• Transactions of Materials Processing
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• v.15 no.2 s.83
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• pp.105-111
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• 2006

A study was made to investigate the microstructure and the mechanical properties of low-carbon steel, Al-Mg alloy and Ti-6Al-4V alloy each representing bcc, fcc and hcp crystal structures, respectively fabricated by equal-channel angular(ECA) pressing. After a series of ECA pressings was performed, most grains were significantly refined below ${\mu}m$ in diameter with high mis-orientation of grain boundaries irrespective of different crystal structure used. Regarding the strain hardening capability, tensile tests of ultrafine grain (UFG) dual-phase (ferrite/martensite) steel which was different from UFG ferrite-pearlite steel were carried out at ambient temperature, and corresponding mechanical properties were discussed in relation to modified C-J analysis. Low-temperature and/or high strain-rate superplasticity of the UFG Al-Mg alloy and UFG Ti-6Al-4V alloy were also studied. Based on the analysis used in this study, it was concluded that UFG alloys exhibited the enhanced mechanical properties as compared to coarse-grained (CG) counterparts.

• Transactions of the Korean Society of Automotive Engineers
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• v.15 no.3
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• pp.106-113
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• 2007

The effect of chemical composition on the microstructural change and tensile property in TRIP-assisted steels with different chemical composition was investigated by using SEM, TEM, XRD and UTM. As a result of microscopic observation, the morphology of retained austenite could be identified as two types : a granular type in a steel containing higher sillicon and a film type in a steel having higher carbon. For the case of higher carbon-containing steel with a tensile strength of 860 MPa and a total elongation of 38%, film-typed retained austenite could be observed between lath bainitic ferrite. Actually, metastable retained austenite was a requisite for the good formability, which means that chemical composition plays a significant role in the microstructure and tensile property of TRIP-assisted steels. With respect to tensile property, the steels containing suitable silicon and manganese, respectively, showed a typical TRIP effect in stress-strain curve, while a steel containing higher manganese content exhibited the assimilar behavior shown in dual phase steel.

• Journal of the Korean institute of surface engineering
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• v.45 no.6
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• pp.284-288
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• 2012

A study on microstructure control of multi-phase steel have been implemented to higher strength with improved formability. However, it is well known that the high strength of steel are susceptible to hydrogen embrittlement. The mechanisms of hydrogen embrittlement is caused by complex interactions. In this paper, the test specimens were fabricated to 5 type of 590DP steels at different levels of volume faction. The hydrogen charging was conducted by electrochemical hydrogen-charge method with varying charging time. The relationship between hydrogen concentration and volume fraction of 590DP steel was established by SP test and SEM-fractography. It was shown that the hydrogen amounts charged in 590DP steels increased with increasing the volume faction of austenite. The maximum loads of the 590DP steels in SP test were sharply decreased with increasing hydrogen charging time. The results of SEM-fractography investigation showed typical brittle-fracture surfaces for hydrogen-charged 590DP steels.

• Journal of Power System Engineering
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• v.16 no.5
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• pp.76-82
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• 2012

Duplex stainless steels have the dual microstructure of austenite and ferrite phases. This steel exhibits generally a high corrosion resistance and higher mechanical strength compared with austenitic stainless steels. The steels used in the investigation have the chemical composition of Fe-22Cr-xNi-yMn-0.2N in which the contents of Ni and Mn were varied with maintaining the equal [Ni/Cr] equivalent. The fraction of ferrite phase was increased with the increase of annealing temperature. The impact factor of Mn element on the [Ni] equivalent was amended on the basis of the results of the investigation. 4Mn-2Ni alloy showed the highest pitting corrosion resistance. The fraction ratio, grain size and misorientation angle between grains were measured, and the correlation with pitting potential was investigated.

• Corrosion Science and Technology
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• v.19 no.3
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• pp.146-155
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• 2020

To elucidate the effect of heat inputs on phase transformation and resistance to intergranular corrosion of F316 austenitic stainless steel (ASS), thermodynamic calculations of each phase and time-temperature-transformation diagram were conducted using JMaPro simulation software, oxalic acid etch test, double-loop electrochemical potentiokinetic reactivation test (DL-EPR), field emission scanning electron microscopy with energy dispersive spectroscopy, and transmission electron microscopy analyses of Cr carbide (Cr₂₃C₆), austenite phase and ferrite phase. F316 ASS containing a relatively low C content of 0.043 wt% showed a slightly sensitized microstructure (acceptably dual structure) due to a small amount of Cr carbide precipitated at heat affected zone irrespective of heat inputs. Based on results of DL-EPR test, although heat input was increased, the ratio of I_r to I_a was only increased very slightly due to a slight sensitization. Therefore, heat inputs have little influences on resistance to intergranular corrosion of F316 austenitic stainless steel containing 0.043 wt% C.

• Transactions of the Korean Society of Automotive Engineers
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• v.23 no.3
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• pp.279-286
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• 2015

To achieve lightweight design, research & development of various lightweighting technologies such as hydroforming are underway worldwide. In the case of hydroforming, application of ultra high strength steel is essential for weight reduction of the car. However, considering common high-strength carbon steel, it is not suitable to the actual hydroformed parts since the lack of formability. DP steel offers an outstanding combination of strength and formability as a result of their microstructure. DP steel has high strength and good formability but it's difficult to secure stable quality of welding section because of softening of weld section and chemical composition. Therefore, most of companies use LASER welding when making high strength tube. Electric resistance welding is excellent production method for steel tube manufacturing considering the productivity. Optimum electric resistance welding technology is needed to be developed for application of high strength hydroformed parts using DP steel. This study is comprehensive research & development from electric resistance welding to actual formabililty evaluation.

• Journal of Powder Materials
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• v.29 no.3
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• pp.233-239
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• 2022

Aluminum alloys are extensively employed in several industries, such as automobile, aerospace, and architecture, owing to their high specific strength and electrical and thermal conductivities. However, to meet the rising industrial demands, aluminum alloys must be designed with both excellent mechanical and thermal properties. Computer-aided alloy design is emerging as a technique for developing novel alloys to overcome these trade-off properties. Thus, the development of a new experimental method for designing alloys with high-throughput confirmation is gaining focus. A new approach that rapidly manufactures aluminum alloys with different compositions is required in the alloy design process. This study proposes a combined approach to rapidly investigate the relationship between the microstructure and properties of aluminum alloys using a direct energy deposition system with a dual-nozzle metal 3D printing process. Two types of aluminum alloy powders (Al-4.99Si-1.05Cu-0.47Mg and Al-7Mg) are employed for the 3D printing-based combined method. Nine types of Al-Si-Cu-Mg alloys are manufactured using the combined method, and the relationship between their microstructures and properties is examined.

• Journal of the Korean Society for Heat Treatment
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• v.34 no.6
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• pp.302-308
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• 2021

The aim of this study was to investigate the dependence of the hardness and thermal conductivity on the volume fraction of discontinuous precipitates (DPs) in the Mg-9.3%Al alloy with (α-(Mg)+DPs) dual phase structure. In order to obtain various DPs volume fractions, the alloy was solution-treated at 688 K for 24 h and then aged at 418 K for up to 144 h. The volume fraction of DPs increased from 0% to 63% with an increase in the aging time up to 72 h, over which, continuous precipitation was observed within the α-(Mg) grains. It is noticeable that the hardness and thermal conductivity of the alloy increased linearly with the volume fraction of DPs. The improved hardness and thermal conductivity with respect to volume fraction of DPs are closely associated with the higher hardness of the DPs with fine (α+β) lamellar structure and the lower Al concentration in the α phase layer of the DPs, respectively.

• Applied Microscopy
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• v.50
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• pp.24.1-24.11
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• 2020

The development of the femtosecond laser (fs laser) with its ability to provide extremely rapid athermal ablation of materials has initiated a renaissance in materials science. Sample milling rates for the fs laser are orders of magnitude greater than that of traditional focused ion beam (FIB) sources currently used. In combination with minimal surface post-processing requirements, this technology is proving to be a game changer for materials research. The development of a femtosecond laser attached to a focused ion beam scanning electron microscope (LaserFIB) enables numerous new capabilities, including access to deeply buried structures as well as the production of extremely large trenches, cross sections, pillars and TEM H-bars, all while preserving microstructure and avoiding or reducing FIB polishing. Several high impact applications are now possible due to this technology in the fields of crystallography, electronics, mechanical engineering, battery research and materials sample preparation. This review article summarizes the current opportunities for this new technology focusing on the materials science megatrends of engineering materials, energy materials and electronics.

• Transactions of Materials Processing
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• v.32 no.3
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• pp.107-113
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• 2023

The importance of dual-fuel engines has increased for reducing CO₂ emissions. However, the low operating temperature of this engine may induce low-temperature corrosion at combustion parts, which reduces the engine service life. To overcome this problem, NiCr38Al4 alloy was developed for valve spindle, but the cost of this alloy is expensive due to its high Cr content. For reducing the manufacturing cost of valve spindle, in the present work, NiCr38Al4 alloy was welded with Nimonic80A alloy by conducting friction welding. The tensile test results show that the strength of friction-welded specimens follows the properties of the lower-strength parent materials, without severe cracks at the interface. The large shear strain and frictional heat from friction welding not only reduce grain size but also induce solute element diffusion at the interfacial region. Because of the low Cr diffusivity compared with Ti, Cr carbides were not observed in the Nimonic80A matrix, while Ti carbides were distributed in both the Nimonic80A and SNCrW matrices.