• Title/Summary/Keyword: Drying plate

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Freeze Drying Process and Pore Structure Characteristics of Porous Cu with Various Sublimable Vehicles (다양한 동결제를 이용하여 동결건조 공정으로 제조한 Cu 다공체의 기공구조 특성)

  • Lee, Gyuhwi;Oh, Sung-Tag;Suk, Myung-Jin;Jeong, Young-Keun
    • Journal of Powder Materials
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    • v.27 no.3
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    • pp.198-202
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    • 2020
  • The effect of sublimable vehicles on the pore structure of Cu fabricated by freeze drying is investigated. The 5 vol% CuO-dispersed slurries with camphene and various camphor-naphthalene compositions are frozen in a Teflon mold at -25℃, followed by sublimation at room temperature. After hydrogen reduction at 300℃ and sintering at 600 ℃, the green bodies of CuO are completely converted to Cu with various pore structures. The sintered samples prepared using CuO/camphene slurries show large pores that are aligned parallel to the sublimable vehicle growth direction. In addition, a dense microstructure is observed in the bottom section of the specimen where the solidification heat was released, owing to the difference in the solidification behavior of the camphene crystals. The porous Cu shows different pore structures, such as dendritic, rod-like, and plate shaped, depending on the composition of the camphornaphthalene system. The change in pore structure is explained by the crystal growth behavior of primary camphor and eutectic and primary naphthalene.

Influence of Differential Moisture Distribution on SRC Column Shortening

  • Seol Hyun-Cheol;Kim Jin-Keuna;Kim Yun-Yonga;Kwon Seung-Heea
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05a
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    • pp.423-426
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    • 2005
  • Steel reinforced concrete (SRC) columns, which are widely employed in high-rise buildings, exhibit particular time-dependent behavior due to creep and shrinkage of the concrete, and this behavior may cause problems related to serviceability and structural stability. SRC columns also exhibit a time-dependent, cross-sectional relative humidity distribution that differs from reinforced concrete (RC) columns, due to the presence of an inner steel plate, which interferes with the moisture diffusion of concrete. This differential moisture distribution of SRC columns may reduce the drying shrinkage and the drying creep as contrasted with RC columns. Therefore, we propose that the differential moisture distribution be taken into account to accurately predict SRC column shortening.

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Development of Microarrayer for Manufacturing DNA Chip (DNA 칩 제작을 위한 로봇 시스템의 개발)

  • 이현동;김기대;나건영;임용표
    • Journal of Biosystems Engineering
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    • v.28 no.5
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    • pp.429-438
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    • 2003
  • This study exploits the robot system which is necessary in gene study and bio-technology industry. As well, a DNA chip, which of use has been increased recently, can be manufactured with this system. The robot consists of a device spotting DNA on the silylated slide, a well plate, a bed for fixing well plates, devices of washing and drying the pin in DNA spotting .device, a distillation-water vessel, and a discharge vessel of wash water. We made the period of sticking DNA to the pin on the well plate to be 15 seconds. The spot size of DNA was set to be 0.28 mm on the average by bringing the slide into contact with pin during 1 second. If DNA is spotted in minimum space possible about 0.32mm, this system can stick about 8,100 DNA spots on the well plate with this rate. Analyzing the procedure: Movement starts, Pin washes, dries, and smears DNA on the well plate. Spotting DNA onto 12 chips took 2 minutes and 50 seconds.

The Effect of Sample Handling on the Rheological Measurement of Regenerated Silk Fibroin Formic Acid Solution using Parallel Plate Geometry

  • Cho, Hee-Jung;Um, In-Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • v.22 no.1
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    • pp.5-10
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    • 2011
  • The effect of sample handling condition on the rheological measurement of regenerated silk fibroin formic acid solution using parallel plate geometry was investigated. In case of loading method, the loading by pouring sample solution resulted in the best reproducibility of rheological measurement. Loading with spoon showed a high variance of viscosity value at low shear rate region ($0.01{\sim}1sec^{-1}$) while loading with syringe exhibited a low reproducibility of viscosity at high shear region ($1{\sim}100sec^{-1}$) with a disappearance of shear thinning phenomenon. It was revealed that the sample loading with small extra amount lead to the most reproducible result. The sample loading with the exact amount for the measuring plate resulted in a lack of reproducibility of high shear viscosity, while the loading with large extra volume produced a limited consistency of low shear viscosity. It was turned out that 3 min. of waiting time before measurement was the optimum condition for reliable result. When the waiting time was less than 1 min., the low shear viscosity was obtained with a lack of consistency. On the other hand, the sample solution started drying when the waiting time increased up to 5 min.

Development of microarrayer for manufacturing DNA chip used in genome project (유전자 검색을 위한 DNA 칩 제작용 microarrayer의 개발)

  • Lee, Hyun-Dong;Kim, Ki-Dae;Kim, Chan-Soo;Lim, Yong-Pyo;Park, Jung-Kyu
    • Korean Journal of Agricultural Science
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    • v.30 no.1
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    • pp.76-88
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    • 2003
  • This study exploits the robot system which is necessary in gene study, bio-technology industry. As well, it can achieve the job of DNA chip manufacturing whose use rate has been increased recently. The robot consists of DNA spotting device for spotting DNA on the silylated slide and well plate, bed for fixing well-plate, washing & drying device of washing and drying the pin part of DNA spotting device, distillation-water vessel, and discharge vessel of wash water. We made the term of sticking DNA to the pin on well plate to be 15 seconds. The spot size of DNA was set to be 0.28 mm on the average by bringing the slide into contact with pin for 1 second. At this rate, if DNA is spotted in the minimum space possible of about 0.32mm, it can stick about 8,100 DNA spots on the well plate. Analyzing the procedure: Movement starts. Pin washes, dries, and smears DNA on the well plate. Spots DNA onto 12 chips takes 2 minutes and 50 seconds.

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Long-term Behavior of Deck-plate Concrete Slab Reinforced with Steel Fiber (강섬유 보강 데크플레이트 콘크리트 슬래브의 장기 거동)

  • Hong, Geon-Ho;Hwang, Seung-Koo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.4
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    • pp.30-38
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    • 2017
  • Recently, research on the development of a composite slab system for shorting the construction period by simplifying the process by omitting the form work and the reinforcement placing is underway. The purpose of this study is to evaluate the long-term behavior of a simplified slab system that replaces the form work and tensile reinforcement using structural deck-plate and replaces the temperature reinforcement using steel fiber reinforced concrete. In the conventional composite deck-plate slab method, w.w.f is generally used for crack control by drying shrinkage. But previous research results by various researchers were pointed out it is not effective to control the shrinkage and temperature cracking. In this study, the long-term cracking and structural behavior of steel fiber reinforced deck plate slab specimen with two continuous spans constructed under typical load conditions were evaluated. Experimental results showed that the number and width of long-term cracks decreased remarkably in the simplified slab specimen, and the deflection was also decreased compared with conventional RC slab specimen. However, in the continuous end of the slab where the negative moment is applied, it is analyzed that reinforced details are necessary to control the crack width in the service load and to recover deflection at load removal.

Application Performances of the Simplified Solar Collectors and for the Drying of Red Pepper (간이(簡易) 태양열(太陽熱) 집열기(集熱器)의 유형별(類型別) 분석(分析) 및 고추건조(乾燥)에의 이용(利用))

  • Choi, Boo-Dol;Chun, Jae-Kun
    • Korean Journal of Food Science and Technology
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    • v.18 no.6
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    • pp.479-484
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    • 1986
  • Two different types of solar collector for farm dryer- the flatplate type and the modified tubular type-were constructed and analyzed on their performances. The transparent plastic film, black painted galvanized iron sheet and black vinyl film were used for the cover and absorber of the flat-plate types. The simplified tubular type was constructed with transparent films for the cover and black vinyl films for the absorber Two elliptical iron rings were used to form a tubular shape through which air could pass. No remarkable differences were found in thermal efficiences between the absorbers made with galvanized iron sheet and black vinyl film. The average thermal efficiencies of the solar collectors were 42.8%(max.48.2%, min.38.2%) for flat plate type and 22.971 (max. 25.4%, min. 14.8%)) for tubular one. The empirical equations were proved to be applicable to the prediction of temperature elevation. The tubular solar heat collector was successfully applied to red peppers drying as a practical farm dryer. The drying rate was almost doubled compared to a conventional sun drying.

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Study on the Performance of the Flat-Plate Solar Collectors (평면식 태양열 집열기의 성능에 관한 연구)

  • 장규섭;김만수
    • Journal of Biosystems Engineering
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    • v.2 no.2
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    • pp.37-45
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    • 1977
  • Solar energy is a potential source of power that offers much promise being used for low-temperature applications like drying farm crops, space heating, and water heating for domestic uses. Already much of it are being used for those purpose in foreign countries. However, very little research has been done to determine the possibility of using the solar energy in Korea. This study was conducted to develop the general prediction equation of the total radiation on a horizontal surface in Daejeon area based on 5 years 91972, Jun.1-1976. Dec.31) meteorological data (bright sunshine hours, average total horizontal radiation), and to obtain experimentally the thermal efficiency of solar air and water collectors, which will be used as a basic data of designing flat-plate solar collector system.In addition to the thermal efficiency of the collectorsthe relationship among those factors affecting it such as weather condition, orientation factor, and tilted angle of collector was analyzed. The results of this study were as follows. 1. The general predicted equation of the total radiation on a horizontal surface in Daejeon area based on bright sunshine hours was developed as $H_{av} =(1.546\frac{n}{N}-0.582)H_o$. Predicting the total radiation on a horizontal surface by the above equation was thought to be possible because to values of 0.882 was smaller than any t values at above 0.05 level on the basis of two tailed test of the difference between the calculated and the recorded values. 2.It was observed that optimum tilt angle of the collector in the summer and the autumn drying season was 13 degrees and 51 degrees respectively, these values could be obtained by adding or substracting approximately 25 degrees from the latitude of this area $(36.3^{\circ}N)$ .The relationship between orientation factor and declination of sun at suitable tilt angle of 33 degrees $(s=0.9\O)$ was shown at Fig.4. 3.The thermal efficiency of solar wdter collector was shown 13.4-51. 6% on Aug. 15 (the minimum radiation recorded) and 43.8 ~537% Aug.20 (the maximum radiation recorded), and 13.8~ 46.6 and 44.3~ 49.7 were shown on each corresponding day. 4.The thermal efficiency of the collectors according to the weather condition was shown a big difference of about 10% between the day of the maximum radiation recorded and the minimum, but the differen of efficiency between the air and the water collector was at most 2 ~ 3%. 5. Even if the efficiency of the solar water collector was a little higher than the solar air collector, for drying farm products, the solar air collector was thought to be more effective because the air heated by collector could be directly used for drying them.

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Toothbrush sterilizing effects of using microwave (Microwave를 이용한 칫솔 살균효과)

  • Ji, Yun-Jeong
    • Journal of Korean society of Dental Hygiene
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    • v.12 no.3
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    • pp.641-646
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    • 2012
  • Objectives : The purpose of this study is to analyze the sterilizing effects of toothbrushes by administering bacteria into toothbrushes and reproducing the antibacterial effects using a microwave oven. Methods : The heads of four-row mid-strength toothbrushes were cut, put in a bacterial solution ($3{\times}10^9cells/ml$) for vortexing, and sterilized with microwaves for 0, 30, and 60 seconds. They were then moved into four tubes containing DW 10 ml and suspended in a vortex mixer for two minutes to separate bacteria from them. DW 9ml was added by 1ml of bacteria for dilution of $10{\sim}10^6$ times. It was then administered to the BHI agar plate by 0.1ml and cultured at $37^{\circ}C$ for 24 hours. Total number of bacteria adhered to a toothbrush was obtained by multiplying the number of colonies by the dilution factor. The experiment was done in the first, second, and third step, being repeated in a normal temperature drier ($23^{\circ}C$) after 5, 9 and 24 hours. Results : The results of the experiment revealed that the sterilizing effects were 95% or over. When toothbrushes were sterilized for 60 seconds, the number of colonies is about 11 after drying for 5 hours, 7 after drying for 9 hours and 2 after drying for 24 hours. The sterilizing effects reached 98% when the bacteria-administered toothbrush was sterilized for 1 minute after drying for 24 hours. Conclusions : The results demonstrated that toothbrush sterilizing by using microwave is a suitable way to prevent cross-contamination of toothbrushes by oral bacterial infection and thus easy to use at home. However, this study suggests that toothbrush sterilizing by using microwave should be limited within two times a week because the physical properties of toothbrush might be changed.

Synthesis and Microstructure of Porous Al2O3 with Nano-Sized Cu Dispersions (나노크기 Cu 분산입자를 갖는 Al2O3 다공체의 제조 및 미세조직 특성)

  • Yoo, Ho-Suk;Kim, An-Gi;Hyun, Chang-Yong
    • Korean Journal of Materials Research
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    • v.23 no.1
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    • pp.67-71
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    • 2013
  • Porous $Al_2O_3$ dispersed with nano-sized Cu was fabricated by freeze-drying process and solution chemistry method using Cu-nitrate. To prepare porous $Al_2O_3$, camphene was used as the sublimable vehicle. Camphene slurries with $Al_2O_3$ content of 10 vol% were prepared by milling at $50^{\circ}C$ with a small amount of oligomeric polyester dispersant. Freezing of the slurry was done in a Teflon cylinder attached to a copper bottom plate cooled to $-25^{\circ}C$ while unidirectionally controlling the growth direction of the camphene. Pores were subsequently generated by sublimation of the camphene during drying in air for 48 h. The green body was sintered in a furnace at $1400^{\circ}C$ for 1 h. Cu particles were dispersed in porous $Al_2O_3$ by calcination and hydrogen reduction of Cu-nitrate. The sintered samples showed large pores with sizes of about $150{\mu}m$; these pores were aligned parallel to the camphene growth direction. Also, the internal walls of the large pores had relatively small pores due to the traces of camphene left between the concentrated $Al_2O_3$ particles on the internal wall. EDS analysis revealed that the Cu particles were mainly dispersed on the surfaces of the large pores. These results strongly suggest that porous $Al_2O_3$ with Cu dispersion can be successfully fabricated by freeze-drying and solution chemistry routes.