fine structure than that with the output velocity of 250 mm/min. According to increasing in reheating temperature, numbers of fatigue cycles, U.T.S and elongation increased at same time.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.06a
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• pp.15-32
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• 1999

A relationship between stress and stain is very important to design a die to avoid defects of products during semi-solid forming process. Since the liquid will be of eutectic composition in alloys liquid segregation will result in significant or undesirable situation. The materials used in this experiment are A 357. A390, Al2024 alloys that is fabricated by the electro-magnetic stirring process from Pechiney in France. The compression test was performed by induction heating equipment and MTS. In order to prevent the liquid segregation these measured temperature would be useful to control of strain rate during compression test. The liquid segregation is controlled as change of the strain rate and solid fraction during the compression process, The characteristics of flow between solid and liquid phase considering liquid segregation is examined through the above experiments. In the case of medium and high volume fractions of solid the distribution of strain rate is calculated by using compression test data of semi-solid materials (SSM). The thixoforming experiments with the designed die are carried out successfully. The die filling patterns of SSM for variation of die temperature and pressing force have been investigated. The hardness of the thixoformed scroll products is evaluated in terms of the microstructure for each position.