• Analytical Science and Technology
• /
• v.5 no.3
• /
• pp.309-317
• /
• 1992

Inorganic/organic composite was synthesized by using sol-gel process, and the bonding characteristics of composite was investigated with glass transition temperature(Tg), measured by DMTA(Dynamic Mechanical Thermal Analyzer). It was found from shift of Tg to higher temperature that composite reaction was proceeded better with the amount of HCl and water. But Tg was not varied with reaction time.

• Elastomers and Composites
• /
• v.52 no.4
• /
• pp.326-331
• /
• 2017

Two kinds of polyurethane elastomers were prepared and their acoustical properties underwater investigated. Their dynamic mechanical properties were measured using a dynamic mechanical analyzer. The sound speed and echo reduction in the 1-50 kHz frequency range were calculated from the data obtained using the analyzer. The sound speed, transmission and attenuation cofficient in 300-800 kHz were measured in a water-filled tank. Impedance tube experiments were performed to determine the reflective coefficient and echo reduction in the 3-8 kHz range. The polyurethane elastomer containing a hollow glass sphere showed a lower reflective coefficient and a higher echo reduction than the polyurethane elastomer without a filler.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.26 no.7
• /
• pp.1416-1425
• /
• 2002

In this study, the effects of combined environmental factors on mechanical and thermal analysis properties of graphite/epoxy composites were evaluated by the use of an accelerated aging test. Environmental factors such as temperature, moisture. and ultraviolet were considered. A xenon-arc lamp was utilized for ultraviolet light. and exposure times of up to 3000 hours were applied. Several types of specimens - tensile. bending, and shear specimens those are transverse to the fiber direction, and bending specimens those are parallel to the tiber direction - were used to investigate the effects of environmental factors on mechanical properties of the composites. Also, glass transition temperature, storage shear modulus, loss shear modulus, and tan ${\delta}$ were measured as a function of exposure times through a dynamic mechanical analyzer. In addition. a suitable testing method for determining the effect of environmental factors on mechanical properties is suggested by comparing the results from using two different types of strain measuring sensors. Finally, composite surfaces exposed to environmental factors were examined using a scanning electron microscope.

• Proceedings of the Korean Society For Composite Materials Conference
• /
• 2004.04a
• /
• pp.139-142
• /
• 2004

As fiber reinforced composite materials are widely used in aircraft, space structures and robot arms, the study on the non-destructive testing methods of the composite materials has become an important research area for improving their reliability and safety. In this paper, the AE signal analyzer with the resonance circuit to extract the specified frequency of the acoustic emission signal were designed and fabricated. The noise levels of the fabricated AE signal analyzer by the disturbance such as impact or mechanical vibration had a very small value comparable to those of the conventional AE signal analyzer. Also, the crack detection capabilities of the fabricated AE signal analyzer under the static and dynamic tensile test were evaluated and compared with the conventional AE signal analyzer.

• Journal of Biosystems Engineering
• /
• v.37 no.1
• /
• pp.28-35
• /
• 2012

Purpose: This study performed the oscillatory test using the texture analyzer to characterize the viscoelastic behavior of apples such as the storage modulus (E'), the loss modulus (E"), the complex modulus (${\mid}E^*{\mid}$) and the energy dissipated per cycle ($W_{diss}$). Methods: The sinusoidal deformation with the frequency of 1-10 Hz and the maximum displacement of 0.1 mm were applied to the flesh tissues of Fuji, Golden Delicious and Red Delicious apples. The Lissajous figure was used to measure the phase angle(${\delta}$) between stress and strain curve. Results: Trigger force was critical to the measurement of the phase angle. E', E", ${\mid}E^*{\mid}$ and Wdiss were measured using the Lissajous figure and the phase angle. The complex modulus of Golden Delicious apple was significantly lower than those of Fuji apple and Red Delicious apple. Conclusions: Apple flesh was exhibiting more elasticity at low frequency, and more viscosity at high frequency. Dynamic compressive properties of Fuji apple were similar to those of Red Delicious apple but significantly different from those of Golden Delicious apple.

• Korean Journal of Materials Research
• /
• v.10 no.3
• /
• pp.184-190
• /
• 2000

We investigated the effect of filler content on the thermo-mechanical properties of modified ACA composite materials by incorporation of non-conducting fillers and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACA s composites with different content of non-conducting fillers, differential scanning calorimeter (DSC), and thermo-gravimetric analyzer (TGA), dynamic mechanical analyzer (DMA), and thermo-mechnical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in the content of filler brought about the increase of Tg^{DSC}$ and $Tg^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significantly affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.

• Journal of Mechanical Science and Technology
• /
• v.17 no.1
• /
• pp.129-138
• /
• 2003

A 1 : 20 laboratory scale test rig of a 200 MW tangentially fired boiler is built up with completely simulated structures such as platen heaters and burners. Iso-thermal turbulent flow in the boiler is mapped by 3-D PDA (Particle Dynamic Analyzer). The 3-D numerical models for the same case are proposed based on the solution of к-$\varepsilon$ model closed RANS (Reynolds time-Averaged Navier-Stokes) equations, which are written in the framework of general coordinates and discretized in the corresponding body-fitted meshes. Not only are the grid lines arranged to fit the inner/outer boundaries. but also to align with the streamlines to the best possibility in order to reduce the NDE (numerical diffusion errors). Extensive comparisons of profiles of mean velocities are carried out between experiment and calculation. Predicted velocities in burner region were quantitatively similar with measured ones, while those in other area have same tendency with experimental counterpart.

• Proceedings of the International Microelectronics And Packaging Society Conference
• /
• 2000.04a
• /
• pp.9-15
• /
• 2000

Flip chip assembly on organic substrates using ACAs have received much attentions due to many advantages such as easier processing, good electrical performance, lower cost, and low temperature processing compatible with organic substrates. ACAs are generally composed of epoxy polymer resin and small amount of conductive fillers (less than 10 wt. %). As a result, ACAs have almost the same CTE values as an epoxy material itself which are higher than conventional underfill materials which contains lots of fillers. Therefore, it is necessary to lower the CTE value of ACAs to obtain more reliable flip chip assembly on organic substrates using ACAs. To modify the ACA composite materials with some amount of conductive fillers, non-conductive fillers were incorporated into ACAs. In this paper, we investigated the effect of fillers on the thermo-mechanical properties of modified ACA composite materials and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACAs composites with different content of non-conducting fillers, dynamic scanning calorimeter (DSC), and thermo-gravimetric analyzer (TGA), dynamic mechanical analyzer (DMA), and thermo-mechanical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in tile content of filler brought about the increase of Tg$^{DSC}$ and Tg$^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significant affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.ers.

• Journal of the Semiconductor & Display Technology
• /
• v.22 no.3
• /
• pp.90-95
• /
• 2023

We describe an optimal alignment method for improving accuracy of dynamic spectroscopic polarimeter based on monolithic polarizing interferometer. The dynamic spectroscopic polarimeter enables real-time measurements of spectral ellipsometric parameters by using a spectral carrier frequency concept. However, the non-polarizing beam splitter used in the monolithic polarizing interferometer cannot maintain the polarization state perfectly due to phase retardation caused by optical anisotropic characteristics of the non-polarizing beam splitter, resulting in degraded measurement accuracy. The effect of the beam splitter can be minimized through optimal alignment of the polarizers used in the polarizing interferometer and the analyzer. We demonstrate how much the proposed alignment method can enhance the measurement accuracy by comparing with previous alignment approach.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.18 no.3
• /
• pp.635-644
• /
• 1994

This study investigated mainly on the flow characteristics of a droplet in the cross region of twin spray. The velocities of the droplet were measured along the axial and radial direction, and the flow characteristics of the droplet were statistically analyzed. For the statistical analysis, the probability density of the turbulent components has been studied, and then the Reynolds shear stress, the skewness and the flatness factors were calculated, and compared with the Gaussian value. Two pressure swirl stomizers were used for the twin spray system and kerosene was employed as the working liquid. 2-D PDA(particle dynamic analyzer) was used for the purpose of the measurement of droplet size and velocities. As a result, it was found that (1) the droplets collision was taken place strongly in the cross region. So, a large momentum loss of droplets due to the loss of natural movement direction was occurred, and momentum loss of radial direction was greater than that of axial direction. (2) The axial direction skewness factor approached to zero like the Gaussian distribution in the cross region of twin spray. (3) In the cross region of twin spray, the fluctuation instability of droplet was increased because of the development of the turbulence characteristics due to the droplet collision.