• Title/Summary/Keyword: Duplex Process

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A Study on the Duplex Treatment of Simultaneous Aluminizing-Chromizing and Plasma Nitriding for Improvement of Surface Properties (Al-Cr의 동시확산과 플라즈마 질화의 복합처리에의한 표면향상에 관한연구)

  • 양준혁;이상률;한전건
    • Journal of the Korean institute of surface engineering
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    • v.31 no.6
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    • pp.325-333
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    • 1998
  • A duplex surface treatment process of simultaneous aluminizing-chromizing process followed by plasma nitriding was performed on AISI HI3 steel and STS 403 steel. The properties of these duplex-treated steels were investigated and were compared with those of steels treated by single process of either simultaneous aluminizing-chromizing or plasma nilriding, in terms of microstructure, microhardness and high temperature wear resistance. Sim~dtaneous alumizing-chromizing process was done using a 2-step coating cycle and plasma nitriding process was done at $530^{\circ}C$ for 1.5 hour. AISI HI3 steel and STS 403 steel showed a FeA1 compound layer of approximately 350$\mu\textrm{m}$ thickness on the surface after simultaneous diffusion coating and nitrided layer of approximately 70-80$\mu\textrm{m}$ formed after the subsequent plasma nitriding process. The microhardness was improved much more by the duplex surface heatment than only by plasma nitriding. In addition the duplex treated specimens showed an improved high temperature wear resistance.

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STUDIES ON THE HIGH TEMPERATURE PROPERTIES OF DUPLEX-TREATED AISI H13 STEEL

  • Chung, J.W.;Lee, S.Y.;Kim, C.W.;Kim, S.S.;Han, J.G.;Lee, S.Y.
    • Journal of the Korean institute of surface engineering
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    • v.29 no.6
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    • pp.634-639
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    • 1996
  • In oder to improve the wear resistance as well as oxidation resistance at high temperature a AISI H13 steel was treated by a duplex process of calorizing followed by plasma nitriding. The surface properties of the duplex-treated AISI H13 steel was characterized and compared with those treated by single surface process of calorizing and plasma nitriding, in terms of microstruture, microhardness, wear resistance at $500^{\circ}C$, and the oxidation behaviours at $700^{\circ}C$, Duplex process on H13 steel had created duplex layer of approximately $190\mu\textrm{m}$ on the surface, and surface microhardness was measured to be above 1450Hv(0.1Kgf). There was considerable improvement of the high temperature wear resistance at $500^{\circ}C$ in the duplex-treated steel when both wear volume and weight change due to oxidation were considered. In addition the duplex-treated steel showed an improved high temperature oxidation resistance than the plasma nitrided steel at $700^{\circ}C$.

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A Study on the Formation Mechanism of Microconstituents in Brazed Joint of Duplex Stainless Steel and Cr-Cu Alloy (2상 스테인리스강과 크롬동합금의 브레이징부 생성상의 생성기구에 관한 연구)

  • 김대업
    • Journal of Welding and Joining
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    • v.19 no.5
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    • pp.534-539
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    • 2001
  • The formation mechanism of microconstituents in brazed joints of duplex stainless steel and Cr-Cu alloy which is an essential process of rocket engine manufacturing was investigated using Cu base insert metal. $SUS329J_3L$ and C18200 were used for base metal and AMS 4764 was used for insert metal. The brazing was carried out under various conditions. There were various phases in the joints, because of reaction between liquid insert metal and base metals. Since liquid insert metal reacts with duplex stainless steel, liquid Cu from insert metal infiltrated into the $\alpha/\beta$ interface of duplex stainless steel. Through the process of Cu infiltration, isolated stainless steel pieces come into the liquid insert metal. Since liquid insert metal reacts with Cr-Cu alloy. Cr precipitates from C18200 come into the liquid insert metal. With increment of bonding temperature and holding time, amounts and sizes of phases increased. but Cr-Mn compounds decreased at 1303k for 1.2ks and Mn-rich phases disappeared Fe-Cr compounds formed.

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Low Temperature Tensile Properties of High Temperature Gas-nitrided Duplex Stainless Steel

  • On, Han-Yong;Kong, Jung-Hyun;Kim, Mi-Jeong;Park, Sang-Joon;Kang, Chang-Yong;Sung, Jang-Hyun
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.5
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    • pp.263-268
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    • 2010
  • This investigation was focused on the low temperature tensile properties, phase change, changes in nitrogen content and corrosion resistance in the 22Cr-5Ni-3Mo duplex stainless steel after high temperature gas nitriding and solution annealing (HTGN-SA). From the HTGN-SA treatment, the duplex (ferrite + austenite) phase changed into austenite single phase. The nitrogen content of austenite single-phase steel showed a value of ~0.54%. For the HTGN-SA treated austenitic steel, tensile strength increased with lowering test temperature, on the other hand elongation showed the maximum value of 28.2% at $-100^{\circ}C$. The strain-induced martensitic transformation gave rise to lead the maximum elongation. After HTGN-SA treatment, corrosion resistance of the austenite single-phase steel increased remarkably compared with HTGN- treated steel.

Fabrication of Duplex Ceramic Composites by Organic-Inorganic Solution Process

  • Lee, Sang-Jin;Kim, Youn-Cheol
    • Journal of the Korean Ceramic Society
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    • v.40 no.9
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    • pp.837-841
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    • 2003
  • Duplex microstructure of zirconia and alumina has been achieved via an organic-inorganic solution technique. Zirconium 2,4-pentanedionate, aluminum nitrate and polyethylene glycol were dissolved in ethyl alcohol without any precipitation. The organicinorganic precursor gels were turned to porous powders having volume expansion through explosive, exothermic reaction during drying process. The volume expansion was caused by abrupt decomposition of the organic groups in the gels during the vigorous exothermic reaction. The volume expanded, porous powders were crystallized and densified at 1500$^{\circ}C$ for 1 h. At the optimum amount of the PEG polymer, the metal cations were well dispersed in the solution and a homogeneous polymeric network was formed. The polymer content also affected on the specific surface area of the synthesized powder and the grain size of the sintered composite.

Effect of oxygen content on impact toughness of austenitic-and duplex stainless steel weld metal (오스나이트계 및 이상계스테인레스강 용착부의 산소가 충격인성에 미치는 영향)

  • 문영훈;김환태;허성도
    • Journal of Welding and Joining
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    • v.5 no.3
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    • pp.38-45
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    • 1987
  • An investigation was conducted to find out the factors influencing on the impact toughness of austenitic-and duplex stainless steel weld metal. Various welding process with commerically available consumables was adopted to get weld doposited metal. The oxygen content of each weld metal was very sensitiive to welding process, involving flux composition, shielding gas and structural features. The results of this study show tat the content of oxygen as an oxide inclusion significantly affects impact toughness, and .delta.-ferrite distribution is also correlated with resultant toughness value.

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Link Adaptation for Full Duplex Systems

  • Kim, Sangchoon
    • International journal of advanced smart convergence
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    • v.7 no.4
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    • pp.92-100
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    • 2018
  • This paper presents a link adaptation scheme for adaptive full duplex (AFD) systems. The signal modulation levels and communication link patterns are adaptively selected according to the changing channel conditions. The link pattern selection process consists of two successive steps such as a transmit-receive antenna pair selection based on maximum sum rate or minimum maximum symbol error rate, and an adaptive modulation based on maximum minimum norm. In AFD systems, the antennas of both nodes are jointly determined with modulation levels depending on the channel conditions. An adaptive algorithm with relatively low complexity is also proposed to select the link parameters. Simulation results show that the proposed AFD system offers significant bit error rate (BER) performance improvement compared with conventional full duplex systems with perfect or imperfect self-interference cancellation under the same fixed sum rate.

Mechanical Properties of DLC Films and Duplex Plasma Nitriding/DLC Coating Treatment Process (DLC 박막과 복합처리(Nitriding/DLC)한 박막의 기계적 특성 비교)

  • Park, Hyun-Jun;Kim, Min-Chae;Kim, Sang-Sub;Moon, Kyoung-Il
    • Journal of the Korean institute of surface engineering
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    • v.53 no.6
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    • pp.306-311
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    • 2020
  • In this work, diamond-like carbon (DLC) films are coated onto plasma nitrided AISI 4140 steel by DC-pulsed PECVD. One problem of DLC films is their very poor adhesion on steel substrates. The purpose of the nitriding was to enhance adhesion between the substrate and the DLC films. The white layer formation is avoided. Plasma nitriding increased adhesion from 8 N for DLC coating to 25 N for duplex coating. Duplex plasma nitriding/DLC coating was proven to be more effective in improving the adhesion. The purpose of the bond layer was to enhance adhesion between the substrate and the DLC films.

Applicability of Air Cooling Heat-treatment for a Duplex Stainless Steel Casting (2상 스테인레스 주강의 공냉 열처리 적용 가능성)

  • Kim, Bong-Whan;Yang, Sik;Shin, Je-Sik;Lee, Sang-Mok;Moon, Byung-Moon
    • Journal of Korea Foundry Society
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    • v.26 no.1
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    • pp.17-26
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    • 2006
  • The substitution of cooling method from water quenching to air cooling after solution heat treatment was aimed for the development of a convenient and economical heat treatment process of duplex stainless steels without deterioration of mechanical and corrosion resistant properties for the industry. In order to achieve this goal, the mechanical properties and corrosion properties of a ASTM A890-4A duplex stainless steel were systematically investigated as functions of casting condition and cooling method after solution heat treatment. A 3-stepped sand mold and a permanent Y-block mold were used to check the effects of solidification structure and cooling rate after solution heat treatment. The microstructural characteristics such as the ferrite/austenite phase ratio and the precipitation behavior of ${\sigma}$ phase and carbides were investigated by combined analysis of OM and SEM-EDX with an aid of TTT diagram. Hardness and tension test were performed to evaluate the mechanical properties. Impact property at $-40^{\circ}C$ and corrosion resistance were also examined to check the possibility of the industrial application of this basic study. Throughout this investigation, air-cooling method was proved to effectively substitute for water-quenching process after the solution heat treatment, when the duplex stainless steel was sand mold cast with a thickness below 15 mm or permanent mold cast with a thickness below 20 mm.

Wear Characteristics of Al/SiCp Composites (SiC입자강화 알루미늄기 복합재료의 마모특성)

  • Kim, Sug-Won;Park, Jin-Sung;Ogi, K.
    • Journal of Korea Foundry Society
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    • v.22 no.4
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    • pp.184-191
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    • 2002
  • This study aims to investigate on the effects of alloying elements and heat treatment on the microstructures, wear and heat resistance of Al-Si-Cu-Mg-(Ni)/SiCp prepared by the duplex process developed in previous study, which consists of squeeze infiltration (1st process) and squeeze casting (2nd process). The hardness of composite increased with decrease in SiCp size and Ni addition in both the heat exposured composite and the as-cast one. And the heat and wear resisting properties was improved by the SiCp reinforcement and the Ni addition. The wear amount of Al/SiCp composite decreased with decreasing in the size of silicon carbide particle.