• Title/Summary/Keyword: Dynamic Complex Modulus

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Effect of Storage Temperature on Dynamic Rheological Properties of Hot Pepper-Soybean Pastes Mixed with Guar Gum and Xanthan Gum

  • Choi, Su-Jin;Yoo, Byoung-Seung
    • Food Science and Biotechnology
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    • v.16 no.3
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    • pp.496-499
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    • 2007
  • Dynamic rheological properties of hot pepper-soybean paste (HPSP) samples mixed with guar gum and xanthan gum were evaluated at different storage temperatures (5, 15, and $25^{\circ}C$) by using a dynamic rheometer. Magnitudes of storage modulus (G'), loss modulus (G"), and complex viscosity (${\eta}^*$) in the HPSP-gum mixtures increased with an increase in storage temperature from 5 to $25^{\circ}C$. After 3-month storage at 5 and $15^{\circ}C$ there were no significant changes in dynamic rheological properties. The increase in dynamic moduli (G', G", and ${\eta}^*$) with storage temperature is less pronounced at HPSP-xanthan gum mixtures in comparison to HPSP-guar gum mixtures. The slopes of G' (0.16-0.18) of HPSP-guar gum mixtures at 3-month storage were much higher than that (0.10) at 0-month storage, indicating that the elastic properties of the HPSP-guar gum mixtures can be decreased after 3-month storage. However, there were not much differences between the slopes of G' in HPSP-xathan gum mixtures. Xanthan gum was observed to be better structure stabilizer for HPSP during storage.

RHEOLOGIC STUDY ON THE VISCOELASTIC PROPERTIES OF FLOWABLE AND CONDENSABLE RESIN COMPOSITES (유동성 및 응축성 복합레진의 점탄성에 관한 유변학적 연구)

  • Lee, In-Bog;Cho, Byeong-Hoon;Son, Ho-Hyun;Kwon, Hyuk-Choon;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.25 no.3
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    • pp.359-370
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    • 2000
  • The purpose of this investigation was to observe the viscoelastic properties of five commercial flowable(Aeliteflo, Flow it, Revolution, Tetric flow, Compoglass flow), three conventional hybrid(Z-100, Z-250, P-60) and two condensable(Synergy compact, SureFil) resin composites. A dynamic oscillatory shear test was done to evaluate the storage shear modulus (G'), loss shear modulus(G"), loss tangent(tan ${\delta}$) and complex viscosity(${\eta}^*$) of the resin composites as a function of frequency - dynamic frequency sweep test from 0.01 to 100 rad/s at $25^{\circ}C$ - by using Advanced Rheometric Expansion System(ARES). To investigate the effect on the viscosity of resin composites of filler volume fraction, the filler weight % and volume % were measured by means of Archimedes' principle using a pyknometer. The results were as follows 1. The complex viscosity ${\eta}^*$ of flowable resins was lower than that of hybrid resins and significant differences were observed between brands. The complex viscosity ${\eta}^*$ of condensable resins was higher than that of hybrid resins. The order of complex viscosity ${\eta}^*$ at ${\omega}$=10 rad/s was as follows, Surefil, Synergy compact, P-60, Z-250, Z-100, Aeliteflo, Tetric flow, Compoglass flow, Flow it, Revolution. The relative complex viscosity of flowable resins compared to Z-100 was 0.04~0.56 but Surefil was 30.4 times higher than that of Z-100. 2. The storage shear modulus G' and the loss shear modulus G" of flowable resins were lower than those of hybrid resins but those of condensable resins were higher. The patterns of the change of loss tangent, tan ${\delta}$, of resin composites with increasing frequency were significantly different between brands. The phase angles, ${\delta}$, ranged from $30.2{\sim}78.1^{\circ}$ at ${\omega}$=10 rad/s. 3. All composite resins represent pseudoplastic nature with increasing shear rate. 4. The complex shear modulus $G^*$ and the phase angle ${\delta}$ was represented by the frequency domain phasor form, $G^*({\omega})=G^*e^{i{\delta}}=G^*{\angle}{\delta}$. The locus of frequency domain phasor plots in a complex plane was a valuable method that represent the viscoelastic properties of composite resins. 5. There was no direct linear correlationship but a weak positive relation was observed between filler volume % or weight % and the viscosity of the resin composites.

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Dynamic analysis of frames with viscoelastic dampers: a comparison of damper models

  • Lewandowski, R.;Bartkowiak, A.;Maciejewski, H.
    • Structural Engineering and Mechanics
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    • v.41 no.1
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    • pp.113-137
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    • 2012
  • Frame structures with viscoelastic (VE) dampers mounted on them are considered in this paper. It is the aim of this paper to compare the dynamic characteristics of frame structures with VE dampers when the dampers are modelled by means of different models. The classical rheological models, the model with the fractional order derivative, and the complex modulus model are used. A relatively large structure with VE dampers is considered in order to make the results of comparison more representative. The formulae for dissipation energy are derived. The finite element method is used to derive the equations of motion of the structure with dampers and such equations are written in terms of both physical and state-space variables. The solution to motion equations in the frequency domain is given and the dynamic properties of the structure with VE dampers are determined as a solution to the appropriately defined eigenvalue problem. Several conclusions concerning the applicability of a family of models of VE dampers are formulated on the basis of results of an extensive numerical analysis.

Steady and Dynamic Shear Rheological Properties of Buckwheat Starch-galactomannan Mixtures

  • Choi, Dong-Won;Chang, Yoon-Hyuk
    • Preventive Nutrition and Food Science
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    • v.17 no.3
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    • pp.192-196
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    • 2012
  • This study investigated the effects of galacomannans (guar gum, tara gum, and locust bean gum) on the rheological properties of buckwheat starch pastes under steady and dynamic shear conditions. The power law and Casson models were applied to describe the flow behavior of the buckwheat starch and galactomannan mixtures. The values of the apparent viscosity (${\eta}_{a,100}$), consistency index (K), and yield stress (${\sigma}_{oc}$) for buckwheat starch-galactomannan mixtures were significantly greater than those for the control, indicating that there was a high synergism of the starch with galactomannans. The magnitudes of storage modulus (G') and loss modulus (G") for the starch-galactomannan mixtures increased with increasing frequency (${\omega}$). The dynamic moduli (G', G"), and complex viscosity (${\eta}^*$) for the buckwheat starch-galactomannan mixtures were significantly higher than those for the control.

The dynamic response of the FGM coated half-plane with hysteretic damping under time harmonic loading

  • Xiao-Min Wang;Liao-Liang Ke;Yue-Sheng Wang
    • Structural Engineering and Mechanics
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    • v.87 no.1
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    • pp.95-106
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    • 2023
  • This paper investigates the dynamic response of a functionally graded material (FGM) coated half-plane excited by distributed time harmonic loading. Three types of typical distributed surface loads, including uniform load, Hertz load, and square-root singular load, are considered. The mass density and elastic modulus of the FGM coating are supposed to be described by the exponential function. The material damping is modelled by a linearly hysteretic damping which is expressed by a complex modulus in the time harmonic motion. Using Fourier integral transform technique and numerical integral method, the effects of the excitation frequency, gradient index, damping, and load type on the dynamic stresses and displacements are discussed.

A Study on the Characteristics of Dynamic Elastic Modulus in GyeongGi Gneiss Complex by Down Hole Test (하향식 탄성파를 통한 경기 편마암의 동탄성 특성연구)

  • Lee, Byok-Kyu;Lee, Su-Gon
    • The Journal of Engineering Geology
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    • v.18 no.4
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    • pp.371-379
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    • 2008
  • In this study, seismic elastic wave and dynamic elastic modulus properties are investigated by down-hole seismic tests that were applied to the 11 gneiss area. The research results show that the realtionship between the two properties are $V_s=0.5589{\times}V_p$ in gneiss. The relationship between the two properties are separated into two groups. Group 1 is influenced mainly by the specific gravity of rock, but group 2 is influenced mainly by the joint aperture. As weathering progresses, group 1 clearly shows a decreasing tendency. In fresh and slightly weathered rock-mass, correlations between $V_p$ and dynamic elastic modulus is expressed in linear line but in moderately-highly weathered rock-mass, correlations between $V_p$ and dynamic elastic modulus is expressed curve as a quadratic function. Correlations between $V_s$ and dynamic elastic modulus are analyzed similar with a $V_p$ case.

Vertical and torsional soil reactions for radially inhomogeneous soil layer

  • El Naggar, M. Hesham
    • Structural Engineering and Mechanics
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    • v.10 no.4
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    • pp.299-312
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    • 2000
  • The response of an embedded body to dynamic loads is greatly influenced by the reactions of the soil to the motion of the body. The properties of the soil surrounding embedded bodies (e.g., piles) may be different than those of the far-field for a variety of reasons. It may be weakened or strengthened according to the method of installation of piles, or altered due to applying one of the soil strengthening technique (e.g., electrokinetic treatment of soil, El Naggar et al. 1998). In all these cases, the shear strength of the soils and its shear modulus vary gradually in the radial direction, resulting in a radially inhomogeneous soil layer. This paper describes an analysis to compute vertical and torsional dynamic soil reactions of a radially inhomogeneous soil layer with a circular hole. These soil reactions could then be used to model the soil resistance in the analysis of the pile vibration under dynamic loads. The soil layer is considered to have a piecewise, radial variation for the complex shear modulus. The model is developed for soil layers improved using the electrokinetic technique but can be used for other situations where the soil properties vary gradually in the radial direction (strengthened or weakened). The soil reactions (impedance functions) are evaluated over a wide range of parameters and compared with those obtained from other solutions. A parametric study was performed to examine the effect of different soil improvement parameters on vertical and torsional impedance functions of the soil. The effect of the increase in the shear modulus and the width of the improved zone is investigated.

A Study on Determining Complex Young's Modulus of Acoustic Materials (음향 재질의 복소수 모듈러스 추출에 관한 연구)

  • Kim, In-Su;Lee, Hyo-Keun;Kim, Sung-Hee
    • The Journal of the Acoustical Society of Korea
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    • v.10 no.1
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    • pp.30-36
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    • 1991
  • Since the Complex Young's Modulus of acoustic materials is a function of frequency under a static load, a cylindrical specimen modelled by rod-like one with losses is used to determine the dynamic characteristics of materials. The specimen is excited into longitudinal vibration at its one end by shaker and at the other end, loaded by a mass corresponding to the desired static load and thus the transfer function of specimen is measured. This transfer function method is analyzed theoretically and experimentally over a frequency range of 50 Hz to 20 KHz. The analysis includes the measurability of the transfer function, the frequency range of the method and lateral motion effect.

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Measurement Method of Complex Dynamic Viscoelastic Material Properties (점탄성 재료의 복소수 동특성 측정방법)

  • Lee, In-Won;An, Nam-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.33 no.5
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    • pp.489-495
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    • 2009
  • A novel technique to measuret of viscoelastic properties of polymers is proposed to investigate complex Poisson's ratio as a function of frequency. The forced vibration responses for the samples under the normal and the shear deformation are to be measured with varying load masses. The measured data were used to obtain the viscoelastic properties of the material based on an accurate 2D numerical deformation model of the sample. The 2D model enabled us to exclude data correction by the empirical form factor used in 1D model. Comprehensive measurements of viscoelastic properties of two slightly varied silicone RTV rubber ($Silastic^{(R)}$ S2) compositions were performed. Standard composition (90% PDMS polymer + 10% catalyst) and modified composition (92.5% polymer + 7.5% catalyst) were tested in temperature range from $30^{\circ}C$ to $70^{\circ}C$. Shear modulus, modulus of elasticity, loss factor, and both the real and the imaginary parts of the Poisson's ratio were determined for frequencies from 50 to 400Hz in the linear deformation regime (at relative deformations $10^{-4}{\sim}10^{-3}$).

RHEOLOGICAL CHARACTERIZATION OF COMPOSITES USING A VERTICAL OSCILLATION RHEOMETER (수직 진동형 Rheometer를 이용한 복합레진의 유변학적 성질의 측정)

  • Lee, In-Bog;Cho, Byung-Hoon;Son, Ho-Hyun;Lee, Sang-Tag;Um, Chung-Moon
    • Restorative Dentistry and Endodontics
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    • v.29 no.6
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    • pp.489-497
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    • 2004
  • Objective: The purpose of this study was to investigate the viscoelastic properties related to handling characteristics of composite resins, Methods: A custom designed vertical oscillation rheometer (VOR) was used for rheological measurements of composites. The VOR consists of three parts: (1) a measuring unit, (2) a deformation induction unit and (3) a force detecting unit, Two medium viscous composites, Z100 and Z250 and two packable composites, P60 and SureFil were tested. The viscoelastic material function, including complex modulus $E^{*}$ and phase angle ${\delta}$, were measured. A dynamic oscillatory test was used to evaluate the storage modulus (E'), loss modulus (E") and loss tangent ($tan{\delta}$) of the composites as a function of frequency ($\omega$) from 0.1 to 20 Hz at $23^{\circ}C$. Results: The E' and E" increased with increasing frequency and showed differences in magnitude between brands. The $E^{*}s$ of composites at ${\omega}{\;}={\;}2{\;}Hz$, normalized to that of Z100, were 2.16 (Z250), 4,80 (P60) and 25.21 (SureFil). The magnitudes and patterns of the change of $tan{\delta}$ of composites with increasing frequency were significantly different between brands. The relationships between the complex modulus $E^{*}$, the phase angle ${\delta}$ and the frequency \omega were represented by frequency domain phasor form, $E^{*}{\;}(\omega){\;}={\;}E^{*}e^{i{\delta}}{\;}={\;}E^{*}{\angle}{\delta}$. Conclusions: The viscoelasticity of composites that influences handling characteristics is significant different between brands, The VOR is a relatively simple device for dynamic, mechanical analysis of high viscous dental composites. The locus of frequency domain phasor plots in a complex plane is a valuable method of representing the viscoelastic properties of composites.